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ZrN İnce Film Kaplamasının 1.2379 Soğuk İş Takım Çeliğindeki Aşınma Özelliğine Etkisinin İncelenmesi

Year 2022, Issue: 36, 1 - 5, 31.05.2022
https://doi.org/10.31590/ejosat.1091504

Abstract

Bu çalışmada katodik ark buharlaştırma yöntemi kullanılarak üretilen ZrN kaplamaların morfolojik, yapısal, sertlik ve sürtünme-aşınma özellikleri incelenmiştir. Kaplama işlemi için endüstride soğuk iş takım çeliği olarak sıklıkla kullanılan 1.2379 (AISI D2), taban malzeme olarak seçilmiştir. Üretilen ZrN kaplamasının yüzey özellikleri optik mikroskop ile tespit edilmiştir. Kaplamada oluşan fazlar ve yönlenmeler X-Işını difraksiyonu kullanılarak analiz edilmiştir. Hem taban hem de kaplanmış malzemenin sertlikleri Vickers tipi mikrosertlik cihazı kullanılarak belirlenmiştir. Aşınma deneyleri ise bilye-disk tipi aşınma test cihazında 2 N sabit yük altında 2500 ve 5000 çevrimlerde Al2O3 aşındırıcı yüzey kullanılarak gerçekleştirilmiştir. Oluşan aşınma oranları, aşınma izlerinin optik profilometre incelemeleri neticesinde belirlenmiştir. Aşınma mekanizmaları ise, oluşan aşınma izlerinin SEM’den elde edilen görüntüleri vasıtasıyla karakterize edilmiştir. ZrN kaplamada, NaCl tipi kübik kristal kafese sahip ZrN (111) fazının baskın yoğunlukta olduğu görülmüştür. ZrN kaplamasının sertliği yaklaşık 1882 HV0,01 değerinde olduğu ve taban malzemenin sertliği 448 HV0,01 değerinde olduğu görülmüştür. Bu durumda ZrN kaplanmış malzemenin sertlik değerinin taban malzemeye nazaran yaklaşık %300 daha yüksek olduğu tespit edilmiştir. Her iki çevrimde ZrN kaplamanın aşınma performansı taban malzemeye göre daha yüksek olduğu görülmüştür. İşlemsiz malzemede baskın aşınma mekanizması plastik deformasyon ve adezif aşınma iken, ZrN kaplanmış malzemede pullanma kaynaklı soyulmaların baskın mekanizma olduğu tespit edilmiştir.

