Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor

Oğuz Karaahmet

doi:10.16984/saufenbilder.1760764

Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor

Abstract

Zirconium diboride (ZrB2) was synthesized via a carbothermic method using a ZrO2 powder mixture, which was obtained a reactant by mixing B2O3 and a carbon source derived from a polymer precursor as well as by combining glassy B2O3 with activated carbon. The polymer precursor was calcined to obtain the reactant powder. ZrB2 particles were synthesized with two different temperatures (1400 °C and 1500 °C). At 1500 °C, the product mainly consisted of short, cubic and prismatic grains exhibiting agglomerated morphologies, wheras at 1400 °C, longer rod-like grains and agglomerated prismatic structures were observed. The final products contained impurities such as ZrO₂ and ZrC. ZrB2 with rod-like morphology was synthesized at different temperatures using the reactant. It was observed that the particle size decreased with increasing synthesis temperature. A higher synthesis temperature also reduced the amount of residual ZrO2 and increased ZrC formation, likely due to boron source deficiency at high temperatures.

Keywords

References

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Details

Primary Language

English

Subjects

Materials Engineering (Other)

Journal Section

Research Article

Authors

Oğuz Karaahmet ^*
0000-0001-9120-2932
Türkiye

Early Pub Date

April 21, 2026

Publication Date

April 30, 2026

Submission Date

August 11, 2025

Acceptance Date

March 10, 2026

Published in Issue

Year 2026 Volume: 30 Number: 2

DOI

https://doi.org/10.16984/saufenbilder.1760764

IZ

https://izlik.org/JA79ED38XL

Cite

RIS / Bibtex

APA

Karaahmet, O. (2026). Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor. Sakarya University Journal of Science, 30(2), 158-165. https://doi.org/10.16984/saufenbilder.1760764

AMA

1.Karaahmet O. Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor. SAUJS. 2026;30(2):158-165. doi:10.16984/saufenbilder.1760764

Chicago

Karaahmet, Oğuz. 2026. “Synthesis of ZrB2 by Carbothermic Method With Reactant Material Obtained from Polymer Precursor”. Sakarya University Journal of Science 30 (2): 158-65. https://doi.org/10.16984/saufenbilder.1760764.

EndNote

Karaahmet O (April 1, 2026) Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor. Sakarya University Journal of Science 30 2 158–165.

IEEE

[1]O. Karaahmet, “Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor”, SAUJS, vol. 30, no. 2, pp. 158–165, Apr. 2026, doi: 10.16984/saufenbilder.1760764.

ISNAD

Karaahmet, Oğuz. “Synthesis of ZrB2 by Carbothermic Method With Reactant Material Obtained from Polymer Precursor”. Sakarya University Journal of Science 30/2 (April 1, 2026): 158-165. https://doi.org/10.16984/saufenbilder.1760764.

JAMA

1.Karaahmet O. Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor. SAUJS. 2026;30:158–165.

MLA

Karaahmet, Oğuz. “Synthesis of ZrB2 by Carbothermic Method With Reactant Material Obtained from Polymer Precursor”. Sakarya University Journal of Science, vol. 30, no. 2, Apr. 2026, pp. 158-65, doi:10.16984/saufenbilder.1760764.

Vancouver

1.Oğuz Karaahmet. Synthesis of ZrB2 by Carbothermic Method with Reactant Material Obtained from Polymer Precursor. SAUJS. 2026 Apr. 1;30(2):158-65. doi:10.16984/saufenbilder.1760764