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Enlarged of Nano-Dimensional Vanilla Thin Films and Surface Plasma Resonance Sensor Performance of these Films

Year 2019, , 543 - 552, 31.08.2019
https://doi.org/10.18185/erzifbed.446029

Abstract

In order to determine the thin film properties of vanilla, nano-sized
thin films were obtained on a suitable substrate using the spin coating method.
UV-visible absorption spectroscopy and
surface plasma resonance method were used for the characterization of the deposited thin film.
Characterization results obtained using these techniques indicated that the
vanillin molecules are suitable to transfer onto a gold coated glass or quartz
glass substrates. Gas sensing
properties and thickness of these thin films were elucidated, using the surface
plasmon resonance (SPR) method. Firstly, thicknesses of the vanillin spun films
were obtained for different spinning speed and then, the gas sensing properties
were examined towards vapours of three volatile organic compounds (VOC’s)
(methanol, chloroform, benzene). Compared the results
it was determined that, vanilla thin films are selective for the benzene vapour, with rapid
response and recovery times. According to these data it was found that, vanilla
thin films obtained by spin coating method, could be used for the detection of
benzene vapor.

References

  • Alexandra, L., Galatios, M., Nychas, G.E., Panagou, E.Z. (2018). “Growth of Listeria Monocytogenes in Pasteurized Vanilla Cream Pudding as Affected by Storage Temperature and the Presence of Cinnamon extract”, Food Research International, 106, 1114-1122.
  • Anonim (2018). file:///C:/Users/Pc/Downloads/getpdf-Vanilla-Extract-025109.pdf
  • Ashwell, G.J., Skjonnemand, K., Roberts, M.P.S., Allen, D.W., Li , X., Sworakowski, J., Chyla, A., Bienkowski, M. (1999). “ Surface Plasmon Resonance and Nonlinear Optical Studies of Langmuir–Blodgett films of a Betaine Dye”, Physicochemical and Engineering Asp., 155(1), 43-46.
  • Baqueiro-Pena, I., Guerrero-Beltrán, J.Á. (2017). “Vanilla (Vanilla planifolia andr.), Its Residues and Other Industrial by-products for Recovering High Value Flavor Molecules”, Journal of Applied Research on Medicinal and Aromatic Plants, 6, 1–9.
  • Capan, R., Göktas¸ H., Özbek, Z., Sen, S., Özel, M.E., Davis, F. (2015). “Langmuir–Blodgett Thin Film for Chloroform Detection”, Applied Surface Science, 350, 129–134.
  • Capan, R., Ozbek, Z., Goktas, H., Sen,S.;Ince, F.G., Ozel, M.E., Stanciu,G.A., Davis, F., (2010). “Characterization of Langmuir-Blodgett Films of a Calix [8] arene and Sensing Properties towards Volatile Organic Vapors”, Sensors and Actuators B Chemical, 148(2), 358-365.
  • Colombelli, A., Manera, M.G., Borovkov, V., Giancane, G., Valli, L., Rella, R. (2017). “Enhanced Sensing Properties of Cobalt bis-porphyrin Derivative Thin Films by a Magneto-plasmonic-opto-chemical Sensor”, Sensorsand Actuators B, 246, 1039–1048.
  • Çapan, İ., Tarımcı, Ç., Erdoğan, M., Hassan, A.K., (2009). “Characterisation and Vapour Sensing Properties of Spin Coated Thin Films of Anthracene Labelled PMMA Polymer”, Materials Science and Engineering C, 29(4), 1114-1117.