References

  • Javari, A., Dehgani, K., Bahaaddini, K., Hataie, A. B., Experimental comparison of abrasive and erosive wear characteristics of four wear-resistant steels, Wear. 416-417: 14-26, (2018).
  • Yang, Y., Huang, L., Shi, Y., Adhesion suppresses atomic wear in single-asperity sliding, Wear. 352-353: 31-41, (2016).
  • Hacısalihoglu, I., Kaya, G., Ergüder, O. T., Mandev, E., Manay, E., Yıldız, F. Tribological and thermal properties of plasma nitrided Ti45Nb alloy, Surf. and Inter. 22: 100893, (2021).
  • Fernandez-Valdes, D., Meneses-Amador, A., Lopez-Lievano, A., Ocampa-Ramirez, A., Sliding wear analysis in borided AISI 316L steels, Mater. Lett. 285: 129138, (2021).
  • Azim, S., Gangopadhyay, S., Mahapatra, S. S., Mittal, R. K., Singh, R. K., Role of PVD coating on wear and surface integrity during environment-friendly micro-drilling of Ni-based superalloy, J. Cleaner Prod. 272: 122741, (2020).
  • Chowdhury, M. S. I., Bose, B., Yamamoto, K., Shuster, L. S., Paiva, J., Fox-Rabinovich, G. S., Veldhuis, S. C., Wear performance investigation of PVD coated and uncoated carbide tools during high-speed machining of TiAl6V4 aerospace alloy, Wear. 446-447: 203168, (2020).
  • Sert, Y., Küçükömeroğlu, T., Ghahramanzadeh Asl, H. The Effect of Al and Ti Transition Metals on the Wear Resistance of Ceramic Based CrN Coatings; Investigation under Ambient Air and Vacuum Conditions, Proc. Inst. Mech. Eng., Part L: J. Mater: Design and App. 236: 455-472, (2022).
  • Movassagh-Alanagh, F., Mahdavi, M., Improving wear and corrosion resistance of AISI 304 stainless steel by a multilayered nanocomposite Ti/TiN/TiSiN coating, Surf. and Inter. 18: 100428, (2020).
  • Chou, W.-J., Yu, G.-P., Huang, J.-H., Corrosion behavior of TiN-coated 304 stainless steel, Corr. Sci. 43: 2023-2035, (2001).
  • Kumar, S., Maity, S. R., Patnaik, L., Effect of heat treatment and TiN coating on AISI O1 cold work tool steel, Mater. Today: Proc. 26: 685-688, (2020).
  • Gonzalez-Carmona, J., Trivino, J. D., Gomez-Ovalle, A., Ortega, C., Alvarado-Orozco, J. M., Sanchez-Sthepa, H., Avila, A., Wear mechanisms identification using Kelvin probe force microscopy in TiN, ZrN and TiN/ZrN hard ceramic multilayers coatings, Ceram. Int. 46: 24592-24604, (2020).
  • Jianxin, D., Jianhua, L., Jinlong, Z., Wenlong, S., Ming, N., Friction and wear behaviors of the PVD ZrN coated carbide in sliding wear tests and in machining processes, Wear. 264: 298-307, (2008).
  • Jianxin, D., Jianhua, L., Jinlong, Z., Wenlong, S., Wear mechanisms of PVD ZrN coated tools in machining, Int. J. of Ref. Metals and Hard Mater. 264: 164-172, (2008).
  • Kuznetsova, T., Lapitskaya, V., Khabarava, A., Chiznik, S., Warcholinski, B., Gilewicz, A., The influence of nitrogen on the morphology of ZrN coatings deposited by magnetron sputtering, Appl. Surf. Sci. 522: 146508, (2020).
  • Feng, Y.-P., Zhang, L., Ke, R.-X., Wan, Q.-L., Wang, Z., Lu, Z.-H., Thermal stability and oxidation behavior of AlTiN, AlCrN and AlCrSiWN coatings, Int. J. Ref. Metals Hard Mater. 43: 241-249, (2014).
  • Maksakova, O. V., Simoes, S., Pogrebnjak, A. D., Bondar, O. V., Kravchenko, O., Koltunowicz, T. N., Shaimardanov, Zh. K., Multilayered ZrN/CrN coatings with enhanced thermal and mechanical properties, J. Alloys and Comp. vol. 776: 679-690, (2019).

Investigation of the Effect of ZrN Thin Film Coating on the Wear Properties of 1.2379 Cold Work Tool Steel

Year 2022, Issue: 36, 1 - 5, 31.05.2022
https://doi.org/10.31590/ejosat.1091504

Abstract

In this study, the morphological, structural, hardness and friction-wear properties of ZrN coatings produced by the cathodic arc evaporation method were investigated. 1.2379 (AISI D2), which is frequently used as a cold work tool steel in the industry, was chosen as the substarate material for coating process. The surface properties of the ZrN coating were determined using optical microscope. The phases and orientations of the coating were analyzed by X-Ray diffraction. The hardness of both the substrate and the coated material was determined using a Vickers type microhardness tester. Wear tests were carried out using Al2O3 ceramic abrader at 2500 and 5000 cycles under 2 N constant load in ball-disc type tribometer. The wear rates of materials were determined as a result of optical profilometer examinations of the wear tracks. The wear mechanisms were characterized by SEM images of the wear tracks. In the ZrN coating, it was observed that the ZrN (111) phase with a NaCl type cubic crystal lattice was dominant. It was observed that the hardness value of the ZrN coating was approximately 1882 HV0.01 and the hardness value of the substrate material was 448 HV0.01. In this case, it has been determined that the hardness value of the ZrN coated material is approximately 300% higher than the substrate material. It was observed that the wear performance of ZrN coatings was higher than the untreated material in both cycles. While the dominant wear mechanism in the untreated material was plastic deformation and adhesive wear, the flaking-induced peeling was the dominant wear mechanism in the ZrN coating.

