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INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING

Year 2021, Volume: 5 Issue: 3, 654 - 662, 30.12.2021
https://doi.org/10.46519/ij3dptdi.1024485

Abstract

Additive Manufacturing (AM) technology produces parts in layers and offers design freedom (3D design), zero waste, reduced expensive tool material requirements, and improved mechanical properties. Maraging steels have superior strength and toughness with adequate ductility. The effect of aging process parameters on the final properties of AM Maraging steels is enormous. In this study, the effects of heat treatment atmospheres and temperatures to the direct metal laser sintered (DMLS) maraging steels were examined. Aging heat treatment was applied in different atmospheres(Ar/H2 and air) and temperatures(4900C,5200C,5500C,5800C). SEM and XRD devices were used to examine the microstructure properties, and Vickers hardness device was used to determine the mechanical properties. When the results are evaluated, it was observed that the increased temperature after 490 0C adversely affected the hardness value. XRD analysis showed martensite and austenite phases in air and Ar/H2 atmospheres. According to the SEM images, it can be said that the traces of the melt pool remaining from the AM disappear with the increasing temperature in general.

References

  • 1. Godec, M., Donik, C. Kocijan, A., Podgornik, B., Skobir Balantic, D. A.. “Effect of post-treated low-temperature plasma nitriding on the wear and corrosion resistance of 316L stainless steel manufactured by laser powder bed fusion”, Additive Manufacturing, Vol.32, Pages:1-9, 2020.
  • 2. Herzog, D., Seyda, V., Wycisk, E., Emmelmann, C. “Additive manufacturing of metals”, Acta Materialia, Vol.117, Pages:371-392, 2016.
  • 3. Çevik Z.A, Özsoy K., Erçetin A, The Effect of Machining Process on The Pyhsical and Surface Morphology of Ti6Al4V Specimens Produced Through Powder Bed Fusion Additive Manufacturing” Int. J. of 3D Printing Tech. Dig. Ind., Vol.5 Issue 2, Pages:187-194, 2021.
  • 4. Casalino, G., Campanelli, S.L., Contuzzi, N., Ludovico, A.D “Experimental investigation and statistical optimisation of the selective laser melting process of a maraging steel”, Optics & Laser Technology, Vol.65, Pages:151-158, 2015.
  • 5. ASTM F2792, F2792-12a - Standard Terminology for Additive ManufacturingTechnologies, ASTM B. Stand, Pages:10-12, 2013.
  • 6. Özer G., “Eklemeli üretim teknolojileri üzerine derleme” NÖHÜ Müh. Bilim. Derg. / NOHU J. Eng. Sci., Vol.9 Issue 1, Pages:606-621, 2020
  • 7. Li, X., & Yin, Z., Reverted austenite during aging in 18Ni(350) maraging steel. Materials Letters, Vol.24 Issue 4, Pages:239-242, 1995
  • 8. Mooney, B., Kourousis, K. I., Raghavendra, R., “Plastic Anisotropy of additively manufactured maraging steel: Influence of the build orientation and heat treatments”, Additive Manufacturing, Vol.25, Pages:19-31, 2018.
  • 9. I. Adam, W. B. du Preez, J. Combrinck, M. Zwemstra, “Conformal cooling channel design for direct metal sintering of maraging steel injection mould inserts”, Pages:1-11, 2019.
  • 10. dos Reis, A. G., Reis, D. A. P., Abdalla, A. J., Otubo, J., Zepka, S., Couto, A. A., & Scheid, V. H. B., “Effect of simultaneous plasma nitriding and aging treatment on the microstructure and hardness of maraging 300 steel”, Advanced Structured Materials, Vol.70, Pages:277–284, 2015.
  • 11. Bai, Y., Wang, D., Yang, Y., & Wang, H., “Effect of heat treatment on the microstructure and mechanical properties of maraging steel by selective laser melting”, Materials Science and Engineering A, Vol.760, Pages:105–117, 2015
  • 12. Yan, X., Huang, C., Chen, C., Bolot, R., Dembinski, L., Huang, R., Ma, W., Liao, H., & Liu, M., “Additive manufacturing of WC reinforced maraging steel 300 composites by cold spraying and selective laser melting”, Surface and Coatings Technology, Vol.371, Pages:161–171, 2019.
  • 13. Aydın İ., “Investigation of Effects of Heat Treatment Process on Microstructural and Mechanical Properties of Additively Manufactured 18Ni300 Maraging Steel”, Graduate thesis, Middle East Technical University, Ankara, 2020
  • 14. Gordon Jones , “https://all3dp.com/2/direct-metal-laser-sintering-dmls-simply-explained/”, 2021.
  • 15. Stornelli, G., Gaggia, D., Rallini, M., & di Schino, A., “Heat treatment effect on maraging steel manufactured by laser powder bed fusion technology: Microstructure and mechanical properties”, Acta Metallurgica Slovaca, Vol.27 Issue 3, Pages:122–126, 2021.
  • 16. EOS, ”Material Data Sheet”, eos.info/03_system-related-assets/material-related-contents/metal-materials-and-examples/metal-material-datasheet/werkzeugstahl_ms1_cx/ms1/ms-ms1-m280_m290_400w_material_data_sheet_05-14_en.pdf”, Erişim:21.12.2016, 2021
  • 17. Gökhan Özer, Ahmet Karaaslan, “A Study on the Effects of Different Heat-Treatment Parameters on Microstructure–Mechanical Properties and Corrosion Behavior of Maraging Steel Produced by Direct Metal Laser Sintering”, Steel research international, Vol. 91 Issue 10, Pages:1-8 ,2020.
  • 18. Song, J., Tang, Q., Feng, Q., Ma, S., Setchi, R., Liu, Y., Han, Q., Fan, X., & Zhang, M., “Effect of heat treatment on microstructure and mechanical behaviours of 18Ni-300 maraging steel manufactured by selective laser melting”, Optics and Laser Technology, Vol.120, 2019.
  • 19. Tan, C., Zhou, K., Ma, W., Zhang, P., Liu, M., & Kuang, T., “Microstructural evolution, nanoprecipitation behavior and mechanicalproperties of selective laser melted high-performance grade 300maraging steel” Materials and Design, Vol.134, Pages:23-34, 2017.

INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING

Year 2021, Volume: 5 Issue: 3, 654 - 662, 30.12.2021
https://doi.org/10.46519/ij3dptdi.1024485

Abstract

Additive Manufacturing (AM) technology produces parts in layers and offers design freedom (3D design), zero waste, reduced expensive tool material requirements, and improved mechanical properties. Maraging steels have superior strength and toughness with adequate ductility. The effect of aging process parameters on the final properties of AM Maraging steels is enormous. In this study, the effects of heat treatment atmospheres and temperatures to the direct metal laser sintered (DMLS) maraging steels were examined. Aging heat treatment was applied in different atmospheres(Ar/H2 and air) and temperatures(4900C,5200C,5500C,5800C). SEM and XRD devices were used to examine the microstructure properties, and Vickers hardness device was used to determine the mechanical properties. When the results are evaluated, it was observed that the increased temperature after 490 0C adversely affected the hardness value. XRD analysis showed martensite and austenite phases in air and Ar/H2 atmospheres. According to the SEM images, it can be said that the traces of the melt pool remaining from the AM disappear with the increasing temperature in general.

References

  • 1. Godec, M., Donik, C. Kocijan, A., Podgornik, B., Skobir Balantic, D. A.. “Effect of post-treated low-temperature plasma nitriding on the wear and corrosion resistance of 316L stainless steel manufactured by laser powder bed fusion”, Additive Manufacturing, Vol.32, Pages:1-9, 2020.
  • 2. Herzog, D., Seyda, V., Wycisk, E., Emmelmann, C. “Additive manufacturing of metals”, Acta Materialia, Vol.117, Pages:371-392, 2016.
  • 3. Çevik Z.A, Özsoy K., Erçetin A, The Effect of Machining Process on The Pyhsical and Surface Morphology of Ti6Al4V Specimens Produced Through Powder Bed Fusion Additive Manufacturing” Int. J. of 3D Printing Tech. Dig. Ind., Vol.5 Issue 2, Pages:187-194, 2021.
  • 4. Casalino, G., Campanelli, S.L., Contuzzi, N., Ludovico, A.D “Experimental investigation and statistical optimisation of the selective laser melting process of a maraging steel”, Optics & Laser Technology, Vol.65, Pages:151-158, 2015.
  • 5. ASTM F2792, F2792-12a - Standard Terminology for Additive ManufacturingTechnologies, ASTM B. Stand, Pages:10-12, 2013.
  • 6. Özer G., “Eklemeli üretim teknolojileri üzerine derleme” NÖHÜ Müh. Bilim. Derg. / NOHU J. Eng. Sci., Vol.9 Issue 1, Pages:606-621, 2020
  • 7. Li, X., & Yin, Z., Reverted austenite during aging in 18Ni(350) maraging steel. Materials Letters, Vol.24 Issue 4, Pages:239-242, 1995
  • 8. Mooney, B., Kourousis, K. I., Raghavendra, R., “Plastic Anisotropy of additively manufactured maraging steel: Influence of the build orientation and heat treatments”, Additive Manufacturing, Vol.25, Pages:19-31, 2018.
