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Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu

Year 2016, Volume: 42 Issue: 2, 136 - 143, 28.10.2016

Alper Kaya Mustafa Koyuncu

Abstract

Bu çalışmada, Baryum titanat
(BaTiO3) nanofiber ve nanotozlar elektroeğirme yöntemiyle
üretilmiştir. Nanofiberler 800 °C sıcaklıkta ısıl işleme
tabi tutularak barium titanat nanotoz elde edilmiştir. Elde edilen numunelerin mikroyapı
analizleri XRD ve SEM ile yapılmıştır. Isıl işlem öncesi SEM görüntülerine göre
ortalama 800 nm çapa sahip düzgün silindirik fiberler elde edilmiştir. Isıl işlem
sonrasındaki SEM görüntülerinde ise 50-250 nm aralığında çapa sahip düzgün ve
homojen yapıdaki küresel baryum titanat tozların elde edildiği bulunmuştur. XRD
analiz sonuçları BaTiO3 nanotozların kübik kristal yapıda olduğunu
göstermiştir.

Keywords

Baryum titanat elektroeğirme nanokompozit nanofiber

References

  • Ashiri R, Moghtada A, Shahrouzianfar A (2015). Processing and characterization of carbonate-free BaTiO3 nanoscale particles obtained by a rapid ultrasound-assisted wet chemical approach, Metall. Mater. Trans. B 46, 1912–1923.
  • Ashiri R, Moghtada A, Shahrouzianfar A, Ajami R (2014). Low temperature synthesis of carbonate-free barium titanate nanoscale crystals; toward a generalized strategy of titanate-based perovskite nanocrystals synthesis, J. Am. Ceram. Soc. 97, 2027–2031.
  • Ashiri R, Nemati A, Ghamsari MS, Sanjabi S, Aalipour M (2011). A modified method for barium titanate nanoparticles synthesis, Mater. Res. Bull. 46, 2291–2295.
  • Fang CY, Wang C, Polotai AV, Agrawal DK, Lanagan MT (2008). Microwave synthesis of nano-sized barium titanate, Mater. Lett. 62, 2551–2553.
  • George CN, Thomas JK, Kumar HP, Suresh MK, Kumar VR, Wariar PRS, Jose R, Koshy J (2009). Characterization, sintering and dilelectric properties of nanocrystalline barium titanate synthesized through a modified combustion process, Mater. Charact. 60, 322–326.
  • Guo W, Datye AK, Ward TL (2005). Synthesis of barium titanate powders by aerosol pyrolysis of a Pechini-type precursor solution, J. Mater. Chem. 15, 470–477.
  • Hotta Y, Tsunekawa K, Isobe T, Sato K, Watari K (2008) Synthesis of BaTiO3 powders by a ball milling-assisted hydrothermal reaction, Mater. Sci. Eng. A 475, 57–61.
  • Joshi NJ, Grewal GS, Shrinet V, Govindan TP, Pratap A (2012). Synthesis and dielectric behavior of nano-scale barium titanate, IEEE Trans. Dielectr. Electr. Insul. 19, 83–90.
  • Kavian R, Said A (2009). Sol-gel derived BaTiO3 nanopowders, J. Alloy Compd. 468, 528–532.
  • Kwon SG, Choi K, Kim BI (2006). Solvothermal synthesis of nano-sized tetragonal barium titanate powder, Mater. Lett. 60, 979–982.

