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Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil

Year 2019, NSP2018 Special Issue, 165 - 173, 28.03.2019

Abstract

The
uncertainty of a measurement is the interval of values within which the true
value is believed to lie with a stated probability when all sources of error
have been taken into account and is therefore represents the reliability of a
measurement. In this study, we evaluate the measurement uncertainty in the determination
of 230Th in the soil sample using a radiochemical separation
procedure and alpha spectrometry. All the sources in the analysis method that
contribute to the combined uncertainty were identified. The uncertainty
associated with a certain parameter was used to determine its partial
contribution to the combined standard uncertainty of the measurand. The spreadsheet
and full matematical approach was used to present the combined standard
uncertainty. 

References

  • Vreček P., Benedik L., “Evaluation of measurement uncertainty in the determination of 210Pb and 210Po using beta counting and alpha spectrometry” Accred. Qual. Assur. 8, 134-137 (2003).
  • Heydorn, K., “Evaluation of the uncertainty of environmental measurements of radioactivity” Journal of Radioanalytical and Nuclear Chemistry. 262, No. 1 249-253 (2004).
  • ISO, 1995. “ISO Guide to the expression of uncertainty in measurement” International Organization for Standardization, Geneva,ISBN:92-67r-r10188-9 (Available online from http://www.bipm.org/en/publications/guides/gum.html)
  • Guimarães Couto, P. R., Damasceno, C. D., and Pinheiro de Oliveira, S., “Monte Carlo Simulations Applied to Uncertainty in Measurement” Theory and Applications of Monte Carlo Simulations. Chapter 2, 27-51, DOI: 10.5772/53014.
  • Modna, D. K., Jerome, S. M., White, M. A., Woods, M. J., “Thorium in workplace measurement intercomparison”. Applied Radiation isotopes, 53, 265-271 (2000).
  • Jia, G., Torri, G., Ocone, R., Di Lullo, A., De Angelis, A., & Boschetto, R., “Determination of thorium isotopes in mineral and environmental water and soil samples by α-spectrometry and the fate of thorium in water” Applied Radiation and Isotopes, 66 (10), 1478-1487, (2008).
  • Eichrom Technologies, LLC Method No: ACW10VBS Analytical Procedure Revision: 1.1 May 1, 2014
  • Eichrom Technologies, LLC Method No: ACW03 Analytical Procedure Revision: 2.2 May 1, 2014
  • Kanisch, G., “Alpha-spectrometric analysis of environmental samples” (IAEA-TEC-DOC-1401). Quantifying Uncertainty in Nuclear Analytical Measurements. International Atomic Energy Agency, Vienna, pp. 127–139 (2004).
  • Holmes, L., “Alpha Spectrometric Analysis of Environmental Samples Spreadsheet approach” (IAEA-TEC-DOC-1401) Quantifying Uncertainty in Nuclear Analytical Measurements. International Atomic Energy Agency, Vienna, pp. 114–149 (2004).

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Year 2019, NSP2018 Special Issue, 165 - 173, 28.03.2019

Abstract

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References

  • Vreček P., Benedik L., “Evaluation of measurement uncertainty in the determination of 210Pb and 210Po using beta counting and alpha spectrometry” Accred. Qual. Assur. 8, 134-137 (2003).
  • Heydorn, K., “Evaluation of the uncertainty of environmental measurements of radioactivity” Journal of Radioanalytical and Nuclear Chemistry. 262, No. 1 249-253 (2004).
  • ISO, 1995. “ISO Guide to the expression of uncertainty in measurement” International Organization for Standardization, Geneva,ISBN:92-67r-r10188-9 (Available online from http://www.bipm.org/en/publications/guides/gum.html)
  • Guimarães Couto, P. R., Damasceno, C. D., and Pinheiro de Oliveira, S., “Monte Carlo Simulations Applied to Uncertainty in Measurement” Theory and Applications of Monte Carlo Simulations. Chapter 2, 27-51, DOI: 10.5772/53014.
  • Modna, D. K., Jerome, S. M., White, M. A., Woods, M. J., “Thorium in workplace measurement intercomparison”. Applied Radiation isotopes, 53, 265-271 (2000).
  • Jia, G., Torri, G., Ocone, R., Di Lullo, A., De Angelis, A., & Boschetto, R., “Determination of thorium isotopes in mineral and environmental water and soil samples by α-spectrometry and the fate of thorium in water” Applied Radiation and Isotopes, 66 (10), 1478-1487, (2008).
  • Eichrom Technologies, LLC Method No: ACW10VBS Analytical Procedure Revision: 1.1 May 1, 2014
  • Eichrom Technologies, LLC Method No: ACW03 Analytical Procedure Revision: 2.2 May 1, 2014
  • Kanisch, G., “Alpha-spectrometric analysis of environmental samples” (IAEA-TEC-DOC-1401). Quantifying Uncertainty in Nuclear Analytical Measurements. International Atomic Energy Agency, Vienna, pp. 127–139 (2004).
  • Holmes, L., “Alpha Spectrometric Analysis of Environmental Samples Spreadsheet approach” (IAEA-TEC-DOC-1401) Quantifying Uncertainty in Nuclear Analytical Measurements. International Atomic Energy Agency, Vienna, pp. 114–149 (2004).
There are 10 citations in total.

Details

Primary Language English
Journal Section Makaleler
Authors

Meryem Seferinoğlu

Pınar Esra Erden This is me

Publication Date March 28, 2019
Submission Date December 4, 2018
Acceptance Date December 21, 2018
Published in Issue Year 2019 NSP2018 Special Issue

Cite

APA Seferinoğlu, M., & Erden, P. E. (2019). Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil. ALKÜ Fen Bilimleri Dergisi165-173.
AMA Seferinoğlu M, Erden PE. Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil. ALKÜ Fen Bilimleri Dergisi. Published online March 1, 2019:165-173.
Chicago Seferinoğlu, Meryem, and Pınar Esra Erden. “Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil”. ALKÜ Fen Bilimleri Dergisi, March (March 2019), 165-73.
EndNote Seferinoğlu M, Erden PE (March 1, 2019) Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil. ALKÜ Fen Bilimleri Dergisi 165–173.
IEEE M. Seferinoğlu and P. E. Erden, “Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil”, ALKÜ Fen Bilimleri Dergisi, pp. 165–173, March 2019.
ISNAD Seferinoğlu, Meryem - Erden, Pınar Esra. “Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil”. ALKÜ Fen Bilimleri Dergisi. March 2019. 165-173.
JAMA Seferinoğlu M, Erden PE. Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil. ALKÜ Fen Bilimleri Dergisi. 2019;:165–173.
MLA Seferinoğlu, Meryem and Pınar Esra Erden. “Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil”. ALKÜ Fen Bilimleri Dergisi, 2019, pp. 165-73.
Vancouver Seferinoğlu M, Erden PE. Estimation of Measurement Uncertainty for 230Th Radioisotope Analysis in Soil. ALKÜ Fen Bilimleri Dergisi. 2019:165-73.