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Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi

Year 2022, , 81 - 90, 17.01.2022

Burak Kıvrak , Mustafa Akyol

https://doi.org/10.21205/deufmd.2022247009

Abstract

Son yıllarda, geçiş metali kalkojenleri (GMK) kendilerine özgü fiziksel ve kimyasal özelliklerinden dolayı çokça çalışılan malzeme gruplarından biri olmuştur. GMK’ler, optoelektronik uygulamalarda, hidrojen evrim reaksiyonları, enerji depolama sistemleri, güneş pili uygulamalarında ve radar emici sistemlerde sıkça kullanılmaktadır. Bu çalışmada, farklı çözücüler ve ısıl işlem süreçleri kullanılarak üretilen GMK grubundan olan MoS2 ince filmlerinin yapısal özellikleri araştırılmıştır. İnce filmler sol-gel spin kaplama yöntemi ile üretilmiştir. Filmlerin kristalizasyonu farklı sıcaklık değerlerinde vakum altında tutulan ve azot gazı (N2) akışı sağlanan fırın sisteminde sağlanmıştır. Isıl işlem sıcaklığı ve çözücü kimyasalın etkisi yapısal analiz metotları ile değerlendirilmiştir. Bu kapsamda, X-ışını kırınım metodu (XRD) ve Raman saçınım ve taramalı elektron mikroskop (SEM) metodu filmlerin yapısal analizlerinin yapılmasında kullanılmıştır.

Keywords

MoS2 İnce film sol-jel termal ayrışma

References

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Investigation of the Effect of Solvent and Heat Treatment Process on Structural Properties of MoS2 Thin Films

Year 2022, , 81 - 90, 17.01.2022

Burak Kıvrak , Mustafa Akyol

https://doi.org/10.21205/deufmd.2022247009

Abstract

In recent years, transition metal dichalcogenides (TMDCs) have become one of the most studied material groups due to their unique physical and chemical properties. The TMDCs are frequently used in optoelectronic applications, hydrogen evolution reactions, energy storage systems, solar cells, and radar absorbing systems. In this study, the structural properties of MoS2 thin films, belonging to one of the TMDCs group, produced by using different solvents and heat treatment processes were investigated. Thin films were produced by using the sol-gel spin coating technique. The crystallization of the films was ensured at different heat treatment temperature values under a vacuum atmosphere by introducing N2 gas flow. The effects of the heat treatment temperature and chemical solvent were evaluated by the structural characterizations techniques. Within this scope, the X-ray diffraction method (XRD), Raman scattering, and scanning electron microscope (SEM) were used to investigate the structural properties of films.

Keywords

: MoS2 Thin Film Sol-gel Thermal decomposition

References

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There are 59 citations in total.

Details

Primary Language Turkish
Journal Section Research Article
Authors

Burak Kıvrak 0000-0002-6785-7346

Mustafa Akyol 0000-0001-8584-0620

Publication Date January 17, 2022
Published in Issue Year 2022

Cite

APA Kıvrak, B., & Akyol, M. (2022). Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi, 24(70), 81-90. https://doi.org/10.21205/deufmd.2022247009
AMA Kıvrak B, Akyol M. Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi. DEUFMD. January 2022;24(70):81-90. doi:10.21205/deufmd.2022247009
Chicago Kıvrak, Burak, and Mustafa Akyol. “Çözücü Ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi 24, no. 70 (January 2022): 81-90. https://doi.org/10.21205/deufmd.2022247009.
EndNote Kıvrak B, Akyol M (January 1, 2022) Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen ve Mühendislik Dergisi 24 70 81–90.
IEEE B. Kıvrak and M. Akyol, “Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi”, DEUFMD, vol. 24, no. 70, pp. 81–90, 2022, doi: 10.21205/deufmd.2022247009.
ISNAD Kıvrak, Burak - Akyol, Mustafa. “Çözücü Ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen ve Mühendislik Dergisi 24/70 (January 2022), 81-90. https://doi.org/10.21205/deufmd.2022247009.
JAMA Kıvrak B, Akyol M. Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi. DEUFMD. 2022;24:81–90.
MLA Kıvrak, Burak and Mustafa Akyol. “Çözücü Ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi, vol. 24, no. 70, 2022, pp. 81-90, doi:10.21205/deufmd.2022247009.
Vancouver Kıvrak B, Akyol M. Çözücü ve Isıl İşlem Sürecinin MoS2 İnce Filmlerinin Yapısal Özelliklerine Etkisinin İncelenmesi. DEUFMD. 2022;24(70):81-90.

Dokuz Eylül Üniversitesi, Mühendislik Fakültesi Dekanlığı Tınaztepe Yerleşkesi, Adatepe Mah. Doğuş Cad. No: 207-I / 35390 Buca-İZMİR.