Synthesis of barium metaborate from boric acid with microwave assisted method
Abstract
Barium metaborate (BaO.B2O3 /BaB2O4) is a very often used additive that uses in dyes, plactics, textile, rubber, glue industry and for protection of wood meterials but it doesn’t produce in Turkey. β-barium metaborate crystal, the low-temperature phase of barium metaborate, is a non-linear optical crystal which has perfect properties. In this experimental study, microwave assisted synthesis was examined to produce barium metaborate for the first time. The experiments were carried out by microwave power level in 270W, 360W and 600W with 1,2,3,4 and 5 min. reaction times. The effects of microwave power level and reaction times changes on the production yield were determined. The 86% production yield was reached in reaction conditions of 360W and 3 min. After the heat treatment in 620 °C, the powder which has the same crystal phase with β- BaB2O4 was produced.
Keywords
References
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Details
Primary Language
English
Subjects
Industrial Biotechnology
Journal Section
Research Article
Publication Date
March 1, 2013
Submission Date
December 31, 2012
Acceptance Date
February 18, 2013
Published in Issue
Year 2013 Volume: 31 Number: 1
APA
Akşener, A. E., & Pişkin, S. (2013). Synthesis of barium metaborate from boric acid with microwave assisted method. Sigma Journal of Engineering and Natural Sciences, 31(1), 63-72. https://izlik.org/JA32DP32KB
AMA
1.Akşener AE, Pişkin S. Synthesis of barium metaborate from boric acid with microwave assisted method. SIGMA. 2013;31(1):63-72. https://izlik.org/JA32DP32KB
Chicago
Akşener, A. Eymen, and Sabriye Pişkin. 2013. “Synthesis of Barium Metaborate from Boric Acid With Microwave Assisted Method”. Sigma Journal of Engineering and Natural Sciences 31 (1): 63-72. https://izlik.org/JA32DP32KB.
EndNote
Akşener AE, Pişkin S (March 1, 2013) Synthesis of barium metaborate from boric acid with microwave assisted method. Sigma Journal of Engineering and Natural Sciences 31 1 63–72.
IEEE
[1]A. E. Akşener and S. Pişkin, “Synthesis of barium metaborate from boric acid with microwave assisted method”, SIGMA, vol. 31, no. 1, pp. 63–72, Mar. 2013, [Online]. Available: https://izlik.org/JA32DP32KB
ISNAD
Akşener, A. Eymen - Pişkin, Sabriye. “Synthesis of Barium Metaborate from Boric Acid With Microwave Assisted Method”. Sigma Journal of Engineering and Natural Sciences 31/1 (March 1, 2013): 63-72. https://izlik.org/JA32DP32KB.
JAMA
1.Akşener AE, Pişkin S. Synthesis of barium metaborate from boric acid with microwave assisted method. SIGMA. 2013;31:63–72.
MLA
Akşener, A. Eymen, and Sabriye Pişkin. “Synthesis of Barium Metaborate from Boric Acid With Microwave Assisted Method”. Sigma Journal of Engineering and Natural Sciences, vol. 31, no. 1, Mar. 2013, pp. 63-72, https://izlik.org/JA32DP32KB.
Vancouver
1.A. Eymen Akşener, Sabriye Pişkin. Synthesis of barium metaborate from boric acid with microwave assisted method. SIGMA [Internet]. 2013 Mar. 1;31(1):63-72. Available from: https://izlik.org/JA32DP32KB