Year 2018, Volume 6, Issue 3, Pages 92 - 96 2018-09-30

The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride
The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Fatma Tuğçe ŞENBERBER [1]

60 288

In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H3BO3 asthe starting materials. The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated. X-ray diffraction (XRD) showed the synthesized sample was santite, which has the chemical formula KB5O84H2O (Powder diffraction file number: 01-1072-1688). The XRD scores increased upon decreasing the reaction temperature and time. The characteristic band values observed for boron and oxygen were investigated using Fourier transform infrared (FT-IR) and Raman spectroscopy. The morphology of the synthesized samples was characterized using scanning electron microscopy (SEM). The samples were found to be on the micro-scale with particle sizes <2.54 µm. The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H3BOasthe starting materials. The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated. X-ray diffraction (XRD) showed the synthesized sample was santite, which has the chemical formula KB5O84H2O (Powder diffraction file number: 01-1072-1688). The XRD scores increased upon decreasing the reaction temperature and time. The characteristic band values observed for boron and oxygen were investigated using Fourier transform infrared (FT-IR) and Raman spectroscopy. The morphology of the synthesized samples was characterized using scanning electron microscopy (SEM). The samples were found to be on the micro-scale with particle sizes <2.54 µm. The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

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Primary Language en
Subjects Engineering
Published Date Eylül
Journal Section Articles
Authors

Orcid: 0000-0002-3257-1524
Author: Fatma Tuğçe ŞENBERBER (Primary Author)
Institution: Atasehir Adiguzel Vocational School, Istanbul, Turkey
Country: Turkey


Dates

Publication Date: September 30, 2018

Bibtex @research article { apjes382382, journal = {Akademik Platform Mühendislik ve Fen Bilimleri Dergisi}, issn = {}, eissn = {2147-4575}, address = {Akademik Platform}, year = {2018}, volume = {6}, pages = {92 - 96}, doi = {10.21541/apjes.382382}, title = {The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride}, key = {cite}, author = {ŞENBERBER, Fatma Tuğçe} }
APA ŞENBERBER, F . (2018). The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride. Akademik Platform Mühendislik ve Fen Bilimleri Dergisi, 6 (3), 92-96. DOI: 10.21541/apjes.382382
MLA ŞENBERBER, F . "The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride". Akademik Platform Mühendislik ve Fen Bilimleri Dergisi 6 (2018): 92-96 <http://dergipark.org.tr/apjes/issue/38780/382382>
Chicago ŞENBERBER, F . "The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride". Akademik Platform Mühendislik ve Fen Bilimleri Dergisi 6 (2018): 92-96
RIS TY - JOUR T1 - The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride AU - Fatma Tuğçe ŞENBERBER Y1 - 2018 PY - 2018 N1 - doi: 10.21541/apjes.382382 DO - 10.21541/apjes.382382 T2 - Akademik Platform Mühendislik ve Fen Bilimleri Dergisi JF - Journal JO - JOR SP - 92 EP - 96 VL - 6 IS - 3 SN - -2147-4575 M3 - doi: 10.21541/apjes.382382 UR - https://doi.org/10.21541/apjes.382382 Y2 - 2018 ER -
EndNote %0 Academic Platform Journal of Engineering and Science The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride %A Fatma Tuğçe ŞENBERBER %T The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride %D 2018 %J Akademik Platform Mühendislik ve Fen Bilimleri Dergisi %P -2147-4575 %V 6 %N 3 %R doi: 10.21541/apjes.382382 %U 10.21541/apjes.382382
ISNAD ŞENBERBER, Fatma Tuğçe . "The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride". Akademik Platform Mühendislik ve Fen Bilimleri Dergisi 6 / 3 (September 2018): 92-96. https://doi.org/10.21541/apjes.382382
AMA ŞENBERBER F . The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride. APJES. 2018; 6(3): 92-96.
Vancouver ŞENBERBER F . The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride. Akademik Platform Mühendislik ve Fen Bilimleri Dergisi. 2018; 6(3): 96-92.