  • Evyapan, M., Kadem, B., Basova, T.V., Yushina, I.V.; Hassan, A.K., (2016). “ Study of the Sensor Response of Spun Metal Phthalocyanine Films to Volatile Organic Vapors Using Surface Plasmon Resonance”, Sensorsand Actuators B, 36, 605–613.
  • Faull, J.D., Gupta,V.K. (2003). “Chemical Selectivity of self-assembled Monolayers of Calix[4]resorcinarene”, Thin Solid Films, 440(1-2),129-137.Gras, A., Parada, M., Rigata, M., Vallèsa, J. (2018). “Folk Medicinal Plant Mixtures: Establishing a Protocol Forfurther Studies”, Journal of Ethnopharmacology, 214, 244-273.
  • Hassan, A.K., Basova, T., Tuncel, S., Yuksel, F., Gürek, A.G., Ahsen,V., (2011). “Phthalocyanine Films as Active Layers of Optical Sensors for Pentachlorophenol and simazine Detection”, Procedia Engineering, 25, 272 – 275.
  • Hassan, A.K., Ray, A.K.; Nabok, A.-V., Davis, F. (2001). “Spun Films of Novel Calix[4]resorcinarene Derivatives for Benzene Vapour Sensing”, Sensors and Actuators B, 77(3), 638-641.
  • Nabok, A.V., Hassan, A.K., Ray, A.K. (2000). “Condensation of Organic Vapours within Nanoporous Calixarene Thin Films”, J. Mater. Chem., 10 (1), 189-194.
  • Oliveira, C.B.S., Meurer, Y.S.R., Oliveira, M.G., Medeiros, W.M.T.Q., Silva, F.O.N., Brito, A.C.F., Pontes, D.L. and Andrade-Neto, V.F. (2014). “Comparative Study on the Antioxidant and Anti-Toxoplasma Activities of Vanillin and Its Resorcinarene Derivative”, Molecules, 19 (5), 5898-5912.
  • Pockrand, I., (1978). “Surface plasma-oscillations at silver surfaces with thin transparent and absorbing coatings”, Surf. Sci. 72 (3) 577-588. Su, L., Guo, X., Han, S. (2014). “Preparationan Devaluation of Vnillin Molecularly Imprinted Polymer Microspheres by Reversible Addition–fragmentation Chain Transfer Precipitation Polymerization”, Anal. Methods, 6(8) 2512-2517.
  • Şen, S., Çapan, R., Özel, M.E., Hassan, A.K., Turhan, O., Namlı, H. (2011). “Thin Film Characterization of Novel Phthalimide Materials”, Optoelectronics and Advanced Materials – Rapid Communications, 5 (11) 1243 – 1247.
  • Tiwari, S.S., Srivastava, A., Srivastava, S., Rawat, A.K.S. (2012). “Isolation and Quantification of Vanillin Through Flash & Hptlc Chromatographic Techniques from Decalepıs Hamıltonii Wight and Arn Root and Their Antioxidant Studies”, Journal of Liquid Chromatography & Related Technologies, 35, :2396–2407.
  • Wilde, J.N. Nagel, J., Petty, M.C. (1998). “Optical Sensing of Aromatic Hydrocarbons Using Langmuir-Blodgett Films of a Schiff Base Co-ordination Polymer”, Thin Solid Films, 327(1), 726-729.
  • Yang, Z., Peng, Z., Li, J., Li, S., Kong, L., Li, P., Wang, Q. (2014). “Development and Evaluation of Novel Flavour Microcapsules Containing Vanilla Oil Using Complex Coacervation Approach”, Food Chemistry, 145 272–277.
  • Gras, A., Parada, M., Rigata, M., Vallèsa, J. (2018). “Folk Medicinal Plant Mixtures: Establishing a Protocol Forfurther Studies”, Journal of Ethnopharmacology, 214, 244-273.
  • Su, L., Guo, X., Han, S. (2014). “Preparationan Devaluation of Vnillin Molecularly Imprinted Polymer Microspheres by Reversible Addition–fragmentation Chain Transfer Precipitation Polymerization”, Anal. Methods, 6(8) 2512-2517.

