Spectrophotometric Determination of Losartan Potassium and Hydrochlorothiazide in tablets by Wavelet Transform Approach

Yıl 2021, Cilt: 25 Sayı: 6, 1432 - 1437, 31.12.2021

Özgür Üstündağ , Erdal Dinç

https://doi.org/10.16984/saufenbilder.989654

Cited By: 3

Öz

A precise, rapid and simple spectrophotometric method development with continuous wavelet transform technique was described in this paper for the simultaneous determination of losartan potassium and hydrochlorothiazide in tablets. The continuous wavelet transform approach based on the application of Symlets5-CWT. If the original UV spectra of losartan potassium and hydrochlorothiazide are examined, it is seen that the spectra of these two substances strongly overlap. With the developed Symlets5-CWT method, the analysis was carried out successfully without any pre-separation process. The calibration equations were obtained at 247.7 nm for the losartan potassium determination and at 259.1 nm for the hydrochlorothiazide determination, respectively. The developed methods were tested in terms of validity and applicability.

Anahtar Kelimeler

Spectrophotometry, Continuous wavelet transform, Losartan potassium, Hydrochlorothiazide, Quantitative determination

Kaynakça

• [1] M. Siddiqui, Z. AlOthman, N. Rahman, “Analytical techniques in pharmaceutical analysis: A review,” Arabian Journal of Chemistry, vol. 10, pp. 1409-1421, 2017.
• [2] R. Valagaleti, P. Burns, M. Gill, “Analytical support for drug manufacturing in the United States—from active pharmaceutical ingredient synthesis to drug product shelf life,” J. Drug. Inform., vol. 37, pp. 407-438, 2003.
• [3] H. Ju, “Grand challenges in analytical chemistry: towards more bright eyes for scientific research, social events and human health,” Front. Chem., 2013, https://doi.org/10.3389/fchem.2013.00005.
• [4] Y. Chhonker, C. Edi, D. Murry, “LC–MS/MS method for simultaneous determination of diethylcarbamazine, albendazole and albendazole metabolites in human plasma: Application to a clinical pharmacokinetic study,” J. Pharm. Biomed. Anal., vol. 20, no. 151, pp. 84–90, 2018.
• [5] J. Sáiz, C. García-Ruiz, B. Gómara, “Comparison of different GC-MS configurations for the determination of prevalent drugs and related metabolites,” Analytical Methods, vol. 9, pp. 2897-2908, 2017.
• [6] H. Maurer, “Toxicological analysis of drugs: GC-MS screening and confirmation,” Acta Medicinæ Legalis, vol. XLIV, pp. 489-492, 1994.
• [7] F. Rocha, L. Teixeira, “Strategies to increase sensitivity in UV-VIS spectrophotometry,” Quimica Nova, vol. 27, no. 5, pp. 807-812, 2004.
• [8] T. Thiem, “Comparison of optical-emission mass-spectroscopy utilizing laser vaporization of solid samples for inorganic analysis,” American Laboratory, vol. 26, no. 3, pp. 48-52, 1994.
• [9] Z. Deyl, J. Janak, V. Schwarz V. “Bibliography section - Liquid column chromatography - Gas chromatography - Planar chromatography - Gel chromatography - Capillary electrophoresis and electrokinetic chromatography,” Journal of Chromatography A, vol. 940, no. 2, pp. 119-219, 2001.
• [10] A. Otieno, S. Mwongela S, “Capillary electrophoresis-based methods for the determination of lipids - A review,” Analytica Chimica Acta, vol. 624, no. 2, pp. 163-174, 2008.
• [11] A. Naggar, A. Kotb, A. Abdelwahab, “Graphite studded with facile-synthesized cu2o nanoparticle-based cubes as a novel electrochemical sensor for highly sensitive voltametric determination of mebeverine hydrochloride,” Chemosensors, 2021, https://doi.org/10.3390/chemosensors9020035.
• [12] I. Daubechies, “Ten Lectures on Wavelets, Society for Industrial and Applied Mathematics,” Philadelphia, pp. 1-357, 1992.
• [13] E. Dinç, D. Baleanu, “Continuous wavelet transform applied to the overlapping absorption signals and their ratio signals for the quantitative resolution of mixture of oxfendazole and oxyclozanide in bolus,” J. Food. Drug. Anal., vol. 15, no. 2, pp. 109-117, 2007.
• [14] Ö. Üstündağ, E. Dinç, “Continuous wavelet transforms and ultra performance liquid chromatography applied to the simultaneous quantitative determination of candesartan cilexetil and hydrochlorothiazide in tablets,” Monatshefte für Chemie, 2021, https://doi.org/10.1007/s00706-021-02822-7.
• [15] M. Toral, O. Saldias, C. Soto, “Strategies used to develop analytical methods for simultaneous determination of organic compounds by derivative spectrophotometry,” Quimica Nova, vol. 32, no. 1, pp. 257-282, 2009.
• [16] D. Nagavalli, V. Vaidhyalingam, O. Divya, “Simultaneous spectrophotometric determination of losartan potassium, amlodipine besilate and hydrochlorothiazide in pharmaceuticals by chemometric methods,” Acta Pharmaceutica, vol. 60, no. 2, pp. 141-152, 2010.
• [17] C. Vetuschi, A. Giannandrea, “Anti-beer evaluation of Hydrochlorothiazide and Losartan by UV derivative spectrophotometry,” Analytical Letters, vol. 36, no. 5, pp. 1051-1064, 2003.
• [18] T. Binh, L. Tram, N. Trang, “Simultaneous Determination of Hydrochlorothiazide and Losartan Potassium in Pharmaceutical Product by UV-Vis Spectrophotometric Method with Kalman Filter Algorithm,” Journal of Analytical Methods in Chemistry, 2021, https://doi.org/10.1155/2021/2754133.
• [19] A. Youssef, “Spectrofluorimetric Assessment of Hydrochlorothiazide Using Optical Sensor Nano-Composite Terbium Ion Doped in Sol-Gel Matrix,” Journal of Fluorescence, vol. 22, no. 3, pp. 827-834, 2012.
• [20] K. Marghany, R. Abdelsalam, G. Haddad, “HPLC method transfer study for simultaneous determination of seven angiotensin II receptor blockers,” Journal of Separation Science, vol. 43, no. 8, pp. 1398-1405, 2020.
• [21] S. Rahaman, K. Micheal, “A new RP-HPLC method for the simultaneous estimation of hydrochlorothiazide and losartan potassium in bulk and pharmaceutical dosage forms,” International Journal of Life Science and Pharma Research, vol. 10, pp. 648-653, 2020.
• [22] N. Mohammed, H. Abdo, H. Hassan, “Method development and validation of simultaneous determination of hydrochlorothiazide and losartan in tablet dosage form by RP-HPLC,” International Journal of Pharmaceutical Sciences and Research, vol. 10, no. 1, pp. 227-231, 2019.
• [23] C. Vishnuvardhan, P. Radhakrishnanand, N. Satheeshkumar, “RP-HPLC Method for the Simultaneous Estimation of Eight Cardiovascular Drugs,” Chromatographia, vol. 77, no. 3-4, pp. 265-275, 2014.
• [24] R. Maggio, P. Castellano, T. Kaufman, “A multivariate approach for the simultaneous determination of losartan potassium and hydrochlorothiazide in a combined pharmaceutical tablet formulation,” Analytical and Bioanalytical Chemistry, vol. 391, no. 8, pp. 2949-2955, 2008.