Research Article

Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+

Volume: 13 Number: 4 October 30, 2025
TR EN

Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+

Abstract

This preliminary study investigates the effect of freezing duration on the impact and strength performance of 3D-printed PLA+ specimens produced with 50% and 100% infill densities in a honeycomb pattern using the FDM technique. Samples were stored at -80 °C for varying time intervals (up to 72 hours), and their dimensional changes, hardness, and impact resistance were evaluated. Results indicate that prolonged exposure to sub-zero temperatures caused a slight reduction in specimen diameter, likely due to material shrinkage. Conversely, hardness values increased with freezing time, reaching a maximum Shore D value of 85.78 for fully solid samples. Impact testing revealed that 100% infill density specimens absorbed more energy than 50% counterparts, with the highest impact strength (24.53 kJ/m²) observed after 72 hours of freezing. Visual analysis showed no significant variation in crack trajectory with freezing duration. Overall, the findings suggest that PLA+ retains and even improves its mechanical robustness under cryogenic conditions, making it a promising candidate for applications requiring durability in extreme environments.

Keywords

Ethical Statement

This study does not involve human or animal participants. All procedures followed scientific and ethical principles, and all referenced studies are appropriately cited.

References

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Details

Primary Language

English

Subjects

Mechanical Engineering (Other)

Journal Section

Research Article

Publication Date

October 30, 2025

Submission Date

August 3, 2025

Acceptance Date

September 30, 2025

Published in Issue

Year 2025 Volume: 13 Number: 4

APA
Aslan, E. (2025). Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+. Duzce University Journal of Science and Technology, 13(4), 1799-1811. https://doi.org/10.29130/dubited.1757310
AMA
1.Aslan E. Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+. DUBİTED. 2025;13(4):1799-1811. doi:10.29130/dubited.1757310
Chicago
Aslan, Enes. 2025. “Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+”. Duzce University Journal of Science and Technology 13 (4): 1799-1811. https://doi.org/10.29130/dubited.1757310.
EndNote
Aslan E (October 1, 2025) Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+. Duzce University Journal of Science and Technology 13 4 1799–1811.
IEEE
[1]E. Aslan, “Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+”, DUBİTED, vol. 13, no. 4, pp. 1799–1811, Oct. 2025, doi: 10.29130/dubited.1757310.
ISNAD
Aslan, Enes. “Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+”. Duzce University Journal of Science and Technology 13/4 (October 1, 2025): 1799-1811. https://doi.org/10.29130/dubited.1757310.
JAMA
1.Aslan E. Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+. DUBİTED. 2025;13:1799–1811.
MLA
Aslan, Enes. “Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+”. Duzce University Journal of Science and Technology, vol. 13, no. 4, Oct. 2025, pp. 1799-11, doi:10.29130/dubited.1757310.
Vancouver
1.Enes Aslan. Influence of Freezing Time on Hardness and Impact Resistance of 3D-Printed PLA+. DUBİTED. 2025 Oct. 1;13(4):1799-811. doi:10.29130/dubited.1757310