4-(5-metil-2- (2-fenilpropan-2-il) siklohekziloksi) ftalonitrilden Hazırlanan Ftalosiyaninlerin Sentezi ve Karakterizasyonu
Abstract
A new the phthalonitrile derivative was synthesized from reaction of 4- nitrophthalonitrile with 5-methyl-2-(2-phenylpropan-2-yl) cyclohexanol. Phthalocyanines prepared from cyclotetramerization of this phthalonitrile in present metal salts. The products were purified by several techniques such as crystallization and washed with different solvents. These compounds were characterized by elemental analysis, IR, 1H-and 13C -NMR, UV-vis, MALDI-TOF mass spectral data . Key words: Phthalonitrile derivative; Solubility; Magnesium; Metallophthalocyanine; Zinc.
Keywords
Characterizationand Synthesis of Phthalocyanines Preparedfrom 4-(5-methyl-2-(2-phenylpropan-2-yl) cyclohexyloxy) phthalonitrile
Abstract
5-metil-2-(2-fenilpropan-2-il)siklohekzanol ile 4-nitroftalonitrilin reaksiyonundan yeni bir ftalonitril türevi sentezlendi. Ftalosiyaninler metal tuzlarının varlığında bu ftalonitril türevinin siklotetramerizasyonundan hazırlandı. Ürünler kristallendirme ve farklı çözücülerle yıkama gibi birkaç teknikle saflaştırıldı. Bu bileşikler IR, 1H - NMR, 13C - NMR, UV-vis, MALD I- TOF kütle spektrumu ve elemental analiz ile karakterize edildi.
Details
| Primary Language | Turkish |
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| Journal Section | Articles |
| Authors | |
| Publication Date | June 1, 2011 |
| Submission Date | August 12, 2015 |
| Published in Issue | Year 2011 Volume: 16 Issue: 1 |