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Mikro Ark Oksidasyon (MAO) Yöntemi ile Grade-2 Titanyum Alaşımı Üzerine Büyütülmüş Katkılı Oksit Kaplamaların Anti-Bakteriyel Duyarlılıklarının İncelenmesi

Year 2017, Volume: 10 Issue: 2, 287 - 295, 22.12.2017

Abstract

Bu çalışma; biyomalzeme olarak kullanılabilen Cp-Ti (Grade-2) titanyum
alaşımının yüzey özelliklerinin MAO yöntemiyle iyileştirilmesine ve anti
bakteriyel duyarlılık kazandırılması üzerine odaklanmıştır. Gümüşün anti
bakteriyel etkisinin MAO yöntemi ile kaplanmış Cp-Ti (Grade-2) titanyum taban
malzemelere kazandırılması amaçlanmaktadır. Bu amaçla kaplamaların yapısal
özellikleri SEM ve XRD cihazları kullanılarak analiz edilmiştir. Anti
bakteriyel duyarlılıklarının ve bakteri adezyonunun incelenmesi için in vitro
anti-bakteriyel etkinlik deneylerinde bakteriler kristal viyole kullanılarak
işaretlenmiştir. Kaplamaların; adezyonu yüksek olan Staphylococous Aureus
(S.aureus-ATCC 29213) bakterisine karşı duyarlılıkları araştırılmıştır.
Çalışmada, gümüş içeren kaplamaların gümüş içermeyen kaplamalara göre
bakteriyel duyarlılıklarının zayıf olduğu ve kaplama yapılmayan örneklerin ise
bakteriye karşı oldukça duyarlı olduğu tespit edilmiştir.

