Electrophoretic Deposition of MnO2 using Folic Acid as Advanced Dispersing Agent

Yıl 2020, Cilt: 1 Sayı: 1, 21 - 29, 02.07.2020

Mustafa Sami Ata

Öz

Abstract
The deposition mechanism of MnO2 has been investigated by using electrophoretic deposition (EPD) method. Folic acid, a biocompatible dispersing agent, was analyzed for the dispersion of MnO2 and MWCNT and anodic deposition of MnO2 in ethanol. Fourier transform infrared spectroscopy and scanning electron microscopy were used for morphology analysis. The amount of the deposited material can be controlled by the variation of dispersing agent concentration in the solution based on the deposition yield measurements and deposition time. The deposition mechanism is discussed. The films prepared by EPD method are promising materials for application in electrochemical supercapacitors.

Özet
MnO2'nin biriktirme mekanizması elektroforetik biriktirme (EPD) yöntemi kullanılarak araştırılmıştır. Biyouyumlu bir dispersiyon ajanı olan folik asit, MnO2 ve MWCNT'nin dispersiyonu ve MnO2'nin etanol içinde anodik birikimi için analiz edildi. Morfoloji analizleri için Fourier dönüşümü kızılötesi spektroskopisi ve tarayıcı elektron mikroskopundan yararlanıldı. Biriken malzemenin miktarı, biriktirme verimi ölçümlerine ve biriktirme süresine bağlı olarak çözelti içindeki dispersiyon maddesi konsantrasyonunun değişimi ile kontrol edilebilir. Biriktirme mekanizması tartışılmıştır. EPD yöntemiyle hazırlanan filmler elektrokimyasal süper kapasitörler de uygulama için ümit vaat eden malzemelerdir.

Anahtar Kelimeler

EPD, Colloidal, Advanced Dispersing Agents

Teşekkür

I would like to thank Dr. Igor Zhitomirksy for his generous help and contribution during the project.

Kaynakça

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