Year 2016, Volume: 42 Issue: 2, 136 - 143, 28.10.2016

Alper Kaya Mustafa Koyuncu

Abstract

References

  • Ashiri R, Moghtada A, Shahrouzianfar A (2015). Processing and characterization of carbonate-free BaTiO3 nanoscale particles obtained by a rapid ultrasound-assisted wet chemical approach, Metall. Mater. Trans. B 46, 1912–1923.
  • Ashiri R, Moghtada A, Shahrouzianfar A, Ajami R (2014). Low temperature synthesis of carbonate-free barium titanate nanoscale crystals; toward a generalized strategy of titanate-based perovskite nanocrystals synthesis, J. Am. Ceram. Soc. 97, 2027–2031.
  • Ashiri R, Nemati A, Ghamsari MS, Sanjabi S, Aalipour M (2011). A modified method for barium titanate nanoparticles synthesis, Mater. Res. Bull. 46, 2291–2295.
  • Fang CY, Wang C, Polotai AV, Agrawal DK, Lanagan MT (2008). Microwave synthesis of nano-sized barium titanate, Mater. Lett. 62, 2551–2553.
  • George CN, Thomas JK, Kumar HP, Suresh MK, Kumar VR, Wariar PRS, Jose R, Koshy J (2009). Characterization, sintering and dilelectric properties of nanocrystalline barium titanate synthesized through a modified combustion process, Mater. Charact. 60, 322–326.
  • Guo W, Datye AK, Ward TL (2005). Synthesis of barium titanate powders by aerosol pyrolysis of a Pechini-type precursor solution, J. Mater. Chem. 15, 470–477.
  • Hotta Y, Tsunekawa K, Isobe T, Sato K, Watari K (2008) Synthesis of BaTiO3 powders by a ball milling-assisted hydrothermal reaction, Mater. Sci. Eng. A 475, 57–61.
  • Joshi NJ, Grewal GS, Shrinet V, Govindan TP, Pratap A (2012). Synthesis and dielectric behavior of nano-scale barium titanate, IEEE Trans. Dielectr. Electr. Insul. 19, 83–90.
  • Kavian R, Said A (2009). Sol-gel derived BaTiO3 nanopowders, J. Alloy Compd. 468, 528–532.
  • Kwon SG, Choi K, Kim BI (2006). Solvothermal synthesis of nano-sized tetragonal barium titanate powder, Mater. Lett. 60, 979–982.
There are 10 citations in total.

Details

Journal Section Research Articles
Authors

Alper Kaya This is me

Mustafa Koyuncu This is me

Publication Date October 28, 2016
Submission Date February 2, 2017
Published in Issue Year 2016 Volume: 42 Issue: 2

Cite

APA Kaya, A., & Koyuncu, M. (2016). Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu. Selçuk Üniversitesi Fen Fakültesi Fen Dergisi, 42(2), 136-143.
AMA Kaya A, Koyuncu M. Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu. sufefd. October 2016;42(2):136-143.
Chicago Kaya, Alper, and Mustafa Koyuncu. “Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber Ve Nanotoz Üretimi Ve Karakterizasyonu”. Selçuk Üniversitesi Fen Fakültesi Fen Dergisi 42, no. 2 (October 2016): 136-43.
EndNote Kaya A, Koyuncu M (October 1, 2016) Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu. Selçuk Üniversitesi Fen Fakültesi Fen Dergisi 42 2 136–143.
IEEE A. Kaya and M. Koyuncu, “Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu”, sufefd, vol. 42, no. 2, pp. 136–143, 2016.
ISNAD Kaya, Alper - Koyuncu, Mustafa. “Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber Ve Nanotoz Üretimi Ve Karakterizasyonu”. Selçuk Üniversitesi Fen Fakültesi Fen Dergisi 42/2 (October 2016), 136-143.
JAMA Kaya A, Koyuncu M. Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu. sufefd. 2016;42:136–143.
MLA Kaya, Alper and Mustafa Koyuncu. “Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber Ve Nanotoz Üretimi Ve Karakterizasyonu”. Selçuk Üniversitesi Fen Fakültesi Fen Dergisi, vol. 42, no. 2, 2016, pp. 136-43.
Vancouver Kaya A, Koyuncu M. Elektroeğirme Yöntemiyle Baryum Titanat (BaTiO3) Nanofiber ve Nanotoz Üretimi ve Karakterizasyonu. sufefd. 2016;42(2):136-43.

Journal Owner: On behalf of Selçuk University Faculty of Science, Rector Prof. Dr. Metin AKSOY
Selcuk University Journal of Science Faculty accepts articles in Turkish and English with original results in basic sciences and other applied sciences. The journal may also include compilations containing current innovations.

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