References

  • Bayati M.R., F. Golestani-Fard, A.Z. Moshfegh, (2010). The effect of growth parameters on photo-catalytic performance of the MAO-synthesized TiO2 nano-porous layers, Materials Chemistry and Physics, 120, 2–3, 582-589.
  • Cao H., Cui T., Jin G., Liu X., Cellular responses to titanium successively treated by magnesium and silver PIII&D, Surf. Coat. Technol, 256, 9-14, 2014.
  • Godoy-Gallardo M., Rodriguez-Hernandez A.G., Delgado L.M., Manero J.M., Gil F.J., Rodriguez D. (2015). Silver deposition on titanium surface by electrochemical anodizing process reduces bacterial adhesion of Streptococcus sanguinis and Lactobacillus salivarius, Clinical Oral Implants Research, 26 (10), 1170-1179.
  • Cao H., Liu X., Meng F., Chu P.K. (2011). Biological actions of silver nanoparticles embedded in titanium controlled by micro-galvanic effects, Biomaterials, 32 (3), 693- 705.
  • Cao H., Qiao Y., Liu X., Lu T., Cui T., Meng F., Chu P.K. (2013). Electron storage mediated dark antibacterial action of bound silver nanoparticles: Smaller is not always better, Acta Biomater., 9 (2), 5100-5110.
  • Demirci E.E. (2014). Manyetik sıçratma (CFUBMS) ve mikro ark oksidasyon (MAO) teknikleri ile Ti6Al4V alaşımının dubleks yüzey modifikasyonu. Yayınlanmamış Doktora Tezi, Atatürk Üniversitesi. Fen Bilimleri Enstitüsü, Erzurum.
  • Gençer G. M., Karadeniz S., Lambrecht F.Y., Havıtçıoğlu H., Özkal S., Baskın H. (2017). Plazma daldırma iyon implantasyonu ve biriktirme (PIII&D) prosesi gerilimlerinin azot plazmasında ortopedik implant malzemesi Ti6Al4V yüzeyinde oluşturulan Ag kaplamalarının morfolojilerine, faz oluşumlarına ve E. coli adezyonuna etkileri. Journal of the Faculty of Engineering and Architecture of Gazi University, 32:1, 231-241
  • Hanawa T. (1999). In vivo metallic biomaterials and surface modification, Materials Science and Engineering, A267, 260-266.
  • Krishna, R. L., Somaraju K.R.C. (2003). The Tribological Performance Of Ultra-Hard Ceramic Composite Coatings Obtained Through Microarc Oxidation, Surface and Coatings Technology, 163–164 484–490
  • Matykina, E., Berkani, A., Skeldon, P., Thompson, G.E., (2007). Real-time imaging of coating growth during plasma electrolytic oxidation of titanium, Electrochimica Acta, 53, 4, 1987-1994,
  • Niinomi M. (2003). Titanium Alloys for Medical and Dental Applications, Medical Device Materials,Procceedings of the Materials & Processes for Medical Device Conference, Ed. S.Shrivastava, Anaheim CA, pp. 417-422.
  • Parfenov, E.V., Yerokhin, A.L., Matthews, A., (2007). Frequency response studies for the plasma electrolytic oxidation process, Surface and Coatings Technology, 201, 21, 8661–8670.
  • Pilliar R.M. (2003). Metals and Orthopaedic Implants-Past Successes, Present Limitations,Future Challenges, Medical Device Materials, Procceedings of the Materials & Processes for Medical Device Conference, Ed. S. Shrivastava, Anaheim CA, pp. 8-22.
  • Tikici S. (2014). PEO ve EPD yöntemleri ile CP-titanyum üzerine TiO2/HA hibrit kaplamasının büyütülmesi ve biyoaktivite karakterizasyonu. Yayınlanmamış Yüksek Lisans Tezi, Atatürk Üniversitesi. Fen Bilimleri Enstitüsü, Erzurum.
  • Wang C. (2006). Growth process and wear resistance for ceramic coatings formed on Al-Cu-Mg alloy by micro-arc oxidation, Surface Science, 1-5.
  • Zhang Z., Zhang Y., Chang L., Jiang Z., Yao, Z., Liu X., (2012). Effects of Frequency on Growth Process of Plasma Electrolytic Oxidation Coating, Materials Chemistry and Physics, 132, 909-915.
  • Yerokhin, A.L., Leyland, A., Matthews, A. (2002). Kinetcis Aspects of Aluminium Titanete Layer Formation on Titanium Alloys By Plasma Electrolytic Oxidation, Applied Surface Science, 200, 172-184.
  • Yerokhin, A.L., Nie, X., Leyland, A., Matthews, A., Dowey S.J. (1999). Plasma electrolysis for surface engineering, Surface and Coatings Technology, 122, 73.
  • Wang, Y., Lei, T., Guo L., Jiang B. (2006). Fretting Wear Behaviour of Micro-Arc Oxidation Coatings Formed on Titanium Alloy Against Steel in Unlubrication and Oil Lubrication, Applied Surface Science, 252, 8113–8120.
  • Wang, Y.M., Jia, D.C., Guo, L.X., Lei, T.Q., Jiang, B.L. (2005). Effect of Discharge Pulsating on Microarc Oxidation Coatings Formed on Ti6Al4V Alloy, Materials Chemistry and Physics, 90, 128–133.
  • Wang, Y.M., Jiang, B.L., Guo, L.X., Lei T.C. (2004). Controlled Synthesis of Micro arc Oxidation Coating on Ti6Al4V Alloy and Its Antifriction Properties, Materials Science and Technology, 20, 12, 1590-1594.
  • Yao, Z., Jiang, Y., Jia, F., Jiang, Z., Wang, F. (2008). Growth Characteristics of Plasma Electrolytic Oxidation Ceramic Coatings on Ti-6Al-4V Alloy Applied Surface Science, 254, 13, 4084-4091.
  • Zhang, Z., Zhang Y., Chang L., Jiang Z., Yao, Z., Liu X., (2012). Effects of Frequency on Growth Process of Plasma Electrolytic Oxidation Coating, Materials Chemistry and Physics, 132, 909-915.

