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Freeze-drying kinetics and diffusion modeling of hawthorn

Year 2023, , 876 - 884, 04.08.2023
https://doi.org/10.18186/thermal.1327094

Abstract

This study tests freeze-drying (FD) technology (Scanvac Coolsafe model, Labogene brand) to preserve hawthorn fruit. First, 100g hawthorn slices were frozen and then freeze-dried. Kinet-ic models were applied, and hawthorn’s moisture ratio and weight loss were noted after every two hours during the 14-hour freeze-drying process. Matlab program is used to perform a to-tal of eight kinetic drying models. Results show that the root mean square error was 0.011063, the highest determination coefficient was 0.9987, the least chi-square was 1.959x10-4, and the effective diffusivity was 2.33742x10-10m2/s. The diffusion approach is the best among the eight models.

References

  • References [1] Kowalski R, Kowalski G, Kalwa K, Sujka M. Essential oil composition of hawthorn crataegus monogyna inflorescence. Chem Nat Compd 2018;54:995997. [CrossRef] [2] Ozcan M, Haciseferogulları H, Marakoglu T, Arslan D. Hawthorn (Crataegus spp.) fruit: some physical and chemical properties. J Food Eng 2005;69:409413. [CrossRef]
  • [3] Zhang Z, Chang Q, Zhu M, Huang Y, Ho W-K-K, Chen Z-Y. Characterization of Antioxidants Present in Hawthorn Fruits. J. Nutr. Biochem 2001;12:144152. [CrossRef]
  • [4] Ammon H-P-T, Handel M. Crataegus, toxicology and pharmacology. Part II: Pharmacodynamics. Planta Med 1981;43:209239. [CrossRef]
  • [5] Zhang Z, Ho W-K-K, Huang Y, Chen Z-Y. Hypocholesterolemic activity of hawthorn fruit is mediated by regulation of cholesterol-7α-hydroxylase and acyl CoA: Cholesterol acyltransferase. Food Res Int 2002;35:885891. [CrossRef] [6] Marques L-G, Freire J-T. Analysis of freeze-drying of tropical fruits. Dry Technol 2005;23:21692184. [CrossRef]
  • [7] Kırmacı V, Usta H, Menlik T. An experimental study on freeze-drying behavior of strawberries. Dry Technol 2008;26:15701576. [CrossRef]
  • [8] Moraga G, Talens P, Moraga M-J, Martinez N-N. Implication of water activity and glass transition on the mechanical and optical properties of freeze-dried apple and banana slices. J Food Eng 2011;106;212219. [CrossRef]
  • [9] Kopjar M, Pilizota V, Hribar J, Simcic M, Zlatic E, Tiban N-N. Influence of trehalose addition and storage conditions on the quality of strawberry cream filling. J Food Eng 2011;106:212219.
  • [10] Zaichick V, Zaichick S. A search for losses of chemical elements during freeze-drying of biological materials. J Rad Nuc Chem 1997;218:249253. [CrossRef]
  • [11] Oetjen G, Haseley P. Freeze-drying. Weinheim: Wiley-VCH Press: 2004. [CrossRef]
  • [12] Kochs M, Körber C, Nunner B, Heschel I. The influence of the freezing process on vapour transport during sublimation in vacuum-freeze-drying. Int J Heat Mass Transf 1991;34:23952408. [CrossRef]
  • [13] Acar B, Sadikoglu H, Ozkaymak M. Freeze Drying of Saffron (Crocus Sativus L.). Dry. Technol 2011;29:16221627. [CrossRef]
  • [14] Liapis A-I, Pikal M-J, Bruttini R. Research and development needs and opportunities in freeze drying. Dry Technol 1996;14:12651300. [CrossRef] [15] Sadikoglu H, Ozdemir M, Seker M. Freeze-drying of pharmaceutical products: Research and development needs. Dry Technol 2006;24:849861. [CrossRef]
