Research Article
BibTex RIS Cite

Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi

Year 2025, Volume: 14 Issue: 2, 1 - 1

Abstract

Yapılan bu çalışmada toz metalürjisi ve sıcak presleme yöntemleriyle Al7075 matrise ağırlıkça %1, 3, 6, 9 ve 12 katkı oranlarında Si3N4 ilave edilerek kompozit malzemeler üretilmiştir. Üretilen kompozitlere yoğunluk, Vickers sertliği, aşınma ve sürtünme testleri uygulanmıştır. Ayrıca kompozitlerin mikroyapılarını incelemek amacıyla XRD, SEM ve SEM-EDX analizleri yapılmıştır. Sonuç olarak en yüksek deneysel yoğunluk (2.65 g/cm3), en yüksek Vickers sertliği (205 HV), en düşük aşınma oranı (0.00018 mm3/(Nm)), en düşük kütle kaybı (0.0025 g) ve en düşük sürtünme katsayısı (0.38) değerleri Al7075-%9 Si3N4 kompozitte elde edilmiştir. Ancak ağırlıkça %12 Si3N4 katkı oranında takviye partiküllerinin topaklanmasından dolayı kompozitin tribolojik özellikleri kötüleşmiştir. Sonuç olarak Al7075 matrise %9 Si3N4 katkısının kompozitin tribolojik özelliklerini iyileştirdiği tespit edilmiştir.

