Hirfanlı baraj gölünde eser elementlerin ICP-OES ile tayini

Şükrü Kalaycı

doi:10.29109/gujsc.718105

Hirfanlı baraj gölünde eser elementlerin ICP-OES ile tayini

Öz

Bu çalışmada, Kızılırmak üzerine kurulmuş olan Hirfanlı Baraj Gölü`nde eser elementlerin tayin için ICP-OES kullanıldı. Hirfanlı Baraj Gölü`nün değişik yerlerinden polietilen şişelere bir iki mililitre HCl eklenerek su örnekleri alındı. Bu örneklerdeki eser elementler, Perkin Elmer marka ICP-OES cihazıyla tayin edildi. ICP-OES cihazıyla, barajdan gelen su örneklerindeki demir, bakır, kurşun, krom, çinko, molibden ve selenyum elementleri tayin edildi. Uygun standart çözeltilerle belirli dalga boylarında elementlerin kalibrasyon işlemi yapıldı. Cihaz önce sertifikalı örnekteki elementlerin ölçümleri yapılarak duyarlılığı tespit edildi. Daha sonra su örneklerindeki elementlerin analizleri yapıldı. Baraj gölünde yapılan ölçümlere göre; Fe (III) 40 ± 0,3 µg/L, Cu (II) 10 ± 0,1 µg/L, Pb (II) 25 ± 0,1 µg/L, Cr (III) 15 ± 0,2 µg/L, Zn (II) 22 ± 0,2 µg/L, Mo (VI) 8 ± 0,1 µg/L, Se (IV) 35 ± 0,3 µg/L olarak % 95 güven aralığı ve 4 ölçümün sonunda bulunmuştur.

Anahtar Kelimeler

ICP-OES,Tayin,Eser elementler,Hirfanlı Baraj Gölü

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Details

Primary Language

Turkish

Subjects

Chemical Engineering

Journal Section

Research Article

Authors

Şükrü Kalaycı ^*
0000-0002-8643-6731
Türkiye

Publication Date

June 28, 2020

Submission Date

April 10, 2020

Acceptance Date

May 15, 2020

Published in Issue

Year 2020 Volume: 8 Number: 2

DOI

https://doi.org/10.29109/gujsc.718105

IZ

https://izlik.org/JA68DW28GG

Cite

RIS / Bibtex

APA

Kalaycı, Ş. (2020). Hirfanlı baraj gölünde eser elementlerin ICP-OES ile tayini. Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım Ve Teknoloji, 8(2), 451-457. https://doi.org/10.29109/gujsc.718105

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