  • [16] Sadikoglu H, Liapis A-I. Mathematical modelling of the primary and secondary drying stages of bulk solution freeze-drying in trays: parameter estimation and model discrimination by comparison of theoretical results with experimental data. Dry Technol 1997;15:791810. [CrossRef] [17] Acar B, Sadikoglu H, Doymaz I. Freeze-drying kinetics and diffusion modeling of saffron (crocus sativus L.). J Food Process Preserv 2015:29;142149. [CrossRef]
  • [18] Ishwaya S-P, Anandharamakrishnan C. Spray-freeze-drying approach for soluble coffee processing and its effect on quality characteristics. J Food Eng 2015;149:171180. [CrossRef]
  • [19] Wang J, Li Y-Z, Chen R-R, Bao J-Y, Yang G-M. Comparison of volatiles of banana powder dehydrated by vacuum belt drying, freeze-drying and air-drying. Food Chem 2007;104:15161521. [CrossRef]
  • [20] Jiang H, Zhang M, Mujumdar A-S. Physico-chemical changes during different Stages of MFD/FD banana chips. J Food Eng 2010;101:140145. [CrossRef]
  • [21] Khampakool A, Soisungwan S, Park S-H. Potential application of infrared assisted freeze drying (IRAFD) for banana snacks: Drying kinetics, energy consumption, and texture. Food Sci Tech 2019;99:355363. [CrossRef]
  • [22] Maskan M. Drying, shrinkage and rehydration characteristics of kiwifruits during hot air and microwave drying. J Food Eng 2001;48:177182. [CrossRef] [23] Maskan M. Microwave/air and microwave finish drying of banana. J Food Eng 2000;44:7178. [CrossRef]
  • [24] Sadikoglu H, Liapis A-I, Grosser O-K. Optimal control of the primary and secondary drying stages of bulk solution freeze drying in trays. Dry Technol 1998;16:399431. [CrossRef]
  • [25] Menges H-O, Ertekin C. Mathematical modeling of thin layer drying of golden apples. J Food Eng 2006;77:119125. [CrossRef] [26] Rayaguru K, Routray W, Mohanty S-N. Mathematical modeling and quality parameters of air-dried betel leaf (piper betle L.). J Food Process Preserv 2011;35:394401. [CrossRef]
  • [27] Sadikoglu H, Ozdemir M, Seker M. Optimal control of the primary drying stage of freeze drying of solutions in vials using variational calculus. Dry Technol 2003;21:13071331. [CrossRef]
  • [28] Senadeera W, Bhandari B-R, Young G, Wijesinghe B. Influence of shapes of selected vegetable materials on drying kinetics during fluidized bed drying. J Food Eng 2003;58:277283. [CrossRef]
  • [29] Souret F-F, Weathers P-J. The growth of saffron (Crocus sativus L.) in aeroponics and hydroponics. J Herbs Spices Med Plants 2000;7:2535. [CrossRef]
  • [30] Tapaneyasin R, Devahastin S, Tansakul A. Drying methods and quality of shrimp dried in a jet-spouted bed dryer. J Food Process Eng 2005;28:3552. [CrossRef] [31] Vega-Galvez A, Miranda M, Bilbao-Sainz C, Uribe E, Lemus-Mondaca R. Freeze-drying kinetics and diffusion modeling of saffron (crocus sativus L.). J Food Process Preserv 2008;32:972986. [CrossRef] [32] Crank J. The mathematics of Diffusion. Great Britain: Oxford University Press: 1975.
  • [33] Zogzas N-P, Maroulis Z-B, Marinos-Kouris D. Moisture diffusivity data compilation in foodstuffs. Dry Technol 1996;14:22252253. [CrossRef]
Year 2023, , 876 - 884, 04.08.2023
https://doi.org/10.18186/thermal.1327094