Nano-Boyutlu Vanilya İnce Filmlerin Büyütülmesi ve Yüzey Plazma Rezonansı Sensör Performansı

Year 2019, , 543 - 552, 31.08.2019
https://doi.org/10.18185/erzifbed.446029

Abstract

Vanilya ince film özelliklerinin belirlenmesi için, uygun bir alt tabaka
üzerinde, spin kaplama yöntemi kullanılarak nano boyutta ince filmler büyütülmüştür.
Bu ince filmin karakterizasyonu için UV-görünür soğurma spektroskopisi ve yüzey
plazma rezonansı kullanılmıştır. Bu teknikler sayesinde elde edilen
karakterizasyon sonuçları, vanilya moleküllerinin altın kaplı cam veya kuvars
cam alttaşlar üzerine aktarılmaya elverişli olduğunu göstermektedir. Spin kaplama
yöntemi ile büyütülen vanilya ince
filmlerin gaz algılama özellikleri ve
kalınlığı, yüzey plazma rezonansı (SPR) yöntemi kullanılarak incelenmiştir.
Öncelikle farklı dönüş hızlarında üretilen ince filmlerin kalınlıkları elde
edilmiş ve daha sonra, üç farklı uçucu organik bileşiğin (UOB) (metanol,
kloroform, benzen) buharına karşı gaz algılama özellikleri incelenmiştir.
Sonuçlar karşılaştırıldığında vanilya ince filmlerinin benzen buharı için
seçici olduğu, bu buhara karşı olan tepkisinin ve filmlere hava verildiği
zamanki geri dönüşümünün hızlı olduğu tespit edilmiştir. Bu verilere göre spin
kaplama yöntemiyle büyütülen vanilya ince filmlerin, benzen buharının tespiti
için kullanılabileceği bulunmuştur.

