Filtration and Optimization for the Recovery of Powder Soap Used in Wire Drawing Process

Abstract

Today, the amount of production and production-related waste has increased in order to meet the rapidly increasing consumption. Recycling processes have become inevitable in order to dispose of the resulting wastes without harming the environment and human health and to bring them into the economy. In this study, the recovery of sodium-based waste powder soap used in wire drawing processes was carried out. The ion solution method, which is a physical separation method, was used. With this method, the recovery rate was found to be 98%. Thermal and chemical analyzes were carried out with thermogravimetric and differential thermal analyzes device (TGA/DTA), X-ray fluorescence spectrometer device (XRF) and Fourier transform infrared spectroscopy (FTIR) to determine if there is any change in the structure of the material obtained after recovery.

Keywords

• Wire Drawing
• Die Soap
• Recovery
• Ion Solution.

Supporting Institution

TÜBİTAK

Project Number

3190313

Thanks

This study has been carried out within Hasçelik Cable Industry and Trade Incorporated Company R & D center. Thanks to Hasçelik Cable Industry and Trade Incorporated Company and TUBITAK for its contribution to this work.

Tel Çekme İşleminde Kullanılan Toz Sabunun Geri Kazanımı İçin Filtreleme ve Optimizasyon

Abstract

Günümüzde hızla artan tüketimi karşılamak için üretim ve üretime bağlı atık miktarı artmıştır. Ortaya çıkan atıkların çevreye ve insan sağlığına zarar vermeden bertaraf edilmesi ve ekonomiye kazandırılması için geri dönüşüm süreçleri kaçınılmaz hale gelmiştir. Bu çalışmada, tel çekme işlemlerinde kullanılan sodyum bazlı atık toz sabunun geri kazanımı gerçekleştirilmiştir. Fiziksel ayırma yöntemi olan iyon çözelti yöntemi kullanılmıştır. Bu yöntemle iyileşme oranı %98 olarak bulunmuştur. Termogravimetrik ve diferansiyel termal analiz cihazı (TGA/DTA), X-ışını floresan spektroskopisi cihazı (XRF) ve Fourier transform kızılötesi spektroskopisi (FTIR) ile geri kazanım sonrası elde edilen malzemenin yapısında herhangi bir değişiklik olup olmadığını belirlemek için termal ve kimyasal analizler yapılmıştır.

Keywords

• Tel Çekme
• Hadde Sabunu
• Geri Kazanım
• İyon Çözeltisi

Project Number

3190313

References

1. Brard, D., 1991. Lubrication - Quality and Innevation, Wire Industry, 733-734.
2. Eickemeyer, J., Vogel, H.R., Reichert, J. and Rehm, M., 1996. Metal drawing by means of solid soap films. Journal of Materials Processing Technology, 61, 250-253.
3. European Commission, March 2019. “Best Available Techniques (BAT) Reference Document for the Ferrous Metals Processing Industry”.
4. Felder, E., Levrau, C., Mantel, M. and Dinh, N.G.H., 2011. Experimental study of the lubrication by soaps in stainless steel wire drawing. Part J: Journal of Engineering Tribology, 225, 915-923.
5. Hillery, M.T. and McCabe, V.J., 1995. Wire drawing at elevated temperatures using different die materials and lubricants. Journal of Materials Processing Technology, 55, 53-57.
6. Hwang, J.K., 2020. Effect of drawing speed on microstructure distribution and drawability in twinning-induced plasticity steel during wire drawing. Journal of Iron and Steel Research International, 27, 577-587.
7. Jeimin, R. Joshi, Khodidas, K., Bhanderi, J. and Patel, V., (2023). Waste cooking oil as a promising source for bio lubricants-A review. Journal of the Indian Chemical Society, 100, 100820.
8. Joong-Ki, H. and Young-Chul, C., 2023. Effects of Contact Conditions at Wire–Die Interface on Temperature Distribution during Wire Drawing. Processes, 11, 513-528.

9. Kauffmann, A., Freudenberger, J., Klauß, H., Schillinger, W., Subramanya Sarma, V. and Schultz, L., 2015. Efficiency of the refinement by deformation twinning in wire drawn single phase copper alloys. Material Science and Engineering A, 624, 71-78.
10. Kubota, H., Akimoto, Y., Saito, K., Sakurazawa, W. and Yoshida, K., 2021. Residual Stress Control in Drawn Bar and Wire by Heating-Cooling-Drawing Process. ISIJ International, 61, 2792-2797.
11. Liu, J.P., Chen, J.X., Liu, T.W., Li, C., Chen, Y. and Dai, L.H. 2020. Superior strength-ductility CoCrNi medium-entropy alloy wire. AMI: Scripta Materialia, 181, 19-24.
12. McNulty, M., 2006. Spotlight on Drawing Machines, Wire and Cable Technology, 54 – 56.
13. Murakawa, M., Jin, M. and Hayashi, M., 2004. Study on semidry/dry wire drawing using DLC coated dies. Surface and Coatings Technology, 177, 631-637.
14. Özer, Ö. And Yurci, M. 1997. Tel Çekme İşleminde Matris Açılarının Optimizasyonu ve Sapmaların Belirlenmesi. ODTÜ Makine Fakültesi 1. Makine Mühendisliği Kongresi, İstanbul.
15. Sarma, R.N. and Vinu, R., 2022. Current status and future prospects of biolubricants: properties and applications. Lubricants, 10, 70-91.
16. Strzepek, P., Mamala, A., Zasadznska, M., Franczak, K. And Jurkiewicz, B., 2019. Research on the drawing process of Cu and CuZn wires obtained in the cryogenic conditions. Cryogenics, 100, 11-17.
17. Sun-Ho, K., Gyu-Chul, J. and Chi-Wook, L., 2014. Development and Evaluation of Dry Lubricant Recycle Technologies for Wire Drawing Process. Journal of the Korean Society of Manufacturing Process Engineers, 13, 35-40.
18. Tripp, I., 1998. “Health and Safety Concerns for the Wire Drawing Industry, Wire and Cable Technology”, 55-56.
19. Wei, D., Min, X., Hu, X., Xie, Z. and Fang, F., 2020. Microstructure and mechanical properties of cold drawn pearlitic steel wires: Effects of drawing-induced heating. Material Science and Engineering A, 784, 139341.
20. Wright, R.N., 2011. Wire Technology:Process Engineering and Metallurgy, doi:10.1016/B978-0-12-382092-1.00002-6, Elsevier, Oxford,UK.