Abstract

References

  • References [1] Kowalski R, Kowalski G, Kalwa K, Sujka M. Essential oil composition of hawthorn crataegus monogyna inflorescence. Chem Nat Compd 2018;54:995997. [CrossRef] [2] Ozcan M, Haciseferogulları H, Marakoglu T, Arslan D. Hawthorn (Crataegus spp.) fruit: some physical and chemical properties. J Food Eng 2005;69:409413. [CrossRef]
  • [3] Zhang Z, Chang Q, Zhu M, Huang Y, Ho W-K-K, Chen Z-Y. Characterization of Antioxidants Present in Hawthorn Fruits. J. Nutr. Biochem 2001;12:144152. [CrossRef]
  • [4] Ammon H-P-T, Handel M. Crataegus, toxicology and pharmacology. Part II: Pharmacodynamics. Planta Med 1981;43:209239. [CrossRef]
  • [5] Zhang Z, Ho W-K-K, Huang Y, Chen Z-Y. Hypocholesterolemic activity of hawthorn fruit is mediated by regulation of cholesterol-7α-hydroxylase and acyl CoA: Cholesterol acyltransferase. Food Res Int 2002;35:885891. [CrossRef] [6] Marques L-G, Freire J-T. Analysis of freeze-drying of tropical fruits. Dry Technol 2005;23:21692184. [CrossRef]
  • [7] Kırmacı V, Usta H, Menlik T. An experimental study on freeze-drying behavior of strawberries. Dry Technol 2008;26:15701576. [CrossRef]
  • [8] Moraga G, Talens P, Moraga M-J, Martinez N-N. Implication of water activity and glass transition on the mechanical and optical properties of freeze-dried apple and banana slices. J Food Eng 2011;106;212219. [CrossRef]
  • [9] Kopjar M, Pilizota V, Hribar J, Simcic M, Zlatic E, Tiban N-N. Influence of trehalose addition and storage conditions on the quality of strawberry cream filling. J Food Eng 2011;106:212219.
  • [10] Zaichick V, Zaichick S. A search for losses of chemical elements during freeze-drying of biological materials. J Rad Nuc Chem 1997;218:249253. [CrossRef]
  • [11] Oetjen G, Haseley P. Freeze-drying. Weinheim: Wiley-VCH Press: 2004. [CrossRef]
  • [12] Kochs M, Körber C, Nunner B, Heschel I. The influence of the freezing process on vapour transport during sublimation in vacuum-freeze-drying. Int J Heat Mass Transf 1991;34:23952408. [CrossRef]
  • [13] Acar B, Sadikoglu H, Ozkaymak M. Freeze Drying of Saffron (Crocus Sativus L.). Dry. Technol 2011;29:16221627. [CrossRef]
  • [14] Liapis A-I, Pikal M-J, Bruttini R. Research and development needs and opportunities in freeze drying. Dry Technol 1996;14:12651300. [CrossRef] [15] Sadikoglu H, Ozdemir M, Seker M. Freeze-drying of pharmaceutical products: Research and development needs. Dry Technol 2006;24:849861. [CrossRef]
  • [16] Sadikoglu H, Liapis A-I. Mathematical modelling of the primary and secondary drying stages of bulk solution freeze-drying in trays: parameter estimation and model discrimination by comparison of theoretical results with experimental data. Dry Technol 1997;15:791810. [CrossRef] [17] Acar B, Sadikoglu H, Doymaz I. Freeze-drying kinetics and diffusion modeling of saffron (crocus sativus L.). J Food Process Preserv 2015:29;142149. [CrossRef]
  • [18] Ishwaya S-P, Anandharamakrishnan C. Spray-freeze-drying approach for soluble coffee processing and its effect on quality characteristics. J Food Eng 2015;149:171180. [CrossRef]
  • [19] Wang J, Li Y-Z, Chen R-R, Bao J-Y, Yang G-M. Comparison of volatiles of banana powder dehydrated by vacuum belt drying, freeze-drying and air-drying. Food Chem 2007;104:15161521. [CrossRef]
  • [20] Jiang H, Zhang M, Mujumdar A-S. Physico-chemical changes during different Stages of MFD/FD banana chips. J Food Eng 2010;101:140145. [CrossRef]
  • [21] Khampakool A, Soisungwan S, Park S-H. Potential application of infrared assisted freeze drying (IRAFD) for banana snacks: Drying kinetics, energy consumption, and texture. Food Sci Tech 2019;99:355363. [CrossRef]
  • [22] Maskan M. Drying, shrinkage and rehydration characteristics of kiwifruits during hot air and microwave drying. J Food Eng 2001;48:177182. [CrossRef] [23] Maskan M. Microwave/air and microwave finish drying of banana. J Food Eng 2000;44:7178. [CrossRef]
  • [24] Sadikoglu H, Liapis A-I, Grosser O-K. Optimal control of the primary and secondary drying stages of bulk solution freeze drying in trays. Dry Technol 1998;16:399431. [CrossRef]
  • [25] Menges H-O, Ertekin C. Mathematical modeling of thin layer drying of golden apples. J Food Eng 2006;77:119125. [CrossRef] [26] Rayaguru K, Routray W, Mohanty S-N. Mathematical modeling and quality parameters of air-dried betel leaf (piper betle L.). J Food Process Preserv 2011;35:394401. [CrossRef]
  • [27] Sadikoglu H, Ozdemir M, Seker M. Optimal control of the primary drying stage of freeze drying of solutions in vials using variational calculus. Dry Technol 2003;21:13071331. [CrossRef]
  • [28] Senadeera W, Bhandari B-R, Young G, Wijesinghe B. Influence of shapes of selected vegetable materials on drying kinetics during fluidized bed drying. J Food Eng 2003;58:277283. [CrossRef]
  • [29] Souret F-F, Weathers P-J. The growth of saffron (Crocus sativus L.) in aeroponics and hydroponics. J Herbs Spices Med Plants 2000;7:2535. [CrossRef]
  • [30] Tapaneyasin R, Devahastin S, Tansakul A. Drying methods and quality of shrimp dried in a jet-spouted bed dryer. J Food Process Eng 2005;28:3552. [CrossRef] [31] Vega-Galvez A, Miranda M, Bilbao-Sainz C, Uribe E, Lemus-Mondaca R. Freeze-drying kinetics and diffusion modeling of saffron (crocus sativus L.). J Food Process Preserv 2008;32:972986. [CrossRef] [32] Crank J. The mathematics of Diffusion. Great Britain: Oxford University Press: 1975.
  • [33] Zogzas N-P, Maroulis Z-B, Marinos-Kouris D. Moisture diffusivity data compilation in foodstuffs. Dry Technol 1996;14:22252253. [CrossRef]
There are 25 citations in total.

