Öz
The mix potassium antimonytitrate with chloride of copper (I) is dissolved in ethyleneglycol and to it increases as seleniruyushchy reagent selenidesulphate sodium. The experimental ware in a teflon ditch is located in the microwave electric oven. Test within 10 hours at 1800С to temperature remains in the furnace. The received deposit is filtered via the glass filter, washed out by the diluted solution of hydrochloric acid, ultrapure water, at last, ethyl alcohol, is dried up at 60-70 0C in vacuum. The exit makes 92-94%. Chemical, thermographic and morphological analyses СuSbSe2 are executed, and is established that crystals of connection are presented in the form of nanocores.
Anahtar Kelimeler
Antimony copper selenide solvotermal method chemical analysis thermographic analysis nanorod
Kaynakça
- Ding Tang, Jia Yang, Fangyang Liu//One-Step Electrodeposition and Annealing of CuSbSe2 Thin Films. Electrochemical and Solid-State Letters (ESL), 2011, China.
- Tan D, Jan of J, Liu FY//Growth and the characteristic of CuSbSe2 of the thin films received by a method of electrolytic sedimentation. Electrochimica.
- Chongyin Yang, Yaoming Wang, Shaotang Li//CuSbSe2-assisted sintering of CuInSe2 at low temperature. Journal of Materials Science, 2012, Volume 47, Issue 20, pp 7085-7089.
Öz
Kaliumantimoniltartrat ile bakır (I) klorür karısımı etilen glikol çözülerek üzerine
selenidləsdirici reaktif olarak sodyum selenesulfat çözeltisi ilave edilir. Deney kabı teflon küvetdə Speedwave four mikrodalga elektrik qızdırıcısında 1800C de 10 saat süreyle saklanır. Alınan çöküntü süzülür, zayıf hidroklorik asit solüsyonu, ultra saf su ve alkolle yıkandıktan sonra 60 -700C de vakumda kurutulur. Çıxım 92 - 94% teskil etmistir. Alınan CuSbSe2-in kimyasal, termoqrafik, morfolojik analizleri yapıldı ve kristaller nanoçubuqdan ibaret olduğu belirlenmistir.
Anahtar Kelimeler
Kaynakça
- Ding Tang, Jia Yang, Fangyang Liu//One-Step Electrodeposition and Annealing of CuSbSe2 Thin Films. Electrochemical and Solid-State Letters (ESL), 2011, China.
- Tan D, Jan of J, Liu FY//Growth and the characteristic of CuSbSe2 of the thin films received by a method of electrolytic sedimentation. Electrochimica.
- Chongyin Yang, Yaoming Wang, Shaotang Li//CuSbSe2-assisted sintering of CuInSe2 at low temperature. Journal of Materials Science, 2012, Volume 47, Issue 20, pp 7085-7089.
Ayrıntılar
| Birincil Dil | İngilizce |
|---|---|
| Bölüm | TOPLANTI BILDIRILERI |
| Yazarlar | |
| Yayımlanma Tarihi | 30 Ocak 2015 |
| Gönderilme Tarihi | 27 Ocak 2015 |
| Yayımlandığı Sayı | Yıl 2015 Cilt: 2 Sayı: 2 |
