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Farklı Ülkelerden Sağlanan Kimyon (Cuminum cyminum L.) Tohumlarının Önemli Kalite Parametrelerinin Belirlenmesi

Year 2022, Volume: 32 Issue: 1, 133 - 142, 24.06.2022
https://doi.org/10.18615/anadolu.1131212

Abstract

Kimyon (Cuminum cyminum L.), dünya çapında en çok tüketilen baharatlardan biridir. Bu çalışmada materyal olarak Hindistan, İran, Suriye, Pakistan, Afganistan ve Türkiye'den (Denizli) elde edilen tohumlar kullanılmıştır. Tohumların uçucu yağ içeriği (%), uçucu yağ bileşimi (%), sabit yağ içeriği (%), sabit yağ bileşimi (%), renk değerleri (l, a, b), toplam fenolik madde (mg GAE/ g kuru ağırlık) ve toplam flavonoid madde (mg CE/g kuru ağırlık) belirlenmiştir. Sonuçlar, öğütülmemiş tohumlarda uçucu yağ oranının %1,08 ile %4,68 arasında değiştiğini, öğütülmüş tohumlarda ise %3,20 ile %5,02 arasında değiştiğini göstermiştir. Tüm kimyon tohumu örneklerinde gama-terpinen-7-al, cuminal, gama-terpinen ve beta-pinen öne çıkan ana bileşiklerdir. Sabit yağ oranı öğütülmemiş tohumlarda %2,38 ile %17,50 arasında, öğütülmüş tohumlarda %2,25 ile %17,47 arasında değişmektedir. Sabit yağın içeriği olarak 6 farklı yağ asidi belirlenmiştir. Bu yağ asitleri arasında oleik asit ana bileşendir. Oleik asit oranı %56,63 ile %65,12 arasında değişmektedir. Örneklerin CIE L*, a* ve b* renk değerleri 40,12-45,29, 2,37-7,88, 17,85-25,95 arasında yer almıştır. Kimyon tohumu örneklerinin toplam fenolik madde ve flavonoid içeriği sırasıyla 7,00-11,06 mg GAE/g DW, 2,04-5,08 mg CE/g DW arasında bulunmuştur.

