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EFFECT OF PROBE DIAMETER ON STRUCTURE AND MORPHOLOGICAL PROPERTIES OF TiO2 AND ZrO2 POWDERS IN ULTRASONICATION PROCESS

Year 2016, Volume: 18 Issue: 54, 304 - 316, 01.09.2016

Abstract

The effect of the probe radius on structural and morphological properties of TiO2 and ZrOpowders in ultrasonication process have investigated in this study. The powders have exposed the high-intense ultrasound generated by the titanium probes diameter of 7 mm and 40 mm. X-ray diffraction (XRD) analysis proved that the some phases of the samples have disappeared while the some new phases of them have emerged after ultrasonication. Scanning Electron Microscopy (SEM) showed that the submicron particles could be obtained by the method. 7 mm probe generated by a high amplitude ultrasound was more effective than 40 mm diameter generated by a lower amplitude ultrasound

References

  • Piconi, C. and Maccauro, G. (1999) Zirconia as a ceramic biomaterial. Biomaterials, 20, 1–25. http://dx.doi.org/10.1016/S0142-9612(98)00010-6
  • Kelly, J.R. and Denry, I. (2008) Stabilized zirconia as a structural ceramic: an overview. Dental Materials : Official Publication of the Academy of Dental Materials, 24, 289–98. http://dx.doi.org/10.1016/j.dental.2007.05.005
  • Tsukuma, K., Kubota, Y. and Tsukidate, T. (1983) Thermal and mechanical properties of Y2O3-stabilized tetragonal zirconia polycrystals.
  • Nilüfer, İ., Gökçe, H., Çimenoğlu, H. and Öveçoğlu, L. (2014) Investigation of the Effects of Ceria Addition on the Properties of Zirconia. Mühendis ve Makina, 55, 31–3.
  • Chevalier, J., Gremillard, L., Virkar, A. V. and Clarke, D.R. (2009) The Tetragonal- Monoclinic Transformation in Zirconia: Lessons Learned and Future Trends. Journal of the American Ceramic Society, 92, 1901–20. http://dx.doi.org/10.1111/j.1551- 2916.2009.03278.x
  • Manicone, P.F., Rossi Iommetti, P. and Raffaelli, L. (2007) An overview of zirconia ceramics: basic properties and clinical applications. Journal of Dentistry, 35, 819–26. http://dx.doi.org/10.1016/j.jdent.2007.07.008
  • Bocanegra-Bernal, M.H. and Torre, S.D. de la. Phase transitions in zirconium dioxide and related materials for high performance engineering ceramics. Journal of Materials Science, http://dx.doi.org/10.1023/A:1021099308957 Academic Publishers. 37, 4947–71.
  • Lide, D. (2007) CRC Handbook of Chemistry and Physics, Internet Version, 2007. Taylor and Francis, Boca Raton, FL (Www.hbcpnetbase Com),.
  • Tusseau-Nenez, S., Ganne, J.P., Maglione, M., Morell, a., Niepce, J.C. and Paté, M. (2004) BST ceramics: Effect of attrition milling on dielectric properties. Journal of the European http://dx.doi.org/10.1016/j.jeurceramsoc.2003.11.019 Ceramic Society, 24, 3003–11.
  • Liu, C. and Liu, P. (2014) Microstructure and dielectric properties of BST ceramics derived from high-energy ball-milling. Journal of Alloys and Compounds, Elsevier B.V. 584, 114–8. http://dx.doi.org/10.1016/j.jallcom.2013.09.031
  • Vijatović Petrović, M.M., Bobić, J.D., Uršič, H., Banys, J. and Stojanović, B.D. (2013) The electrical properties of chemically obtained barium titanate improved by attrition milling. http://dx.doi.org/10.1007/s10971-013-3075-9 of Sol-Gel Science and Technology, 67, 267–72.
  • Manzoor, U. and Kim, D.K. (2007) Synthesis of nano-sized barium titanate powder by solid-state reaction between barium carbonate and titania. Journal of Materials Science & Technology, 23, 655–8.
  • Marković, S., Miljković, M., Jovalekić, Č., Mentus, S. and Uskoković, D. (2009) Densification, Microstructure, and Electrical Properties of BaTiO 3 (BT) Ceramics Prepared from Ultrasonically De-Agglomerated BT Powders. Materials and Manufacturing http://dx.doi.org/10.1080/10426910903031750 Taylor & Francis Group. 24, 1114–23.
  • Badr, M.H., El-Deen, L.M.S., Khafagy, A.H. and Nassar, D.U. (2011) Structural and mechanical properties characterization of barium strontium titanate (BST) ceramics. Journal of Electroceramics, 27, 189–96. http://dx.doi.org/10.1007/s10832-011-9664-5
  • Marković, S., Mitrić, M., Starcević, G. and Uskoković, D. (2008) Ultrasonic de- agglomeration of barium titanate powder. Ultrasonics Sonochemistry, 15, 16–20. http://dx.doi.org/10.1016/j.ultsonch.2007.07.008
  • Suslick, K.S., Didenko, Y., Fang, M.M., Hyeon, T., Kolbeck, K.J., McNamara III, W.B. et al. (1999) Acoustic cavitation and its chemical consequences. Philosophical Transactions http://dx.doi.org/10.1098/rsta.1999.0330 the Royal Society A, 357, 335–53.
  • Ashokkumar, M., Lee, J., Kentish, S. and Grieser, F. (2007) Bubbles in an acoustic field: an overview. Ultrasonics Sonochemistry, 14, 470–5.
  • Ashokkumar, M. (2011) The characterization of acoustic cavitation bubbles–an overview. Ultrasonics Sonochemistry, 18, 864–72.
  • Marković, S., Mitrić, M., Starcević, G. and Uskoković, D. (2008) Ultrasonic de- agglomeration of barium titanate powder. Ultrasonics Sonochemistry, 15, 16–20. http://dx.doi.org/10.1016/j.ultsonch.2007.07.008
  • Hielscher. (2016) Ultrasonic Sonotrodes, Flow Cells & Accessories [Internet].

ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ

Year 2016, Volume: 18 Issue: 54, 304 - 316, 01.09.2016

Abstract

Bu çalışmada, ultrasonikasyon işleminde prob çapının, TiO2 ve ZrO2 tozlarının yapısı ve morfolojik özellikleri üzerine etkisi incelenmiştir. Tozlara7 mm ve 40 mm çaplarındaki titanyum prob ile üretilen yüksek yoğunluklu ultrases dalgalarına maruz bırakılmıştır. X-ışını Kırınım (XRD) analizi ile ultrasonikasyon işlemi uygulanan tozlarda bazı yüzeylerin ortadan kaybolduğu ve bazı yeni yüzeylerin ortaya çıktığı bulunmuştur. Taramalı Elektron Mikroskopi (SEM) analizi bu yöntemle mikronaltı tane boyutlu tozların elde edilebildiğini göstermiştir.Büyük genlikli ultrasesüreten 7 mm çaplı probun küçük genlikli ultrases üreten 40 mm çaplı probdan daha etkili olduğu görülmüştür

References

  • Piconi, C. and Maccauro, G. (1999) Zirconia as a ceramic biomaterial. Biomaterials, 20, 1–25. http://dx.doi.org/10.1016/S0142-9612(98)00010-6
  • Kelly, J.R. and Denry, I. (2008) Stabilized zirconia as a structural ceramic: an overview. Dental Materials : Official Publication of the Academy of Dental Materials, 24, 289–98. http://dx.doi.org/10.1016/j.dental.2007.05.005
  • Tsukuma, K., Kubota, Y. and Tsukidate, T. (1983) Thermal and mechanical properties of Y2O3-stabilized tetragonal zirconia polycrystals.
  • Nilüfer, İ., Gökçe, H., Çimenoğlu, H. and Öveçoğlu, L. (2014) Investigation of the Effects of Ceria Addition on the Properties of Zirconia. Mühendis ve Makina, 55, 31–3.
  • Chevalier, J., Gremillard, L., Virkar, A. V. and Clarke, D.R. (2009) The Tetragonal- Monoclinic Transformation in Zirconia: Lessons Learned and Future Trends. Journal of the American Ceramic Society, 92, 1901–20. http://dx.doi.org/10.1111/j.1551- 2916.2009.03278.x
  • Manicone, P.F., Rossi Iommetti, P. and Raffaelli, L. (2007) An overview of zirconia ceramics: basic properties and clinical applications. Journal of Dentistry, 35, 819–26. http://dx.doi.org/10.1016/j.jdent.2007.07.008
  • Bocanegra-Bernal, M.H. and Torre, S.D. de la. Phase transitions in zirconium dioxide and related materials for high performance engineering ceramics. Journal of Materials Science, http://dx.doi.org/10.1023/A:1021099308957 Academic Publishers. 37, 4947–71.
  • Lide, D. (2007) CRC Handbook of Chemistry and Physics, Internet Version, 2007. Taylor and Francis, Boca Raton, FL (Www.hbcpnetbase Com),.
  • Tusseau-Nenez, S., Ganne, J.P., Maglione, M., Morell, a., Niepce, J.C. and Paté, M. (2004) BST ceramics: Effect of attrition milling on dielectric properties. Journal of the European http://dx.doi.org/10.1016/j.jeurceramsoc.2003.11.019 Ceramic Society, 24, 3003–11.
  • Liu, C. and Liu, P. (2014) Microstructure and dielectric properties of BST ceramics derived from high-energy ball-milling. Journal of Alloys and Compounds, Elsevier B.V. 584, 114–8. http://dx.doi.org/10.1016/j.jallcom.2013.09.031
  • Vijatović Petrović, M.M., Bobić, J.D., Uršič, H., Banys, J. and Stojanović, B.D. (2013) The electrical properties of chemically obtained barium titanate improved by attrition milling. http://dx.doi.org/10.1007/s10971-013-3075-9 of Sol-Gel Science and Technology, 67, 267–72.
  • Manzoor, U. and Kim, D.K. (2007) Synthesis of nano-sized barium titanate powder by solid-state reaction between barium carbonate and titania. Journal of Materials Science & Technology, 23, 655–8.
  • Marković, S., Miljković, M., Jovalekić, Č., Mentus, S. and Uskoković, D. (2009) Densification, Microstructure, and Electrical Properties of BaTiO 3 (BT) Ceramics Prepared from Ultrasonically De-Agglomerated BT Powders. Materials and Manufacturing http://dx.doi.org/10.1080/10426910903031750 Taylor & Francis Group. 24, 1114–23.
  • Badr, M.H., El-Deen, L.M.S., Khafagy, A.H. and Nassar, D.U. (2011) Structural and mechanical properties characterization of barium strontium titanate (BST) ceramics. Journal of Electroceramics, 27, 189–96. http://dx.doi.org/10.1007/s10832-011-9664-5
  • Marković, S., Mitrić, M., Starcević, G. and Uskoković, D. (2008) Ultrasonic de- agglomeration of barium titanate powder. Ultrasonics Sonochemistry, 15, 16–20. http://dx.doi.org/10.1016/j.ultsonch.2007.07.008
  • Suslick, K.S., Didenko, Y., Fang, M.M., Hyeon, T., Kolbeck, K.J., McNamara III, W.B. et al. (1999) Acoustic cavitation and its chemical consequences. Philosophical Transactions http://dx.doi.org/10.1098/rsta.1999.0330 the Royal Society A, 357, 335–53.
  • Ashokkumar, M., Lee, J., Kentish, S. and Grieser, F. (2007) Bubbles in an acoustic field: an overview. Ultrasonics Sonochemistry, 14, 470–5.
  • Ashokkumar, M. (2011) The characterization of acoustic cavitation bubbles–an overview. Ultrasonics Sonochemistry, 18, 864–72.
  • Marković, S., Mitrić, M., Starcević, G. and Uskoković, D. (2008) Ultrasonic de- agglomeration of barium titanate powder. Ultrasonics Sonochemistry, 15, 16–20. http://dx.doi.org/10.1016/j.ultsonch.2007.07.008
  • Hielscher. (2016) Ultrasonic Sonotrodes, Flow Cells & Accessories [Internet].
There are 20 citations in total.