References

  • Javari, A., Dehgani, K., Bahaaddini, K., Hataie, A. B., Experimental comparison of abrasive and erosive wear characteristics of four wear-resistant steels, Wear. 416-417: 14-26, (2018).
  • Yang, Y., Huang, L., Shi, Y., Adhesion suppresses atomic wear in single-asperity sliding, Wear. 352-353: 31-41, (2016).
  • Hacısalihoglu, I., Kaya, G., Ergüder, O. T., Mandev, E., Manay, E., Yıldız, F. Tribological and thermal properties of plasma nitrided Ti45Nb alloy, Surf. and Inter. 22: 100893, (2021).
  • Fernandez-Valdes, D., Meneses-Amador, A., Lopez-Lievano, A., Ocampa-Ramirez, A., Sliding wear analysis in borided AISI 316L steels, Mater. Lett. 285: 129138, (2021).
  • Azim, S., Gangopadhyay, S., Mahapatra, S. S., Mittal, R. K., Singh, R. K., Role of PVD coating on wear and surface integrity during environment-friendly micro-drilling of Ni-based superalloy, J. Cleaner Prod. 272: 122741, (2020).
  • Chowdhury, M. S. I., Bose, B., Yamamoto, K., Shuster, L. S., Paiva, J., Fox-Rabinovich, G. S., Veldhuis, S. C., Wear performance investigation of PVD coated and uncoated carbide tools during high-speed machining of TiAl6V4 aerospace alloy, Wear. 446-447: 203168, (2020).
  • Sert, Y., Küçükömeroğlu, T., Ghahramanzadeh Asl, H. The Effect of Al and Ti Transition Metals on the Wear Resistance of Ceramic Based CrN Coatings; Investigation under Ambient Air and Vacuum Conditions, Proc. Inst. Mech. Eng., Part L: J. Mater: Design and App. 236: 455-472, (2022).
  • Movassagh-Alanagh, F., Mahdavi, M., Improving wear and corrosion resistance of AISI 304 stainless steel by a multilayered nanocomposite Ti/TiN/TiSiN coating, Surf. and Inter. 18: 100428, (2020).
  • Chou, W.-J., Yu, G.-P., Huang, J.-H., Corrosion behavior of TiN-coated 304 stainless steel, Corr. Sci. 43: 2023-2035, (2001).
  • Kumar, S., Maity, S. R., Patnaik, L., Effect of heat treatment and TiN coating on AISI O1 cold work tool steel, Mater. Today: Proc. 26: 685-688, (2020).
  • Gonzalez-Carmona, J., Trivino, J. D., Gomez-Ovalle, A., Ortega, C., Alvarado-Orozco, J. M., Sanchez-Sthepa, H., Avila, A., Wear mechanisms identification using Kelvin probe force microscopy in TiN, ZrN and TiN/ZrN hard ceramic multilayers coatings, Ceram. Int. 46: 24592-24604, (2020).
  • Jianxin, D., Jianhua, L., Jinlong, Z., Wenlong, S., Ming, N., Friction and wear behaviors of the PVD ZrN coated carbide in sliding wear tests and in machining processes, Wear. 264: 298-307, (2008).
  • Jianxin, D., Jianhua, L., Jinlong, Z., Wenlong, S., Wear mechanisms of PVD ZrN coated tools in machining, Int. J. of Ref. Metals and Hard Mater. 264: 164-172, (2008).
  • Kuznetsova, T., Lapitskaya, V., Khabarava, A., Chiznik, S., Warcholinski, B., Gilewicz, A., The influence of nitrogen on the morphology of ZrN coatings deposited by magnetron sputtering, Appl. Surf. Sci. 522: 146508, (2020).
  • Feng, Y.-P., Zhang, L., Ke, R.-X., Wan, Q.-L., Wang, Z., Lu, Z.-H., Thermal stability and oxidation behavior of AlTiN, AlCrN and AlCrSiWN coatings, Int. J. Ref. Metals Hard Mater. 43: 241-249, (2014).
  • Maksakova, O. V., Simoes, S., Pogrebnjak, A. D., Bondar, O. V., Kravchenko, O., Koltunowicz, T. N., Shaimardanov, Zh. K., Multilayered ZrN/CrN coatings with enhanced thermal and mechanical properties, J. Alloys and Comp. vol. 776: 679-690, (2019).
There are 16 citations in total.

Details

Primary Language Turkish
Subjects Engineering
Journal Section Articles
Authors

Yaşar Sert 0000-0001-7742-0335

Hüccet Kahramanzade 0000-0002-9078-1933

Tevfik Küçükömeroğlu 0000-0002-4392-9966

Early Pub Date April 11, 2022
Publication Date May 31, 2022
Published in Issue Year 2022 Issue: 36

Cite

APA Sert, Y., Kahramanzade, H., & Küçükömeroğlu, T. (2022). ZrN İnce Film Kaplamasının 1.2379 Soğuk İş Takım Çeliğindeki Aşınma Özelliğine Etkisinin İncelenmesi. Avrupa Bilim Ve Teknoloji Dergisi(36), 1-5. https://doi.org/10.31590/ejosat.1091504