References

  • S. A. Kumar, J. H. Vignesh, and S. P. Joshua, Investigating the effect of porosity on aluminium 7075 alloy reinforced with silicon nitride (Si3N4) metal matrix composites through STIR casting process. Materials Today: Proceedings, 39, 414–419, 2020. https://doi.org/10.1016/j.matpr.2020.07.690.
  • V. V. B. Gurrappa, I., and Prasad, Corrosion characteristics of aluminium based metal matrix composites, Journal of Materials Science & Technology, 22, 115–122, 2006.
  • N. Ramadoss, K. Pazhanivel, A. Ganeshkumar, and M. Arivanandhan, Microstructural, mechanical and corrosion behaviour of B4C/BN-reinforced Al7075 matrix hybrid composites. International Journal of Metalcasting, 17(1), 499–514, 2023. https://doi.org/ 10.1007/s40962-022-00791-z.
  • S. Devaganesh, P. K. D. Kumar, N. Venkatesh, and R. Balaji, Study on the mechanical and tribological performances of hybrid SiC-Al7075 metal matrix composites. Journal of Materials Research and Technology, 9(3), 3759–3766, 2020. https://doi.org/ 10.1016/j.jmrt.2020.02.002.
  • S. Manghnani, D. Shekhawat, C. Goswami, T. K. Patnaik, and T. Singh, Mechanical and tribological characteristics of Si3N4 reinforced aluminium matrix composites: A short review. Materials Today: Proceedings, 44, 4059–4064, 2020. https://doi.org/ 10.1016/j.matpr.2020.10.440.
  • N. H. Alharthi, S. M. Almotairy, and A. M. Almutairi, Frictional Behavior and Mechanical Performance of Al Reinforced with SiC via Novel Flake Powder Metallurgy. Metals (Basel), 12(2), 2022. https://doi.org/10.3390/met12020323.
  • J. M. Mistry and P. P. Gohil, Experimental investigations on wear and friction behaviour of Si3N 4p reinforced heat-treated aluminium matrix composites produced using electromagnetic stir casting process. Composites Part B: Engineering, 161, 190–204, 2019. https://doi.org/10.1016/j.compositesb.20 18.10.074.
  • G. B. V. Kumar, P. Prasad, N. Suresh, R. Pramod, and C. S. P. Rao, Assessment of mechanical and tribological characteristics of Silicon Nitride reinforced aluminum metal matrix composites. Composites Part B: Engineering, 175, 107138, 2019. https://doi .org/10.1016/j.compositesb.2019.107138.
  • V. Mohanavel, K. S. A. Ali, S. Prasath, T. Sathish, and M. Ravichandran, Microstructural and tribological characteristics of AA6351/Si3N4 composites manufactured by stir casting. Journal of Materials Research and Technology, 9(6), 14662–14672, 2020. https://doi.org/10.1016/j.jmrt.2020.09.128.
  • P. Ramu, R. H. K. Reddy, B. K. Kumar, T. Padmanathan, and M. V Phanibhushana, Materials Today : Proceedings Investigation of wear characteristics of Al6061-Si3N4 composites subjected to strain hardening through Equal Channel Angular Pressing. Materials Today: Proceedings, 46, 790–794, 2021. https://doi.org/10.1016/j.matpr.2020.12.765.
  • D. S. R. Smart, J. P. Kumar, and C. Periasamy, Materials Today : Proceedings Microstructural, mechanical and wear characteristics of AA7075/TaC/Si3N4/Ti based hybrid metal matrix composite material. Materials Today: Proceedings, 43, 784–794, 2021. https://doi.org/10.1016/j.matpr. 2020.06.169.
  • M. Şenel and Ü. Mahmutoğlu, Effect of induction heat treatment on the mechanical propertiesof Si3N4–graphene-reinforced Al2024 hybrid composites. Bulletin of Materials Science, 45(1), 1–17, 2022.
  • S. Bai, N. Perevoshchikova, Y. Sha, and X. Wu, Applied sciences the effects of selective laser melting process parameters on relative density of the AlSi10Mg parts and suitable procedures of the archimedes method. 2019, https://doi.org/10.3390/app9030583.
  • M. C. Şenel and M. Üstün, Dry sliding wear and friction behavior of graphene/ZrO2 binary nanoparticles reinforced aluminum hybrid composites. Arabian Journal for Science and Engineering, 47(7), 9253–9269, 2022. https://doi.org/10.1007/s13369-022-06661-4.
  • M. C. Şenel, M. Gürbüz, E, Koç, Fabrication and characterization of SiC and Si3N4 reinforced aluminum matrix composites. Universal Journal of Materials Science, 5(4), 95, 2017.
  • Z. Ahmad, S. Khan, S, S. Hasan, Microstructural characterization and evaluation of mechanical properties of silicon nitride reinforced LM 25 composite. Journal of Materials Research and Technology, 9(4), 9129-9135, 2020.
  • V. V. Zakorzhevskii, I. P. Borovinskaya, Combustion synthesis of silicon nitride using ultrafine silicon powders. Powder Metallurgy and Metal Ceramics, 48, 375-380, 2009.
  • G. Anbuchezhiyan, B. Mohan, N. Senthilkumar, R. Pugazhenthi, Synthesis and characterization of silicon nitride reinforced Al–Mg–Zn alloy composites. Metals and Materials International, 27, 3058-3069, 2021.
  • R. K. Arya, R. Kumar, A. Telang, Influence of microstructure on tribological behaviors of Al6061 metal matrix composite reinforced with silicon nitride (Si3N4) and silicon carbide (SiC) micro particles. Silicon, 15(9), 3987-4001, 2023.
  • W. Zhai, X. Shi, J. Yao, A. M. M. Ibrahim, Z. Xu, Q. Zhu, Y. Xiao, L. Chen, Q. Zhang, Investigation of mechanical and tribological behaviors of multilayer graphene reinforced Ni3Al matrix composites. Composites Part B: Engineering, 70, 149-155, 2015.
  • P. P. Venkat, P. C. Naidu, L. P. Kumar, K. V. Babu, M. K. Prasad, M. V. Rao, Effect of Al2O3 particles on mechanical, microstructural and tribological characteristics of Al5052 metal matrix composite reinforced with Si3N4 particles. Materials Today: Proceedings, 91, 158-166, 2023.
  • D. Bhuvanesh, N. Radhika, A. V. Vidyapeetham, Experimental investigation on tribological characteristics of silicon nitride reinforced aluminium metal matrix composites. Journal of Engineering Science and Technology, 12(5), 1295-1306, 2017.

Investigation of microstructure and tribological properties of Si3N4 reinforced Al7075 matrix composites

Year 2025, Volume: 14 Issue: 2, 1 - 1

Abstract

In this study, composite materials were fabricated by Si3N4 reinforcement (1, 3, 6, 9, and 12wt.%) to the Al7075 matrix using the powder metallurgy and hot-pressing methods. Density, Vickers hardness, wear, and friction tests were applied to the fabricated composites. In addition, XRD, SEM, and SEM-EDX analyses were performed to examine the microstructures of the composites. As a result, the highest experimental density (2.65 g/cm3), the highest Vickers hardness (205 HV), the lowest wear rate (0.00018 mm3/(Nm)), the lowest mass loss (0.0025 g), and the lowest friction coefficient (0.38) values were obtained in the Al7075-9% Si3N4 composite. However, the tribological properties of the composite deteriorated due to the agglomeration of the reinforcement particles at the 12wt.% Si3N4 content. As a result, it was determined that 9% Si3N4 addition to the Al7075 matrix improved the tribological properties of the composite.