References

  • Al-Snafi, A. E. 2016. The pharmacological activities of Cuminum cyminum - A review. IOSR Journal of Pharmacy, 2: 46-65.
  • Alinian, S., J. Razmjoo and H. Zeinali. 2016. Flavonoids, anthocynins, phenolics and essential oil produced in cumin (Cuminum cyminum L.) accessions under different irrigation regimes. Industrial Crops and Products, 81: 49-55.
  • Allaq, A. A., N. J. Sidik, A. Abdul-Aziz and I. A. Ahmed. 2020. Cumin (Cuminum cyminum L.): A review of its ethnopharmacology, phytochemistry. Biomedical Research and Therapy, 7 (9): 4016-4021.
  • Anonymous. 2011. TSE EN ISO 6571-Spices, condiments and herbs - Determination of volatile oil content (hydrodistillation method). Turkish Standards Institute, Ankara.
  • Aruna, G. and V. Baskaran. 2010. Comparative study on the levels of carotenoids lutein, zeaxanthin and b-carotene in Indian spices of nutritional and medicinal importance. Food Chemistry, 123: 404–409.
  • Bettaieb, I., S. Bourgou, J. Sriti, K. Msaada, F. Limam, and B. Marzouk. 2011. Essential oils and fatty acids composition of Tunisian and Indian cumin (Cuminum cyminum L.) seeds: a comparative study J Sci Food Agric 30;91(11): 2100-7.
  • Bhatt, J., S. Kumar, S. Patel and R. Solanki. 2017. Sequence-related amplified polymorphism (SRAP) markers based genetic diversity analysis of cumin genotypes. Annals of Agrarian Science, 15 (4): 434–438. Available from: https://doi.org/10.1016/ j.aasci.
  • Boughendjioua, H. 2019. Characterization of aroma active compounds of cumin (Cuminum cyminum L.) seed essential oil. Mod. Appl. Bioequiv., 4, 2 - DOI: 10.19080/MABB.2019.04.55563.
  • Cemeroglu, B. 2010. Gıda analizleri. Nobel Yayın Dağıtım, Ankara, 682 pp.
  • Çelik, S. Ayşe. and İ. Ayran. 2020. Chemical compositions of essential oil and crude oil of some fruits belonging to umbelliferae family cultivated in Konya ecological conditions. KSÜ Tarım ve Doğa Derg., 23(4): 1030-1038. Garces, R. and M. Mancha. 1993. One step lipid extraction and fatty acids methyl esters preparation from tree plant tissues. Analytical Biochemistry 211: 139-143.
  • Goodarzi, S., M. J. Tabatabaei, M. Jafari, R. Shemirani, F. Tavakoli, S. Mofasseri and M. Tofighi. 2018. Cuminum cyminum fruits as source of luteolin-7-O-glucoside, potent cytotoxic flavonoid against breast cancer cell lines. Natural Product Research, 1-5.
  • Gölükcü, M., R. Toker, H. Tokgöz and O. Çınar. 2016. The Effect of Harvesting Time on Seed Oil Content and Fatty Acid Composition of Some Lemon and Mandarin Cultivars Grown in Turkey. Journal of Agricultural Sciences, 22: 566-575.
  • Hajib, A., H. Harhara, S. Gharbyb, I. Nounaha, B. Matthäus, D. Guillaumed and Z. Charrouf. 2018. Is geographic origin a good marker for cumin seed oil (Cuminum cyminum L.). Rivista Italiana Delle Sostanze Grasse, 95(3): 155-159.
  • Kanani, P., Y. M. Shukla, A. R. Modi, N. Subhash and S. Kumar. 2019. Standardization of an efficient protocol for isolation of RNA from Cuminum cyminum L. Journal of King Saud University Science, 31(4): 1202-1207. Available from: https://doi.org/ 10.1016/j.
  • Karik, Ü., I. Demirbolat, Ö. Toluk and M. Kartal. 2021. Comparative study on yields, chemical compositions, antioxidant and antimicrobial activities of cumin (Cuminum cyminum L.) seed Essential Oils from Different Geographic Origins. Journal of Essential Oil Bearing Plants, 24(4): 724-735. doı: 10.1080/ 0972060X.2021.1983472.
  • Keskin, S. 2015. Umbelliferae Familyasından Bazı Önemli Kültür Türlerinin Isparta Ekolojik Koşullarında Tarımsal ve Teknolojik Özelliklerinin Belirlenmesi. Süleyman Demirel Ün. Fen Bil. Enst. Tar. Bit. Anabilim Yüksek Lisans Tezi, 110 s.
  • Kirkin, C., B. Mitrevsk, G. Gunes and P. J. Marriott. 2014. Combined effects of gamma-irradiation and modified atmosphere packaging on quality of some spices Food Chemistry 154: 255-261.
  • Moghaddam, M., S. N. K. Miran, A. G. Pirbalouti, L. Mehdizadeh and Y. Ghaderi. 2015. Variation in essential oil composition and antioxidant activity of cumin (Cuminum cyminum L.) fruits during stages of maturity. Industrial Crops and Products, 70: 163-169. Available from: https://doi.org/10.1016/j.
  • Nadeem M. and A. Riaz. 2012. Cumin (Cuminum cyminum) as a potential source of antioxidants. Pak. J. Food Sci., 22 (2): 101-107.
  • Özdemir, M. 2001. Mathematical analysis of color changes and chemical parameters of roasted hazelnuts. Ph. D. Thesis. Istanbul Technical University, 161 pp.
  • Piri, R., A. Moradi, H. Balouchi and A. Salehi. 2019. Improvement of cumin (Cuminum cyminum L.) seed performance under drought stress by seed coating and biopriming. Scientia Horticulturae, 257, 108667. Available from: https://doi.org/10.1016/j.
  • Rebey, I. B., S. Bourgou, I. B. Slimen, D. Iness, J. Karoui, I. Hamrouni, S. Kamel, M. F. Limama and B. Marzouk. 2012. Effects of Extraction Solvents and Provenances on Phenolic Contents and Antioxidant Activities of Cumin (Cuminum cyminum L.) Seeds. Food Bioprocess Technol 5.
  • Rebey, I. B., S. Bourgou, F. Z. Rahali, K. Msaada, R. Ksouri and B. Marzouk. 2017. Relation between salt tolerance and biochemical changes in cumin (Cuminum cyminum L.) seeds. Journal of Food and Drug Analysis. 25(2): 391-402. Availablefrom: https://doi.org/ 10.1016/j.jfda.
  • Shahnaz, A., H. Hamid, K. Bushra and J. I. Khan. 2004. Lipid studies of Cuminum cyminum fixed oil Pak. J. Bot., 36 (2): 395-401.
  • Shukla, N., N. R. Siddarth, J. Sharma and S. 2018. Tiwar Evaluation of volatile compounds and fatty acid methyl ester (Fame) through gas Chromatograhy in cumin seeds (Cuminum cyminum). Journal of Pharmacognosy and Phytochemistry, 7(4): 1125-1129.
  • Singh, R. P., H. V. Gangadharappa and K. Mruthunjaya. 2017. Cuminum cyminum – A Popular Spice: An Updated Review. Pharmacogn J., 9(3): 292-301.
  • Spanos, G. and R. E. Wrolstad. 1990. Phenolics of apple. pear and white grape juices and their changes with processing and storage. J Agric Food Chem, 40: 1478-1487.
  • Tayade, P. and R. Adivarekar. 2013. Dyeing of cotton fabric with Cuminum cyminum L. as a natural dye and its comparison with synthetic dye. Journal of the Textile Institute, 104 (10).
  • Thippeswamy, N. and K. A. Naidu. 2005. Antioxidant potency of cumin varieties-cumin, black cumin and bitter cumin-on antioxidant systems. European Food Research and Technology, 220(5-6): 472-476. Available from: https://doi.org/10. 1007/s00217-004-1087-y.
  • Uysal Bayar, F. and O. Çınar. 2020. Yield and quality parameters of some cultivated Origanum spp. Species. Derim, 37(1) : 10-17.
  • Zheljazkov, V. D. and S. Shiwakoti. 2015. Yield, composition, and antioxidantcapacity of ground cumin seed oil fractions obtained at different time points during the hydrodistillation. Hortscience, 50(8): 1213-1217.
  • Zhishen, J., M. Tang, and J. Wu. 1999. The determination of flavonoid contents in mulberry and their scavenging effects on superoxide radicals. Food Chem., 64: 555-559.

Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries

Year 2022, Volume: 32 Issue: 1, 133 - 142, 24.06.2022
https://doi.org/10.18615/anadolu.1131212

Abstract

Cumin (Cuminum cyminum L.) is one of the most consumed spices worldwide. In this study, seeds obtained from India, Iran, Syria, Pakistan, Afghanistan and Türkiye (Denizli) were used as the materials. Different parameters including essential oil content of seeds (%), essential oil composition (%), fixed oil content (%), fatty acid composition (%), colour values (l, a, b), total phenolic substance (mg GAE/g dry herb) and total flavonoid substance (mg CE/g dry herb) were determined. Result showed that the content of essential oil in unground seeds varied between 1.08% and 4.68%, while, the values were 3.20%-5.02% in ground seeds. Gamma-terpinen-7-al, cuminal, gamma-terpinene and beta-pinene were the prominent main compounds in all cumin seed samples. The fixed oil content ranged from 2.38% to 17.50% in unground seeds and 2.25% to 17.47% in ground seeds. Six different fatty acids were found in fixed oil. Among these fatty acids, oleic acid was the main component. Oleic acid level varied between 56.63% and 65.12%. The CIE L*, a* and b* colour values of the samples ranged between 40.12-45.29, 2.37-7.88, and 17.85-25.95, respectively. Total phenolic matter and flavonoid content of the cumin seed samples were founded between 7.00-11.06 mg GAE/g DW and 2.04-5.08 mg CE/g DW, respectively.

