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SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI

Year 2011, Volume: 26 Issue: 4, 0 - , 20.02.2013

Abstract

Bu çalışmada, saf zirkonyumun yüzeyi mikroark oksidasyon yöntemi ile sabit elektriksel şartlarda ve aynıelektrolit kompozisyonunda 5, 15, 30, 45, 60, 90 ve 120 dakika süreyle kaplanmıştır. Zr üzerinde oluşturulankaplamanın faz kompozisyonu, mikroyapısı, yüzey morfolojisi ve mikrosertliği; X-ray kırınımı, taramalıelektron mikroskobu, profilometre ve mikrosertlik ölçümü ile karakterize edilmiştir. Kaplama tabakası gözenekliyapıda olup, önemli miktarda mikro çatlaklar içermektedir. Kaplamanın kristal yapıdaki monoklinik (m-ZrO2) vetetragonal (t-ZrO2) zirkonyum oksit fazlarından oluştuğu ve kaplama süresinin oluşan faz içeriğini etkilemediğitespit edilmiştir. Kaplama içerisinde zirkonyum ve oksijenin yanında silisyumun varlığı da tespit edilmiştir.Kaplama süresindeki artışla beraber kaplama kalınlığı doğrusal şekilde 5 μm’den 135 μm’ye yükselmiştir. Yüzeypürüzlülüğü kaplama süresi ile artarak, 0,5 μm’den 6,4 μm’ye yükselmiştir. Altlık malzeme zirkonyumun 200HV sertliğine karşılık, oksit kaplama tabakası sertliği yaklaşık 600 HV olarak ölçülmüştür ve mikrosertlikdeğerinde kaplama süresine bağlı sistematik bir değişim görülmemiştir.