Details

Other ID JA59MM75HZ
Journal Section Research Article
Authors

H.z. Akbas This is me

Z. Aydın This is me

İ.h. Karahan This is me

T. Dılsızoglu This is me

S. Turgut This is me

Publication Date September 1, 2016
Published in Issue Year 2016 Volume: 18 Issue: 54

Cite

APA Akbas, H., Aydın, Z., Karahan, İ., Dılsızoglu, T., et al. (2016). ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi, 18(54), 304-316.
AMA Akbas H, Aydın Z, Karahan İ, Dılsızoglu T, Turgut S. ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ. DEUFMD. September 2016;18(54):304-316.
Chicago Akbas, H.z., Z. Aydın, İ.h. Karahan, T. Dılsızoglu, and S. Turgut. “ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi 18, no. 54 (September 2016): 304-16.
EndNote Akbas H, Aydın Z, Karahan İ, Dılsızoglu T, Turgut S (September 1, 2016) ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen ve Mühendislik Dergisi 18 54 304–316.
IEEE H. Akbas, Z. Aydın, İ. Karahan, T. Dılsızoglu, and S. Turgut, “ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ”, DEUFMD, vol. 18, no. 54, pp. 304–316, 2016.
ISNAD Akbas, H.z. et al. “ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen ve Mühendislik Dergisi 18/54 (September 2016), 304-316.
JAMA Akbas H, Aydın Z, Karahan İ, Dılsızoglu T, Turgut S. ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ. DEUFMD. 2016;18:304–316.
MLA Akbas, H.z. et al. “ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ”. Dokuz Eylül Üniversitesi Mühendislik Fakültesi Fen Ve Mühendislik Dergisi, vol. 18, no. 54, 2016, pp. 304-16.
Vancouver Akbas H, Aydın Z, Karahan İ, Dılsızoglu T, Turgut S. ULTRASONİKASYON İŞLEMİNDE PROB ÇAPININ TiO2 VE ZrO2 TOZLARININ YAPI VE MORFOLOJİK ÖZELLİKLERİ ÜZERİNE ETKİSİ. DEUFMD. 2016;18(54):304-16.

Dokuz Eylül Üniversitesi, Mühendislik Fakültesi Dekanlığı Tınaztepe Yerleşkesi, Adatepe Mah. Doğuş Cad. No: 207-I / 35390 Buca-İZMİR.