The Investigation of Anti-Bacterial Susceptibilities of doped Oxide Coatings on Grade-2 Titanium Alloys Coated By Micro Arc Oksidasiyon (MAO) Process

Year 2017, Volume: 10 Issue: 2, 287 - 295, 22.12.2017

Abstract



This work, Focuses on improving the surface properties of the Cp-Ti
(Grade-2) titanium alloy, which can be used as biomaterial, with the MAO method
and imparting anti-bacterial susceptibility. The antibacterial effect of silver
is intended to be imparted to the Cp-Ti (Grade-2) titanium base materials
coated with the MAO method. For this purpose, the structural properties of the
coatings were analyzed using SEM, XRD and EDS instruments. In vitro
antibacterial efficacy assays for bacterial susceptibility testing and
bacterial adhesion were performed using bacterial crystal violet markers. The
susceptibility of the coatings against to
Staphylococous aureus (S.aureus-ATCC
29213)
bacteria that has high adhesion was
investigated. In the study, it was determined that the silver-containing
coatings had a weaker bacterial susceptibility than the silver-free coatings
and that the uncoated samples were more sensitive to bacterial contamination.



References

  • Bayati M.R., F. Golestani-Fard, A.Z. Moshfegh, (2010). The effect of growth parameters on photo-catalytic performance of the MAO-synthesized TiO2 nano-porous layers, Materials Chemistry and Physics, 120, 2–3, 582-589.
  • Cao H., Cui T., Jin G., Liu X., Cellular responses to titanium successively treated by magnesium and silver PIII&D, Surf. Coat. Technol, 256, 9-14, 2014.
  • Godoy-Gallardo M., Rodriguez-Hernandez A.G., Delgado L.M., Manero J.M., Gil F.J., Rodriguez D. (2015). Silver deposition on titanium surface by electrochemical anodizing process reduces bacterial adhesion of Streptococcus sanguinis and Lactobacillus salivarius, Clinical Oral Implants Research, 26 (10), 1170-1179.
  • Cao H., Liu X., Meng F., Chu P.K. (2011). Biological actions of silver nanoparticles embedded in titanium controlled by micro-galvanic effects, Biomaterials, 32 (3), 693- 705.
  • Cao H., Qiao Y., Liu X., Lu T., Cui T., Meng F., Chu P.K. (2013). Electron storage mediated dark antibacterial action of bound silver nanoparticles: Smaller is not always better, Acta Biomater., 9 (2), 5100-5110.
  • Demirci E.E. (2014). Manyetik sıçratma (CFUBMS) ve mikro ark oksidasyon (MAO) teknikleri ile Ti6Al4V alaşımının dubleks yüzey modifikasyonu. Yayınlanmamış Doktora Tezi, Atatürk Üniversitesi. Fen Bilimleri Enstitüsü, Erzurum.
  • Gençer G. M., Karadeniz S., Lambrecht F.Y., Havıtçıoğlu H., Özkal S., Baskın H. (2017). Plazma daldırma iyon implantasyonu ve biriktirme (PIII&D) prosesi gerilimlerinin azot plazmasında ortopedik implant malzemesi Ti6Al4V yüzeyinde oluşturulan Ag kaplamalarının morfolojilerine, faz oluşumlarına ve E. coli adezyonuna etkileri. Journal of the Faculty of Engineering and Architecture of Gazi University, 32:1, 231-241
  • Hanawa T. (1999). In vivo metallic biomaterials and surface modification, Materials Science and Engineering, A267, 260-266.
  • Krishna, R. L., Somaraju K.R.C. (2003). The Tribological Performance Of Ultra-Hard Ceramic Composite Coatings Obtained Through Microarc Oxidation, Surface and Coatings Technology, 163–164 484–490
