Year 2018, Volume 14, Issue 3, Pages 327 - 331 2018-09-30

Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography

Hale Seçilmiş Canbay [1]

61 204

A sensitive method for the determination of phenothrin, promecarb and penconazole residues in tobacco has been developed. Several solvents such as, hexane, ethyl acetate and dichloromethane were tested in order to minimize agricultural products residue. In the study, the best recovery was achieved with dichloromethane. Pesticides residues are extracted from the samples with dichloromethane. Additional clean-up steps are not required for tobacco matrices. Determination and quantification of phenothrin, promecarb and penconazole are performed by gas chromatography-flame ionization detector (GC/FID) and gas chromatography-nitrogen/phosphorus (GC/NPD). The method has been validated for tobacco matrices.  Under the optimum conditions, phenothrin R2 value 0.999,   promecarb R2 value 0.999, and penconazole R2 value 0.999. Limits of determination were 0.008 µg mL-1 for phenothrin, 0.011 µg mL-1 for penconazole and 0.007 µg mL-1 for promecarb. The standard deviations (SDs) levels were in the range 0.01-0.20. Recoveries of phenothrin, promecarb and penconazole from tobacco were found to be higher than 85%. Under this developed method, the concentrations of phenothrin, promecarb and penconazole in the 10 tobacco samples were below the LOD values.
Tobacco, GC, phenothrin, promecarb, penconazole, liquid extraction
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Primary Language en
Subjects Engineering
Journal Section Articles
Authors

Orcid: 0000-0002-3783-8064
Author: Hale Seçilmiş Canbay (Primary Author)
Institution: Burdur Mehmet Akif Ersoy Üniversitesi
Country: Turkey


Dates

Publication Date: September 30, 2018

Bibtex @research article { cbayarfbe446820, journal = {Celal Bayar University Journal of Science}, issn = {1305-130X}, eissn = {1305-1385}, address = {Celal Bayar University}, year = {2018}, volume = {14}, pages = {327 - 331}, doi = {10.18466/cbayarfbe.446820}, title = {Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography}, key = {cite}, author = {Seçilmiş Canbay, Hale} }
APA Seçilmiş Canbay, H . (2018). Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography. Celal Bayar University Journal of Science, 14 (3), 327-331. DOI: 10.18466/cbayarfbe.446820
MLA Seçilmiş Canbay, H . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar University Journal of Science 14 (2018): 327-331 <http://dergipark.org.tr/cbayarfbe/issue/39486/446820>
Chicago Seçilmiş Canbay, H . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar University Journal of Science 14 (2018): 327-331
RIS TY - JOUR T1 - Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography AU - Hale Seçilmiş Canbay Y1 - 2018 PY - 2018 N1 - doi: 10.18466/cbayarfbe.446820 DO - 10.18466/cbayarfbe.446820 T2 - Celal Bayar University Journal of Science JF - Journal JO - JOR SP - 327 EP - 331 VL - 14 IS - 3 SN - 1305-130X-1305-1385 M3 - doi: 10.18466/cbayarfbe.446820 UR - https://doi.org/10.18466/cbayarfbe.446820 Y2 - 2018 ER -
EndNote %0 Celal Bayar University Journal of Science Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography %A Hale Seçilmiş Canbay %T Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography %D 2018 %J Celal Bayar University Journal of Science %P 1305-130X-1305-1385 %V 14 %N 3 %R doi: 10.18466/cbayarfbe.446820 %U 10.18466/cbayarfbe.446820
ISNAD Seçilmiş Canbay, Hale . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar University Journal of Science 14 / 3 (September 2018): 327-331. https://doi.org/10.18466/cbayarfbe.446820
AMA Seçilmiş Canbay H . Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography. Celal Bayar Univ J Sci. 2018; 14(3): 327-331.
Vancouver Seçilmiş Canbay H . Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography. Celal Bayar University Journal of Science. 2018; 14(3): 331-327.