References

  • Xue, W., Deng, Z., H. Chen, Ma,, Zhang R. T.,
  • Microstructure and phase composition of microarc
  • oxidation coatings formed on Ti-6Al-4V alloy in
  • aluminate solution, Surface Eng, 17, 323-326,
  • -
  • Yerokhin, A.L., Nie, X., Leyland, A. Matthews, A.,
  • Dowey, S.J., Plasma electrolysis for surface
  • engineering, Surf Coat Tech, 122, 73-93, 1999.
  • G.L. Yang, X.Y. Lu, Y.Z. Bai, Z.S. Jin,
  • Characterization of microarc oxidation discharge
  • process for depositing ceramic coating, Chinese
  • Phys Lett, 18, 1141-1143, 2001.
  • Yerokhin, A.L., Snizhko, L.O., Gurevina, N.L.,
  • Leyland, A., Pilkington, A., Matthews, A., Spatial
  • characteristics of discharge phenomena in plasma
  • electrolytic oxidation of aluminium alloy, Surf
  • Coat Tech, 177, 779-783, 2004.
  • Wu, X.H., Qin, W., Guo, Y., Xie, Z.Y., Selflubricative
  • coating grown by micro-plasma
  • oxidation on aluminum alloys in the solution of
  • aluminate-graphite, Appl Surf Sci, 254, 6395-
  • , 2008.
  • Sundararajan, G., Krishna, L.R., Mechanisms
  • underlying the formation of thick alumina coatings
  • through the MAO coating technology, Surf Coat
  • Tech, 167, 269-277, 2003.
  • Krishna, L.R., Purnima, A.S., N.P. Wasekar, G.
  • Sundararajan, Kinetics and properties of micro arc
  • oxidation coatings deposited on commercial Al
  • alloys, Metall Mater Trans A, 38A, 370-378,
  • -
  • Verdier, S., Boinet, M., Maximovitch, S., Dalard,
  • F., Formation, structure and composition of anodic
  • films on AM60 magnesium alloy obtained by DC
  • plasma anodising, Corros Sci, 47, 1429-1444,
  • -
  • Liang, J., Guo, B.G., Tian, J., Liu, H.W., Zhou,
  • J.F., Liu, W.M., Xu, T., Effects of NaAlO2 on
  • structure and corrosion resistance of microarc
  • oxidation coatings formed on AM60B magnesium
  • alloy in phosphate-KOH electrolyte, Surf Coat
  • Tech, 199, 121-126, 2005.
  • Sun, X.T., Jiang, Z.H., Yao, Z.P., Zhang, X.L., The
  • effects of anodic and cathodic processes on the
  • characteristics of ceramic coatings formed on
  • titanium alloy through the MAO coating
  • technology, Appl Surf Sci, 252, 441-447, 2005.
  • Krishna, L.R., Somaraju, K.R.C., Sundararajan, G.,
  • The tribological performance of ultra-hard ceramic
  • composite coatings obtained through microarc
  • oxidation, Surf Coat Tech, 163, 484-490, 2003.
  • Yerokhin, A.L., Shatrov, A., Samsonov, V.,
  • Shashkov, P., Pilkington, A., Leyland, A.,
  • Matthews, A., Oxide ceramic coatings on
  • aluminium alloys produced by a pulsed bipolar
  • plasma electrolytic oxidation process, Surf Coat
  • Tech, 199, 150-157, 2005.
  • Liang, J., Guo, B.G., Tian, J., Liu, H.W., Zhou,
  • J.F., Xu, T., Effect of potassium fluoride in
  • electrolytic solution on the structure and properties
  • of microarc oxidation coatings on magnesium
  • alloy, Appl Surf Sci, 252, 345-351, 2005.
  • Martini, C., Sabatini, G., Ceschini, L., Williams,
  • J.A., Hutchings, I.M., Improving sliding and
  • abrasive wear behaviour of cast A356 and wrought
  • AA7075 aluminium alloys by plasma electrolytic
  • oxidation, Mater Design, 31, 816-828, 2010.
  • Nie, X., Meletis, E.I., Jiang, J.C., Leyland, A.,
  • Yerokhin, A.L., Matthews, A., Abrasive
  • wear/corrosion properties and TEM analysis of
  • Al2O3 coatings fabricated using plasma
  • electrolysis, Surf Coat Tech, 149, 245-251, 2002.
  • Chen, F., Zhou, H., Zhang, Q.F., Lv, F.X., Friction
  • and Wear of the Ceramic Coating Formed on
  • Magnesium Alloy, Advanced Tribology, 467-470,
  • -
  • Li, J., Bai, X.D., Zhang, D.L., Li, H.Y.,
  • Characterization and structure study of the anodic
  • oxide film on Zircaloy-4 synthesized using NaOH
  • electrolytes at room temperature, Appl Surf Sci,
  • , 7436-7441, 2006.
  • Han,Y., Yan, Y.Y., Lu, C.G., The effect of
  • chemical treatment on apatite-forming ability of
  • the macroporous zirconia films formed by micro arc oxidation, Appl Surf Sci, 254, 4833-4839,
  • -