References

  • S. A. Kumar, J. H. Vignesh, and S. P. Joshua, Investigating the effect of porosity on aluminium 7075 alloy reinforced with silicon nitride (Si3N4) metal matrix composites through STIR casting process. Materials Today: Proceedings, 39, 414–419, 2020. https://doi.org/10.1016/j.matpr.2020.07.690.
  • V. V. B. Gurrappa, I., and Prasad, Corrosion characteristics of aluminium based metal matrix composites, Journal of Materials Science & Technology, 22, 115–122, 2006.
  • N. Ramadoss, K. Pazhanivel, A. Ganeshkumar, and M. Arivanandhan, Microstructural, mechanical and corrosion behaviour of B4C/BN-reinforced Al7075 matrix hybrid composites. International Journal of Metalcasting, 17(1), 499–514, 2023. https://doi.org/ 10.1007/s40962-022-00791-z.
  • S. Devaganesh, P. K. D. Kumar, N. Venkatesh, and R. Balaji, Study on the mechanical and tribological performances of hybrid SiC-Al7075 metal matrix composites. Journal of Materials Research and Technology, 9(3), 3759–3766, 2020. https://doi.org/ 10.1016/j.jmrt.2020.02.002.
  • S. Manghnani, D. Shekhawat, C. Goswami, T. K. Patnaik, and T. Singh, Mechanical and tribological characteristics of Si3N4 reinforced aluminium matrix composites: A short review. Materials Today: Proceedings, 44, 4059–4064, 2020. https://doi.org/ 10.1016/j.matpr.2020.10.440.
  • N. H. Alharthi, S. M. Almotairy, and A. M. Almutairi, Frictional Behavior and Mechanical Performance of Al Reinforced with SiC via Novel Flake Powder Metallurgy. Metals (Basel), 12(2), 2022. https://doi.org/10.3390/met12020323.
  • J. M. Mistry and P. P. Gohil, Experimental investigations on wear and friction behaviour of Si3N 4p reinforced heat-treated aluminium matrix composites produced using electromagnetic stir casting process. Composites Part B: Engineering, 161, 190–204, 2019. https://doi.org/10.1016/j.compositesb.20 18.10.074.
  • G. B. V. Kumar, P. Prasad, N. Suresh, R. Pramod, and C. S. P. Rao, Assessment of mechanical and tribological characteristics of Silicon Nitride reinforced aluminum metal matrix composites. Composites Part B: Engineering, 175, 107138, 2019. https://doi .org/10.1016/j.compositesb.2019.107138.
  • V. Mohanavel, K. S. A. Ali, S. Prasath, T. Sathish, and M. Ravichandran, Microstructural and tribological characteristics of AA6351/Si3N4 composites manufactured by stir casting. Journal of Materials Research and Technology, 9(6), 14662–14672, 2020. https://doi.org/10.1016/j.jmrt.2020.09.128.
  • P. Ramu, R. H. K. Reddy, B. K. Kumar, T. Padmanathan, and M. V Phanibhushana, Materials Today : Proceedings Investigation of wear characteristics of Al6061-Si3N4 composites subjected to strain hardening through Equal Channel Angular Pressing. Materials Today: Proceedings, 46, 790–794, 2021. https://doi.org/10.1016/j.matpr.2020.12.765.
  • D. S. R. Smart, J. P. Kumar, and C. Periasamy, Materials Today : Proceedings Microstructural, mechanical and wear characteristics of AA7075/TaC/Si3N4/Ti based hybrid metal matrix composite material. Materials Today: Proceedings, 43, 784–794, 2021. https://doi.org/10.1016/j.matpr. 2020.06.169.
  • M. Şenel and Ü. Mahmutoğlu, Effect of induction heat treatment on the mechanical propertiesof Si3N4–graphene-reinforced Al2024 hybrid composites. Bulletin of Materials Science, 45(1), 1–17, 2022.
  • S. Bai, N. Perevoshchikova, Y. Sha, and X. Wu, Applied sciences the effects of selective laser melting process parameters on relative density of the AlSi10Mg parts and suitable procedures of the archimedes method. 2019, https://doi.org/10.3390/app9030583.
  • M. C. Şenel and M. Üstün, Dry sliding wear and friction behavior of graphene/ZrO2 binary nanoparticles reinforced aluminum hybrid composites. Arabian Journal for Science and Engineering, 47(7), 9253–9269, 2022. https://doi.org/10.1007/s13369-022-06661-4.
  • M. C. Şenel, M. Gürbüz, E, Koç, Fabrication and characterization of SiC and Si3N4 reinforced aluminum matrix composites. Universal Journal of Materials Science, 5(4), 95, 2017.
  • Z. Ahmad, S. Khan, S, S. Hasan, Microstructural characterization and evaluation of mechanical properties of silicon nitride reinforced LM 25 composite. Journal of Materials Research and Technology, 9(4), 9129-9135, 2020.
  • V. V. Zakorzhevskii, I. P. Borovinskaya, Combustion synthesis of silicon nitride using ultrafine silicon powders. Powder Metallurgy and Metal Ceramics, 48, 375-380, 2009.
  • G. Anbuchezhiyan, B. Mohan, N. Senthilkumar, R. Pugazhenthi, Synthesis and characterization of silicon nitride reinforced Al–Mg–Zn alloy composites. Metals and Materials International, 27, 3058-3069, 2021.
  • R. K. Arya, R. Kumar, A. Telang, Influence of microstructure on tribological behaviors of Al6061 metal matrix composite reinforced with silicon nitride (Si3N4) and silicon carbide (SiC) micro particles. Silicon, 15(9), 3987-4001, 2023.
  • W. Zhai, X. Shi, J. Yao, A. M. M. Ibrahim, Z. Xu, Q. Zhu, Y. Xiao, L. Chen, Q. Zhang, Investigation of mechanical and tribological behaviors of multilayer graphene reinforced Ni3Al matrix composites. Composites Part B: Engineering, 70, 149-155, 2015.
  • P. P. Venkat, P. C. Naidu, L. P. Kumar, K. V. Babu, M. K. Prasad, M. V. Rao, Effect of Al2O3 particles on mechanical, microstructural and tribological characteristics of Al5052 metal matrix composite reinforced with Si3N4 particles. Materials Today: Proceedings, 91, 158-166, 2023.
  • D. Bhuvanesh, N. Radhika, A. V. Vidyapeetham, Experimental investigation on tribological characteristics of silicon nitride reinforced aluminium metal matrix composites. Journal of Engineering Science and Technology, 12(5), 1295-1306, 2017.
There are 22 citations in total.