Details

Primary Language English
Subjects Thermodynamics and Statistical Physics
Journal Section Articles
Authors

Khaled Ali Hagıg This is me 0000-0001-5359-5608

Bahadır Acar This is me 0000-0001-8540-7368

Edip Taşkesen This is me 0000-0002-3052-9883

Edip Taşkesen This is me 0000-0002-3052-9883

Edip Taşkesen This is me 0000-0002-3052-9883

Mehmet Özkaymak This is me 0000-0002-4575-8988

Publication Date August 4, 2023
Submission Date December 8, 2021
Published in Issue Year 2023

Cite

APA Hagıg, K. A., Acar, B., Taşkesen, E., Taşkesen, E., et al. (2023). Freeze-drying kinetics and diffusion modeling of hawthorn. Journal of Thermal Engineering, 9(4), 876-884. https://doi.org/10.18186/thermal.1327094
AMA Hagıg KA, Acar B, Taşkesen E, Taşkesen E, Taşkesen E, Özkaymak M. Freeze-drying kinetics and diffusion modeling of hawthorn. Journal of Thermal Engineering. August 2023;9(4):876-884. doi:10.18186/thermal.1327094
Chicago Hagıg, Khaled Ali, Bahadır Acar, Edip Taşkesen, Edip Taşkesen, Edip Taşkesen, and Mehmet Özkaymak. “Freeze-Drying Kinetics and Diffusion Modeling of Hawthorn”. Journal of Thermal Engineering 9, no. 4 (August 2023): 876-84. https://doi.org/10.18186/thermal.1327094.
EndNote Hagıg KA, Acar B, Taşkesen E, Taşkesen E, Taşkesen E, Özkaymak M (August 1, 2023) Freeze-drying kinetics and diffusion modeling of hawthorn. Journal of Thermal Engineering 9 4 876–884.
IEEE K. A. Hagıg, B. Acar, E. Taşkesen, E. Taşkesen, E. Taşkesen, and M. Özkaymak, “Freeze-drying kinetics and diffusion modeling of hawthorn”, Journal of Thermal Engineering, vol. 9, no. 4, pp. 876–884, 2023, doi: 10.18186/thermal.1327094.
ISNAD Hagıg, Khaled Ali et al. “Freeze-Drying Kinetics and Diffusion Modeling of Hawthorn”. Journal of Thermal Engineering 9/4 (August 2023), 876-884. https://doi.org/10.18186/thermal.1327094.
JAMA Hagıg KA, Acar B, Taşkesen E, Taşkesen E, Taşkesen E, Özkaymak M. Freeze-drying kinetics and diffusion modeling of hawthorn. Journal of Thermal Engineering. 2023;9:876–884.
MLA Hagıg, Khaled Ali et al. “Freeze-Drying Kinetics and Diffusion Modeling of Hawthorn”. Journal of Thermal Engineering, vol. 9, no. 4, 2023, pp. 876-84, doi:10.18186/thermal.1327094.
Vancouver Hagıg KA, Acar B, Taşkesen E, Taşkesen E, Taşkesen E, Özkaymak M. Freeze-drying kinetics and diffusion modeling of hawthorn. Journal of Thermal Engineering. 2023;9(4):876-84.

IMPORTANT NOTE: JOURNAL SUBMISSION LINK http://eds.yildiz.edu.tr/journal-of-thermal-engineering