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4-(5-metil-2- (2-fenilpropan-2-il) siklohekziloksi) ftalonitrilden Hazırlanan Ftalosiyaninlerin Sentezi ve Karakterizasyonu

Year 2011, Volume: 16 Issue: 1, 12 - 16, 01.06.2011

Abstract

  A  new  the  phthalonitrile  derivative  was  synthesized  from  reaction  of  4- nitrophthalonitrile with 5-methyl-2-(2-phenylpropan-2-yl) cyclohexanol. Phthalocyanines prepared from cyclotetramerization of this phthalonitrile in present metal salts. The products were purified by several techniques such as crystallization and washed with different solvents. These compounds were  characterized by elemental  analysis,  IR, 1H-and  13C  -NMR,  UV-vis,  MALDI-TOF  mass spectral data . Key words: Phthalonitrile derivative; Solubility; Magnesium; Metallophthalocyanine; Zinc.

Characterizationand Synthesis of Phthalocyanines Preparedfrom 4-(5-methyl-2-(2-phenylpropan-2-yl) cyclohexyloxy) phthalonitrile

Year 2011, Volume: 16 Issue: 1, 12 - 16, 01.06.2011

Abstract

5-metil-2-(2-fenilpropan-2-il)siklohekzanol ile 4-nitroftalonitrilin reaksiyonundan yeni bir ftalonitril türevi sentezlendi. Ftalosiyaninler  metal tuzlarının varlığında bu ftalonitril  türevinin siklotetramerizasyonundan  hazırlandı.  Ürünler  kristallendirme ve farklı çözücülerle yıkama gibi birkaç teknikle  saflaştırıldı. Bu bileşikler  IR, 1H - NMR, 13C  - NMR, UV-vis,  MALD I- TOF kütle spektrumu ve elemental analiz ile karakterize edildi.

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Details

Primary Language Turkish
Journal Section Articles
Authors

M. Salih Ağırtaş This is me

Bedrettin Savaş This is me

Publication Date June 1, 2011
Submission Date August 12, 2015
Published in Issue Year 2011 Volume: 16 Issue: 1

Cite

APA Ağırtaş, M. S., & Savaş, B. (2011). Characterizationand Synthesis of Phthalocyanines Preparedfrom 4-(5-methyl-2-(2-phenylpropan-2-yl) cyclohexyloxy) phthalonitrile. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 16(1), 12-16.