  • Good, V., Widding, K., Hunter, G., Heuer, D.,
  • Oxidized zirconium: a potentially longer lasting hip
  • implant, Mater Design, 26, 618-622, 2005.
  • Uchida, M., Kim, H.M., Miyaji, F., Kokubo, T.,
  • Nakamura, T., Apatite formation on zirconium
  • metal treated with aqueous NaOH, Biomaterials,
  • , 313-317, 2002.
  • Xue, W.B., Zhu, Q.Z., Jin, Q., Hua, M.,
  • Characterization of ceramic coatings fabricated on
  • zirconium alloy by plasma electrolytic oxidation in
  • silicate electrolyte, Mater Chem Phys, 120, 656-
  • , 2010.
  • Miyake, M., Uno, M., Yamanaka, S., On the
  • zirconium-oxygen-hydrogen ternary system, J Nucl
  • Mater, 270, 233-241, 1999.
  • Setoyama, D., Yamanaka, S., Phase diagram of Zr-
  • O-H ternary system, J Alloy Compd, 370, 144-
  • , 2004.
  • Uchida, M., Kim, H.M., Kokubo, T., Tanaka, K.,
  • Nakamura, T., Structural dependence of apatite
  • formation on zirconia gels in a simulated body
  • fluid, J Ceram Soc Jpn, 110, 710-715, 2002.
  • Kobayashi, A., Shanmugavelayutham, G., Yano, S.,
  • Microstructural characterization and properties of
  • ZrO2/Al2O3 thermal barrier coatings by gas tunneltype
  • plasma spraying, Vacuum, 80, 1336-1340,
  • -
  • Chaim, R., Zhitomirsky, I., GalOr, L., Bestgen, H.,
  • Electrochemical Al2O3-ZrO2 composite coatings on
  • non-oxide ceramic substrates, J Mater Sci, 32,
  • -400, 1997.
  • Leushake, U., Krell, T., Schulz, U., Peters, M.,
  • Kaysser, W.A., Rabin, B.H., Microstructure and
  • phase stability of EB-PVD alumina and
  • alumina/zirconia for thermal barrier coating
  • applications, Surf Coat Tech, 94-5, 131-136, 1997
  • Pauporte, T., Finne, J., Kahn-Harari, A., Lincot, D.,
  • Growth by plasma electrolysis of zirconium oxide
  • films in the micrometer range, Surf Coat Tech,
  • , 213-219, 2005.
  • Ohki, M., Hwu, T.C., Mutoh, T., Thermal cycle
  • damage of wear-resistant ceramic coatings, T
  • Indian I Metals, 53, 135-140, 2000.
  • Han, Y., Yan, Y.Y., Li, D.C., Huang, J.J., Lian, Q.,
  • Effect of NaAlO2 concentrations on microstructure
  • and corrosion resistance of Al2O3/ZrO2 coatings
  • formed on zirconium by micro-arc oxidation, Appl
  • Surf Sci, 256, 6359-6366, 2010.
  • Hobbs, L.W., Rosen, V.B., Mangin, S.P., Treska,
  • M., Hunter, G., Oxidation microstructures and
  • interfaces in the oxidized zirconium knee, Int J
  • Appl Ceram Tec, 2, 221-246, 2005.
  • Han, Y., Yan,Y.Y., Structure and bioactivity of
  • micro-arc oxidized zirconia films, Surf Coat
  • Tech, 201, 5692-5695, 2007.
  • Han, Y., Yan, Y.Y., Lu, C.G., Zhang, Y.M., Xu,
  • K.W., Bioactivity and osteoblast response of the
  • micro-arc oxidized zirconia films, J Biomed
  • Mater Res A, 88A, 117-127, 2009.
  • Liu, L., Liu, Z., Chan, K.C., Luo, H.H., Cai, Q.Z.,
  • Zhang, S.M., Surface modification and
  • biocompatibility of Ni-free Zr-based bulk metallic
  • glass, Scripta Mater, 58, 231-234, 2008.
  • Klapkiv, M.D., State of an electrolytic plasma in
  • the process of synthesis of oxides based on
  • aluminum, Mater Sci+, 31, 494-499, 1995.
  • Wei, T.B., Yan, F.Y., Tian, J., Characterization
  • and wear- and corrosion-resistance of microarc
  • oxidation ceramic coatings on aluminum alloy, J
  • Alloy Compd, 389, 169-176, 2005.
  • Xue, W.B., Deng, Z.W., Lai, Y.C., Chen, R.Y.,
  • Analysis of phase distribution for ceramic coatings
  • formed by microarc oxidation on aluminum alloy,
  • J Am Ceram Soc, 81, 1365-1368, 1998.
  • Yerokhin, A.L., Lyubimov, V.V., Ashitkov, R.V.,
  • Phase formation in ceramic coatings during plasma
  • electrolytic oxidation of aluminium alloys, Ceram
  • Int, 24, 1-6, 1998.
  • Mcpherso, R., Formation of Metastable Phases in
  • Flame-Prepared and Plasma-Prepared Alumina, J
  • Mater Sci, 8, 851-858,1973.
  • Wu, H.H., Jin, Z.S., Long, B.Y., Yu, F.R., Lu,
  • X.Y., Characterization of microarc oxidation
  • process on aluminium alloy, Chinese Phys Lett,
  • , 1815-1818, 2003.
Year 2011, Volume: 26 Issue: 4, 0 - , 20.02.2013