Details

Primary Language Turkish
Subjects Material Design and Behaviors
Journal Section Articles
Authors

Aleyna Taşkın 0000-0002-8308-9957

Elif Işık 0000-0001-8289-9512

Mahmut Can Şenel 0000-0001-7897-1366

Early Pub Date March 3, 2025
Publication Date
Submission Date October 1, 2024
Acceptance Date January 22, 2025
Published in Issue Year 2025 Volume: 14 Issue: 2

Cite

APA Taşkın, A., Işık, E., & Şenel, M. C. (2025). Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, 14(2), 1-1. https://doi.org/10.28948/ngumuh.1559381
AMA Taşkın A, Işık E, Şenel MC. Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi. NOHU J. Eng. Sci. March 2025;14(2):1-1. doi:10.28948/ngumuh.1559381
Chicago Taşkın, Aleyna, Elif Işık, and Mahmut Can Şenel. “Si3N4 katkılı Al7075 Matrisli Kompozitlerin mikroyapısının Ve Tribolojik özelliklerinin Incelenmesi”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 14, no. 2 (March 2025): 1-1. https://doi.org/10.28948/ngumuh.1559381.
EndNote Taşkın A, Işık E, Şenel MC (March 1, 2025) Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 14 2 1–1.
IEEE A. Taşkın, E. Işık, and M. C. Şenel, “Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi”, NOHU J. Eng. Sci., vol. 14, no. 2, pp. 1–1, 2025, doi: 10.28948/ngumuh.1559381.
ISNAD Taşkın, Aleyna et al. “Si3N4 katkılı Al7075 Matrisli Kompozitlerin mikroyapısının Ve Tribolojik özelliklerinin Incelenmesi”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 14/2 (March 2025), 1-1. https://doi.org/10.28948/ngumuh.1559381.
JAMA Taşkın A, Işık E, Şenel MC. Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi. NOHU J. Eng. Sci. 2025;14:1–1.
MLA Taşkın, Aleyna et al. “Si3N4 katkılı Al7075 Matrisli Kompozitlerin mikroyapısının Ve Tribolojik özelliklerinin Incelenmesi”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, vol. 14, no. 2, 2025, pp. 1-1, doi:10.28948/ngumuh.1559381.
Vancouver Taşkın A, Işık E, Şenel MC. Si3N4 katkılı Al7075 matrisli kompozitlerin mikroyapısının ve tribolojik özelliklerinin incelenmesi. NOHU J. Eng. Sci. 2025;14(2):1-.

download