References

  • Al-Snafi, A. E. 2016. The pharmacological activities of Cuminum cyminum - A review. IOSR Journal of Pharmacy, 2: 46-65.
  • Alinian, S., J. Razmjoo and H. Zeinali. 2016. Flavonoids, anthocynins, phenolics and essential oil produced in cumin (Cuminum cyminum L.) accessions under different irrigation regimes. Industrial Crops and Products, 81: 49-55.
  • Allaq, A. A., N. J. Sidik, A. Abdul-Aziz and I. A. Ahmed. 2020. Cumin (Cuminum cyminum L.): A review of its ethnopharmacology, phytochemistry. Biomedical Research and Therapy, 7 (9): 4016-4021.
  • Anonymous. 2011. TSE EN ISO 6571-Spices, condiments and herbs - Determination of volatile oil content (hydrodistillation method). Turkish Standards Institute, Ankara.
  • Aruna, G. and V. Baskaran. 2010. Comparative study on the levels of carotenoids lutein, zeaxanthin and b-carotene in Indian spices of nutritional and medicinal importance. Food Chemistry, 123: 404–409.
  • Bettaieb, I., S. Bourgou, J. Sriti, K. Msaada, F. Limam, and B. Marzouk. 2011. Essential oils and fatty acids composition of Tunisian and Indian cumin (Cuminum cyminum L.) seeds: a comparative study J Sci Food Agric 30;91(11): 2100-7.
  • Bhatt, J., S. Kumar, S. Patel and R. Solanki. 2017. Sequence-related amplified polymorphism (SRAP) markers based genetic diversity analysis of cumin genotypes. Annals of Agrarian Science, 15 (4): 434–438. Available from: https://doi.org/10.1016/ j.aasci.
  • Boughendjioua, H. 2019. Characterization of aroma active compounds of cumin (Cuminum cyminum L.) seed essential oil. Mod. Appl. Bioequiv., 4, 2 - DOI: 10.19080/MABB.2019.04.55563.
  • Cemeroglu, B. 2010. Gıda analizleri. Nobel Yayın Dağıtım, Ankara, 682 pp.
  • Çelik, S. Ayşe. and İ. Ayran. 2020. Chemical compositions of essential oil and crude oil of some fruits belonging to umbelliferae family cultivated in Konya ecological conditions. KSÜ Tarım ve Doğa Derg., 23(4): 1030-1038. Garces, R. and M. Mancha. 1993. One step lipid extraction and fatty acids methyl esters preparation from tree plant tissues. Analytical Biochemistry 211: 139-143.
  • Goodarzi, S., M. J. Tabatabaei, M. Jafari, R. Shemirani, F. Tavakoli, S. Mofasseri and M. Tofighi. 2018. Cuminum cyminum fruits as source of luteolin-7-O-glucoside, potent cytotoxic flavonoid against breast cancer cell lines. Natural Product Research, 1-5.
  • Gölükcü, M., R. Toker, H. Tokgöz and O. Çınar. 2016. The Effect of Harvesting Time on Seed Oil Content and Fatty Acid Composition of Some Lemon and Mandarin Cultivars Grown in Turkey. Journal of Agricultural Sciences, 22: 566-575.
  • Hajib, A., H. Harhara, S. Gharbyb, I. Nounaha, B. Matthäus, D. Guillaumed and Z. Charrouf. 2018. Is geographic origin a good marker for cumin seed oil (Cuminum cyminum L.). Rivista Italiana Delle Sostanze Grasse, 95(3): 155-159.
  • Kanani, P., Y. M. Shukla, A. R. Modi, N. Subhash and S. Kumar. 2019. Standardization of an efficient protocol for isolation of RNA from Cuminum cyminum L. Journal of King Saud University Science, 31(4): 1202-1207. Available from: https://doi.org/ 10.1016/j.
  • Karik, Ü., I. Demirbolat, Ö. Toluk and M. Kartal. 2021. Comparative study on yields, chemical compositions, antioxidant and antimicrobial activities of cumin (Cuminum cyminum L.) seed Essential Oils from Different Geographic Origins. Journal of Essential Oil Bearing Plants, 24(4): 724-735. doı: 10.1080/ 0972060X.2021.1983472.