Abstract

References

  • Xue, W., Deng, Z., H. Chen, Ma,, Zhang R. T.,
  • Microstructure and phase composition of microarc
  • oxidation coatings formed on Ti-6Al-4V alloy in
  • aluminate solution, Surface Eng, 17, 323-326,
  • -
  • Yerokhin, A.L., Nie, X., Leyland, A. Matthews, A.,
  • Dowey, S.J., Plasma electrolysis for surface
  • engineering, Surf Coat Tech, 122, 73-93, 1999.
  • G.L. Yang, X.Y. Lu, Y.Z. Bai, Z.S. Jin,
  • Characterization of microarc oxidation discharge
  • process for depositing ceramic coating, Chinese
  • Phys Lett, 18, 1141-1143, 2001.
  • Yerokhin, A.L., Snizhko, L.O., Gurevina, N.L.,
  • Leyland, A., Pilkington, A., Matthews, A., Spatial
  • characteristics of discharge phenomena in plasma
  • electrolytic oxidation of aluminium alloy, Surf
  • Coat Tech, 177, 779-783, 2004.
  • Wu, X.H., Qin, W., Guo, Y., Xie, Z.Y., Selflubricative
  • coating grown by micro-plasma
  • oxidation on aluminum alloys in the solution of
  • aluminate-graphite, Appl Surf Sci, 254, 6395-
  • , 2008.
  • Sundararajan, G., Krishna, L.R., Mechanisms
  • underlying the formation of thick alumina coatings
  • through the MAO coating technology, Surf Coat
  • Tech, 167, 269-277, 2003.
  • Krishna, L.R., Purnima, A.S., N.P. Wasekar, G.
  • Sundararajan, Kinetics and properties of micro arc
  • oxidation coatings deposited on commercial Al
  • alloys, Metall Mater Trans A, 38A, 370-378,
  • -
  • Verdier, S., Boinet, M., Maximovitch, S., Dalard,
  • F., Formation, structure and composition of anodic
  • films on AM60 magnesium alloy obtained by DC
  • plasma anodising, Corros Sci, 47, 1429-1444,
  • -
  • Liang, J., Guo, B.G., Tian, J., Liu, H.W., Zhou,
  • J.F., Liu, W.M., Xu, T., Effects of NaAlO2 on
  • structure and corrosion resistance of microarc
  • oxidation coatings formed on AM60B magnesium
  • alloy in phosphate-KOH electrolyte, Surf Coat
  • Tech, 199, 121-126, 2005.
  • Sun, X.T., Jiang, Z.H., Yao, Z.P., Zhang, X.L., The
  • effects of anodic and cathodic processes on the
  • characteristics of ceramic coatings formed on
  • titanium alloy through the MAO coating
  • technology, Appl Surf Sci, 252, 441-447, 2005.
  • Krishna, L.R., Somaraju, K.R.C., Sundararajan, G.,
  • The tribological performance of ultra-hard ceramic
  • composite coatings obtained through microarc
  • oxidation, Surf Coat Tech, 163, 484-490, 2003.
  • Yerokhin, A.L., Shatrov, A., Samsonov, V.,
  • Shashkov, P., Pilkington, A., Leyland, A.,
  • Matthews, A., Oxide ceramic coatings on
  • aluminium alloys produced by a pulsed bipolar
  • plasma electrolytic oxidation process, Surf Coat
  • Tech, 199, 150-157, 2005.
  • Liang, J., Guo, B.G., Tian, J., Liu, H.W., Zhou,
  • J.F., Xu, T., Effect of potassium fluoride in
  • electrolytic solution on the structure and properties
  • of microarc oxidation coatings on magnesium
  • alloy, Appl Surf Sci, 252, 345-351, 2005.
  • Martini, C., Sabatini, G., Ceschini, L., Williams,
  • J.A., Hutchings, I.M., Improving sliding and
  • abrasive wear behaviour of cast A356 and wrought
  • AA7075 aluminium alloys by plasma electrolytic
  • oxidation, Mater Design, 31, 816-828, 2010.
  • Nie, X., Meletis, E.I., Jiang, J.C., Leyland, A.,
  • Yerokhin, A.L., Matthews, A., Abrasive
  • wear/corrosion properties and TEM analysis of
  • Al2O3 coatings fabricated using plasma
  • electrolysis, Surf Coat Tech, 149, 245-251, 2002.
  • Chen, F., Zhou, H., Zhang, Q.F., Lv, F.X., Friction
  • and Wear of the Ceramic Coating Formed on
  • Magnesium Alloy, Advanced Tribology, 467-470,
  • -
  • Li, J., Bai, X.D., Zhang, D.L., Li, H.Y.,
  • Characterization and structure study of the anodic
  • oxide film on Zircaloy-4 synthesized using NaOH
  • electrolytes at room temperature, Appl Surf Sci,
  • , 7436-7441, 2006.
  • Han,Y., Yan, Y.Y., Lu, C.G., The effect of
  • chemical treatment on apatite-forming ability of
  • the macroporous zirconia films formed by micro arc oxidation, Appl Surf Sci, 254, 4833-4839,