  • Matykina, E., Berkani, A., Skeldon, P., Thompson, G.E., (2007). Real-time imaging of coating growth during plasma electrolytic oxidation of titanium, Electrochimica Acta, 53, 4, 1987-1994,
  • Niinomi M. (2003). Titanium Alloys for Medical and Dental Applications, Medical Device Materials,Procceedings of the Materials & Processes for Medical Device Conference, Ed. S.Shrivastava, Anaheim CA, pp. 417-422.
  • Parfenov, E.V., Yerokhin, A.L., Matthews, A., (2007). Frequency response studies for the plasma electrolytic oxidation process, Surface and Coatings Technology, 201, 21, 8661–8670.
  • Pilliar R.M. (2003). Metals and Orthopaedic Implants-Past Successes, Present Limitations,Future Challenges, Medical Device Materials, Procceedings of the Materials & Processes for Medical Device Conference, Ed. S. Shrivastava, Anaheim CA, pp. 8-22.
  • Tikici S. (2014). PEO ve EPD yöntemleri ile CP-titanyum üzerine TiO2/HA hibrit kaplamasının büyütülmesi ve biyoaktivite karakterizasyonu. Yayınlanmamış Yüksek Lisans Tezi, Atatürk Üniversitesi. Fen Bilimleri Enstitüsü, Erzurum.
  • Wang C. (2006). Growth process and wear resistance for ceramic coatings formed on Al-Cu-Mg alloy by micro-arc oxidation, Surface Science, 1-5.
  • Zhang Z., Zhang Y., Chang L., Jiang Z., Yao, Z., Liu X., (2012). Effects of Frequency on Growth Process of Plasma Electrolytic Oxidation Coating, Materials Chemistry and Physics, 132, 909-915.
  • Yerokhin, A.L., Leyland, A., Matthews, A. (2002). Kinetcis Aspects of Aluminium Titanete Layer Formation on Titanium Alloys By Plasma Electrolytic Oxidation, Applied Surface Science, 200, 172-184.
  • Yerokhin, A.L., Nie, X., Leyland, A., Matthews, A., Dowey S.J. (1999). Plasma electrolysis for surface engineering, Surface and Coatings Technology, 122, 73.
  • Wang, Y., Lei, T., Guo L., Jiang B. (2006). Fretting Wear Behaviour of Micro-Arc Oxidation Coatings Formed on Titanium Alloy Against Steel in Unlubrication and Oil Lubrication, Applied Surface Science, 252, 8113–8120.
  • Wang, Y.M., Jia, D.C., Guo, L.X., Lei, T.Q., Jiang, B.L. (2005). Effect of Discharge Pulsating on Microarc Oxidation Coatings Formed on Ti6Al4V Alloy, Materials Chemistry and Physics, 90, 128–133.
  • Wang, Y.M., Jiang, B.L., Guo, L.X., Lei T.C. (2004). Controlled Synthesis of Micro arc Oxidation Coating on Ti6Al4V Alloy and Its Antifriction Properties, Materials Science and Technology, 20, 12, 1590-1594.
  • Yao, Z., Jiang, Y., Jia, F., Jiang, Z., Wang, F. (2008). Growth Characteristics of Plasma Electrolytic Oxidation Ceramic Coatings on Ti-6Al-4V Alloy Applied Surface Science, 254, 13, 4084-4091.
  • Zhang, Z., Zhang Y., Chang L., Jiang Z., Yao, Z., Liu X., (2012). Effects of Frequency on Growth Process of Plasma Electrolytic Oxidation Coating, Materials Chemistry and Physics, 132, 909-915.
There are 23 citations in total.

Details

Subjects Engineering
Journal Section Makaleler
Authors

Ebru Emine ŞÜKÜROĞLU 0000-0001-8638-5471

Publication Date December 22, 2017
Published in Issue Year 2017 Volume: 10 Issue: 2

Cite

APA ŞÜKÜROĞLU, E. E. (2017). The Investigation of Anti-Bacterial Susceptibilities of doped Oxide Coatings on Grade-2 Titanium Alloys Coated By Micro Arc Oksidasiyon (MAO) Process. Erzincan University Journal of Science and Technology, 10(2), 287-295. https://doi.org/10.18185/erzifbed.323484