References

  • Alexandra, L., Galatios, M., Nychas, G.E., Panagou, E.Z. (2018). “Growth of Listeria Monocytogenes in Pasteurized Vanilla Cream Pudding as Affected by Storage Temperature and the Presence of Cinnamon extract”, Food Research International, 106, 1114-1122.
  • Anonim (2018). file:///C:/Users/Pc/Downloads/getpdf-Vanilla-Extract-025109.pdf
  • Ashwell, G.J., Skjonnemand, K., Roberts, M.P.S., Allen, D.W., Li , X., Sworakowski, J., Chyla, A., Bienkowski, M. (1999). “ Surface Plasmon Resonance and Nonlinear Optical Studies of Langmuir–Blodgett films of a Betaine Dye”, Physicochemical and Engineering Asp., 155(1), 43-46.
  • Baqueiro-Pena, I., Guerrero-Beltrán, J.Á. (2017). “Vanilla (Vanilla planifolia andr.), Its Residues and Other Industrial by-products for Recovering High Value Flavor Molecules”, Journal of Applied Research on Medicinal and Aromatic Plants, 6, 1–9.
  • Capan, R., Göktas¸ H., Özbek, Z., Sen, S., Özel, M.E., Davis, F. (2015). “Langmuir–Blodgett Thin Film for Chloroform Detection”, Applied Surface Science, 350, 129–134.
  • Capan, R., Ozbek, Z., Goktas, H., Sen,S.;Ince, F.G., Ozel, M.E., Stanciu,G.A., Davis, F., (2010). “Characterization of Langmuir-Blodgett Films of a Calix [8] arene and Sensing Properties towards Volatile Organic Vapors”, Sensors and Actuators B Chemical, 148(2), 358-365.
  • Colombelli, A., Manera, M.G., Borovkov, V., Giancane, G., Valli, L., Rella, R. (2017). “Enhanced Sensing Properties of Cobalt bis-porphyrin Derivative Thin Films by a Magneto-plasmonic-opto-chemical Sensor”, Sensorsand Actuators B, 246, 1039–1048.
  • Çapan, İ., Tarımcı, Ç., Erdoğan, M., Hassan, A.K., (2009). “Characterisation and Vapour Sensing Properties of Spin Coated Thin Films of Anthracene Labelled PMMA Polymer”, Materials Science and Engineering C, 29(4), 1114-1117.
  • Evyapan, M., Kadem, B., Basova, T.V., Yushina, I.V.; Hassan, A.K., (2016). “ Study of the Sensor Response of Spun Metal Phthalocyanine Films to Volatile Organic Vapors Using Surface Plasmon Resonance”, Sensorsand Actuators B, 36, 605–613.
  • Faull, J.D., Gupta,V.K. (2003). “Chemical Selectivity of self-assembled Monolayers of Calix[4]resorcinarene”, Thin Solid Films, 440(1-2),129-137.Gras, A., Parada, M., Rigata, M., Vallèsa, J. (2018). “Folk Medicinal Plant Mixtures: Establishing a Protocol Forfurther Studies”, Journal of Ethnopharmacology, 214, 244-273.
  • Hassan, A.K., Basova, T., Tuncel, S., Yuksel, F., Gürek, A.G., Ahsen,V., (2011). “Phthalocyanine Films as Active Layers of Optical Sensors for Pentachlorophenol and simazine Detection”, Procedia Engineering, 25, 272 – 275.
  • Hassan, A.K., Ray, A.K.; Nabok, A.-V., Davis, F. (2001). “Spun Films of Novel Calix[4]resorcinarene Derivatives for Benzene Vapour Sensing”, Sensors and Actuators B, 77(3), 638-641.
  • Nabok, A.V., Hassan, A.K., Ray, A.K. (2000). “Condensation of Organic Vapours within Nanoporous Calixarene Thin Films”, J. Mater. Chem., 10 (1), 189-194.
  • Oliveira, C.B.S., Meurer, Y.S.R., Oliveira, M.G., Medeiros, W.M.T.Q., Silva, F.O.N., Brito, A.C.F., Pontes, D.L. and Andrade-Neto, V.F. (2014). “Comparative Study on the Antioxidant and Anti-Toxoplasma Activities of Vanillin and Its Resorcinarene Derivative”, Molecules, 19 (5), 5898-5912.
  • Pockrand, I., (1978). “Surface plasma-oscillations at silver surfaces with thin transparent and absorbing coatings”, Surf. Sci. 72 (3) 577-588. Su, L., Guo, X., Han, S. (2014). “Preparationan Devaluation of Vnillin Molecularly Imprinted Polymer Microspheres by Reversible Addition–fragmentation Chain Transfer Precipitation Polymerization”, Anal. Methods, 6(8) 2512-2517.
  • Şen, S., Çapan, R., Özel, M.E., Hassan, A.K., Turhan, O., Namlı, H. (2011). “Thin Film Characterization of Novel Phthalimide Materials”, Optoelectronics and Advanced Materials – Rapid Communications, 5 (11) 1243 – 1247.
  • Tiwari, S.S., Srivastava, A., Srivastava, S., Rawat, A.K.S. (2012). “Isolation and Quantification of Vanillin Through Flash & Hptlc Chromatographic Techniques from Decalepıs Hamıltonii Wight and Arn Root and Their Antioxidant Studies”, Journal of Liquid Chromatography & Related Technologies, 35, :2396–2407.
  • Wilde, J.N. Nagel, J., Petty, M.C. (1998). “Optical Sensing of Aromatic Hydrocarbons Using Langmuir-Blodgett Films of a Schiff Base Co-ordination Polymer”, Thin Solid Films, 327(1), 726-729.
  • Yang, Z., Peng, Z., Li, J., Li, S., Kong, L., Li, P., Wang, Q. (2014). “Development and Evaluation of Novel Flavour Microcapsules Containing Vanilla Oil Using Complex Coacervation Approach”, Food Chemistry, 145 272–277.
  • Gras, A., Parada, M., Rigata, M., Vallèsa, J. (2018). “Folk Medicinal Plant Mixtures: Establishing a Protocol Forfurther Studies”, Journal of Ethnopharmacology, 214, 244-273.
  • Su, L., Guo, X., Han, S. (2014). “Preparationan Devaluation of Vnillin Molecularly Imprinted Polymer Microspheres by Reversible Addition–fragmentation Chain Transfer Precipitation Polymerization”, Anal. Methods, 6(8) 2512-2517.
There are 21 citations in total.

Details

Primary Language Turkish
Subjects Engineering
Journal Section Makaleler
Authors

Sibel Şen

Publication Date August 31, 2019
Published in Issue Year 2019

Cite

APA Şen, S. (2019). Nano-Boyutlu Vanilya İnce Filmlerin Büyütülmesi ve Yüzey Plazma Rezonansı Sensör Performansı. Erzincan University Journal of Science and Technology, 12(2), 543-552. https://doi.org/10.18185/erzifbed.446029