  • -
  • Good, V., Widding, K., Hunter, G., Heuer, D.,
  • Oxidized zirconium: a potentially longer lasting hip
  • implant, Mater Design, 26, 618-622, 2005.
  • Uchida, M., Kim, H.M., Miyaji, F., Kokubo, T.,
  • Nakamura, T., Apatite formation on zirconium
  • metal treated with aqueous NaOH, Biomaterials,
  • , 313-317, 2002.
  • Xue, W.B., Zhu, Q.Z., Jin, Q., Hua, M.,
  • Characterization of ceramic coatings fabricated on
  • zirconium alloy by plasma electrolytic oxidation in
  • silicate electrolyte, Mater Chem Phys, 120, 656-
  • , 2010.
  • Miyake, M., Uno, M., Yamanaka, S., On the
  • zirconium-oxygen-hydrogen ternary system, J Nucl
  • Mater, 270, 233-241, 1999.
  • Setoyama, D., Yamanaka, S., Phase diagram of Zr-
  • O-H ternary system, J Alloy Compd, 370, 144-
  • , 2004.
  • Uchida, M., Kim, H.M., Kokubo, T., Tanaka, K.,
  • Nakamura, T., Structural dependence of apatite
  • formation on zirconia gels in a simulated body
  • fluid, J Ceram Soc Jpn, 110, 710-715, 2002.
  • Kobayashi, A., Shanmugavelayutham, G., Yano, S.,
  • Microstructural characterization and properties of
  • ZrO2/Al2O3 thermal barrier coatings by gas tunneltype
  • plasma spraying, Vacuum, 80, 1336-1340,
  • -
  • Chaim, R., Zhitomirsky, I., GalOr, L., Bestgen, H.,
  • Electrochemical Al2O3-ZrO2 composite coatings on
  • non-oxide ceramic substrates, J Mater Sci, 32,
  • -400, 1997.
  • Leushake, U., Krell, T., Schulz, U., Peters, M.,
  • Kaysser, W.A., Rabin, B.H., Microstructure and
  • phase stability of EB-PVD alumina and
  • alumina/zirconia for thermal barrier coating
  • applications, Surf Coat Tech, 94-5, 131-136, 1997
  • Pauporte, T., Finne, J., Kahn-Harari, A., Lincot, D.,
  • Growth by plasma electrolysis of zirconium oxide
  • films in the micrometer range, Surf Coat Tech,
  • , 213-219, 2005.
  • Ohki, M., Hwu, T.C., Mutoh, T., Thermal cycle
  • damage of wear-resistant ceramic coatings, T
  • Indian I Metals, 53, 135-140, 2000.
  • Han, Y., Yan, Y.Y., Li, D.C., Huang, J.J., Lian, Q.,
  • Effect of NaAlO2 concentrations on microstructure
  • and corrosion resistance of Al2O3/ZrO2 coatings
  • formed on zirconium by micro-arc oxidation, Appl
  • Surf Sci, 256, 6359-6366, 2010.
  • Hobbs, L.W., Rosen, V.B., Mangin, S.P., Treska,
  • M., Hunter, G., Oxidation microstructures and
  • interfaces in the oxidized zirconium knee, Int J
  • Appl Ceram Tec, 2, 221-246, 2005.
  • Han, Y., Yan,Y.Y., Structure and bioactivity of
  • micro-arc oxidized zirconia films, Surf Coat
  • Tech, 201, 5692-5695, 2007.
  • Han, Y., Yan, Y.Y., Lu, C.G., Zhang, Y.M., Xu,
  • K.W., Bioactivity and osteoblast response of the
  • micro-arc oxidized zirconia films, J Biomed
  • Mater Res A, 88A, 117-127, 2009.
  • Liu, L., Liu, Z., Chan, K.C., Luo, H.H., Cai, Q.Z.,
  • Zhang, S.M., Surface modification and
  • biocompatibility of Ni-free Zr-based bulk metallic
  • glass, Scripta Mater, 58, 231-234, 2008.
  • Klapkiv, M.D., State of an electrolytic plasma in
  • the process of synthesis of oxides based on
  • aluminum, Mater Sci+, 31, 494-499, 1995.
  • Wei, T.B., Yan, F.Y., Tian, J., Characterization
  • and wear- and corrosion-resistance of microarc
  • oxidation ceramic coatings on aluminum alloy, J
  • Alloy Compd, 389, 169-176, 2005.
  • Xue, W.B., Deng, Z.W., Lai, Y.C., Chen, R.Y.,
  • Analysis of phase distribution for ceramic coatings
  • formed by microarc oxidation on aluminum alloy,
  • J Am Ceram Soc, 81, 1365-1368, 1998.
  • Yerokhin, A.L., Lyubimov, V.V., Ashitkov, R.V.,
  • Phase formation in ceramic coatings during plasma
  • electrolytic oxidation of aluminium alloys, Ceram
  • Int, 24, 1-6, 1998.
  • Mcpherso, R., Formation of Metastable Phases in
  • Flame-Prepared and Plasma-Prepared Alumina, J
  • Mater Sci, 8, 851-858,1973.
  • Wu, H.H., Jin, Z.S., Long, B.Y., Yu, F.R., Lu,
  • X.Y., Characterization of microarc oxidation
  • process on aluminium alloy, Chinese Phys Lett,
  • , 1815-1818, 2003.
There are 170 citations in total.