  • Keskin, S. 2015. Umbelliferae Familyasından Bazı Önemli Kültür Türlerinin Isparta Ekolojik Koşullarında Tarımsal ve Teknolojik Özelliklerinin Belirlenmesi. Süleyman Demirel Ün. Fen Bil. Enst. Tar. Bit. Anabilim Yüksek Lisans Tezi, 110 s.
  • Kirkin, C., B. Mitrevsk, G. Gunes and P. J. Marriott. 2014. Combined effects of gamma-irradiation and modified atmosphere packaging on quality of some spices Food Chemistry 154: 255-261.
  • Moghaddam, M., S. N. K. Miran, A. G. Pirbalouti, L. Mehdizadeh and Y. Ghaderi. 2015. Variation in essential oil composition and antioxidant activity of cumin (Cuminum cyminum L.) fruits during stages of maturity. Industrial Crops and Products, 70: 163-169. Available from: https://doi.org/10.1016/j.
  • Nadeem M. and A. Riaz. 2012. Cumin (Cuminum cyminum) as a potential source of antioxidants. Pak. J. Food Sci., 22 (2): 101-107.
  • Özdemir, M. 2001. Mathematical analysis of color changes and chemical parameters of roasted hazelnuts. Ph. D. Thesis. Istanbul Technical University, 161 pp.
  • Piri, R., A. Moradi, H. Balouchi and A. Salehi. 2019. Improvement of cumin (Cuminum cyminum L.) seed performance under drought stress by seed coating and biopriming. Scientia Horticulturae, 257, 108667. Available from: https://doi.org/10.1016/j.
  • Rebey, I. B., S. Bourgou, I. B. Slimen, D. Iness, J. Karoui, I. Hamrouni, S. Kamel, M. F. Limama and B. Marzouk. 2012. Effects of Extraction Solvents and Provenances on Phenolic Contents and Antioxidant Activities of Cumin (Cuminum cyminum L.) Seeds. Food Bioprocess Technol 5.
  • Rebey, I. B., S. Bourgou, F. Z. Rahali, K. Msaada, R. Ksouri and B. Marzouk. 2017. Relation between salt tolerance and biochemical changes in cumin (Cuminum cyminum L.) seeds. Journal of Food and Drug Analysis. 25(2): 391-402. Availablefrom: https://doi.org/ 10.1016/j.jfda.
  • Shahnaz, A., H. Hamid, K. Bushra and J. I. Khan. 2004. Lipid studies of Cuminum cyminum fixed oil Pak. J. Bot., 36 (2): 395-401.
  • Shukla, N., N. R. Siddarth, J. Sharma and S. 2018. Tiwar Evaluation of volatile compounds and fatty acid methyl ester (Fame) through gas Chromatograhy in cumin seeds (Cuminum cyminum). Journal of Pharmacognosy and Phytochemistry, 7(4): 1125-1129.
  • Singh, R. P., H. V. Gangadharappa and K. Mruthunjaya. 2017. Cuminum cyminum – A Popular Spice: An Updated Review. Pharmacogn J., 9(3): 292-301.
  • Spanos, G. and R. E. Wrolstad. 1990. Phenolics of apple. pear and white grape juices and their changes with processing and storage. J Agric Food Chem, 40: 1478-1487.
  • Tayade, P. and R. Adivarekar. 2013. Dyeing of cotton fabric with Cuminum cyminum L. as a natural dye and its comparison with synthetic dye. Journal of the Textile Institute, 104 (10).
  • Thippeswamy, N. and K. A. Naidu. 2005. Antioxidant potency of cumin varieties-cumin, black cumin and bitter cumin-on antioxidant systems. European Food Research and Technology, 220(5-6): 472-476. Available from: https://doi.org/10. 1007/s00217-004-1087-y.
  • Uysal Bayar, F. and O. Çınar. 2020. Yield and quality parameters of some cultivated Origanum spp. Species. Derim, 37(1) : 10-17.
  • Zheljazkov, V. D. and S. Shiwakoti. 2015. Yield, composition, and antioxidantcapacity of ground cumin seed oil fractions obtained at different time points during the hydrodistillation. Hortscience, 50(8): 1213-1217.
  • Zhishen, J., M. Tang, and J. Wu. 1999. The determination of flavonoid contents in mulberry and their scavenging effects on superoxide radicals. Food Chem., 64: 555-559.
There are 32 citations in total.

Details

Primary Language English
Subjects Agricultural Engineering (Other), Agricultural, Veterinary and Food Sciences
Journal Section Makaleler
Authors

Ünal Karık This is me 0000-0001-6707-191X

Orçun Çınar This is me 0000-0002-8356-384X

Muharrem Gölükçü This is me 0000-0003-1646-5876

Early Pub Date June 21, 2022
Publication Date June 24, 2022
Submission Date March 21, 2022
Published in Issue Year 2022 Volume: 32 Issue: 1

Cite

APA Karık, Ü., Çınar, O., & Gölükçü, M. (2022). Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries. ANADOLU Ege Tarımsal Araştırma Enstitüsü Dergisi, 32(1), 133-142. https://doi.org/10.18615/anadolu.1131212
AMA Karık Ü, Çınar O, Gölükçü M. Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries. ANADOLU. June 2022;32(1):133-142. doi:10.18615/anadolu.1131212
Chicago Karık, Ünal, Orçun Çınar, and Muharrem Gölükçü. “Determination of Important Quality Parameters of Cumin (Cuminum Cyminum L.) Seeds Provided by Different Countries”. ANADOLU Ege Tarımsal Araştırma Enstitüsü Dergisi 32, no. 1 (June 2022): 133-42. https://doi.org/10.18615/anadolu.1131212.
EndNote Karık Ü, Çınar O, Gölükçü M (June 1, 2022) Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries. ANADOLU Ege Tarımsal Araştırma Enstitüsü Dergisi 32 1 133–142.
IEEE Ü. Karık, O. Çınar, and M. Gölükçü, “Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries”, ANADOLU, vol. 32, no. 1, pp. 133–142, 2022, doi: 10.18615/anadolu.1131212.
ISNAD Karık, Ünal et al. “Determination of Important Quality Parameters of Cumin (Cuminum Cyminum L.) Seeds Provided by Different Countries”. ANADOLU Ege Tarımsal Araştırma Enstitüsü Dergisi 32/1 (June 2022), 133-142. https://doi.org/10.18615/anadolu.1131212.
JAMA Karık Ü, Çınar O, Gölükçü M. Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries. ANADOLU. 2022;32:133–142.
MLA Karık, Ünal et al. “Determination of Important Quality Parameters of Cumin (Cuminum Cyminum L.) Seeds Provided by Different Countries”. ANADOLU Ege Tarımsal Araştırma Enstitüsü Dergisi, vol. 32, no. 1, 2022, pp. 133-42, doi:10.18615/anadolu.1131212.
Vancouver Karık Ü, Çınar O, Gölükçü M. Determination of Important Quality Parameters of Cumin (Cuminum cyminum L.) Seeds Provided by Different Countries. ANADOLU. 2022;32(1):133-42.
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