Details

Primary Language Turkish
Journal Section Makaleler
Authors

Yücel Gençer This is me

Mehmet Tarakçı This is me

Sezgin Cengiz

Publication Date February 20, 2013
Submission Date February 20, 2013
Published in Issue Year 2011 Volume: 26 Issue: 4

Cite

APA Gençer, Y., Tarakçı, M., & Cengiz, S. (2013). SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi, 26(4).
AMA Gençer Y, Tarakçı M, Cengiz S. SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI. GUMMFD. March 2013;26(4).
Chicago Gençer, Yücel, Mehmet Tarakçı, and Sezgin Cengiz. “SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI”. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi 26, no. 4 (March 2013).
EndNote Gençer Y, Tarakçı M, Cengiz S (March 1, 2013) SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi 26 4
IEEE Y. Gençer, M. Tarakçı, and S. Cengiz, “SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI”, GUMMFD, vol. 26, no. 4, 2013.
ISNAD Gençer, Yücel et al. “SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI”. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi 26/4 (March 2013).
JAMA Gençer Y, Tarakçı M, Cengiz S. SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI. GUMMFD. 2013;26.
MLA Gençer, Yücel et al. “SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI”. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi, vol. 26, no. 4, 2013.
Vancouver Gençer Y, Tarakçı M, Cengiz S. SAF ZİRKONYUMUN MİKROARK OKSİDASYON YÖNTEMİYLE OKSİT ESASLI SERAMİK KAPLANMASI. GUMMFD. 2013;26(4).