  • 9. I. Adam, W. B. du Preez, J. Combrinck, M. Zwemstra, “Conformal cooling channel design for direct metal sintering of maraging steel injection mould inserts”, Pages:1-11, 2019.
  • 10. dos Reis, A. G., Reis, D. A. P., Abdalla, A. J., Otubo, J., Zepka, S., Couto, A. A., & Scheid, V. H. B., “Effect of simultaneous plasma nitriding and aging treatment on the microstructure and hardness of maraging 300 steel”, Advanced Structured Materials, Vol.70, Pages:277–284, 2015.
  • 11. Bai, Y., Wang, D., Yang, Y., & Wang, H., “Effect of heat treatment on the microstructure and mechanical properties of maraging steel by selective laser melting”, Materials Science and Engineering A, Vol.760, Pages:105–117, 2015
  • 12. Yan, X., Huang, C., Chen, C., Bolot, R., Dembinski, L., Huang, R., Ma, W., Liao, H., & Liu, M., “Additive manufacturing of WC reinforced maraging steel 300 composites by cold spraying and selective laser melting”, Surface and Coatings Technology, Vol.371, Pages:161–171, 2019.
  • 13. Aydın İ., “Investigation of Effects of Heat Treatment Process on Microstructural and Mechanical Properties of Additively Manufactured 18Ni300 Maraging Steel”, Graduate thesis, Middle East Technical University, Ankara, 2020
  • 14. Gordon Jones , “https://all3dp.com/2/direct-metal-laser-sintering-dmls-simply-explained/”, 2021.
  • 15. Stornelli, G., Gaggia, D., Rallini, M., & di Schino, A., “Heat treatment effect on maraging steel manufactured by laser powder bed fusion technology: Microstructure and mechanical properties”, Acta Metallurgica Slovaca, Vol.27 Issue 3, Pages:122–126, 2021.
  • 16. EOS, ”Material Data Sheet”, eos.info/03_system-related-assets/material-related-contents/metal-materials-and-examples/metal-material-datasheet/werkzeugstahl_ms1_cx/ms1/ms-ms1-m280_m290_400w_material_data_sheet_05-14_en.pdf”, Erişim:21.12.2016, 2021
  • 17. Gökhan Özer, Ahmet Karaaslan, “A Study on the Effects of Different Heat-Treatment Parameters on Microstructure–Mechanical Properties and Corrosion Behavior of Maraging Steel Produced by Direct Metal Laser Sintering”, Steel research international, Vol. 91 Issue 10, Pages:1-8 ,2020.
  • 18. Song, J., Tang, Q., Feng, Q., Ma, S., Setchi, R., Liu, Y., Han, Q., Fan, X., & Zhang, M., “Effect of heat treatment on microstructure and mechanical behaviours of 18Ni-300 maraging steel manufactured by selective laser melting”, Optics and Laser Technology, Vol.120, 2019.
  • 19. Tan, C., Zhou, K., Ma, W., Zhang, P., Liu, M., & Kuang, T., “Microstructural evolution, nanoprecipitation behavior and mechanicalproperties of selective laser melted high-performance grade 300maraging steel” Materials and Design, Vol.134, Pages:23-34, 2017.
There are 19 citations in total.

Details

Primary Language English
Subjects Biomaterial
Journal Section Research Article
Authors

İlkgül Öksüzcan This is me 0000-0002-8308-9615

Derya Çakan This is me 0000-0003-3482-5994

Mustafa Safa Yılmaz 0000-0003-2614-9121

Onur Ertuğrul 0000-0001-9017-9443

Publication Date December 30, 2021
Submission Date November 16, 2021
Published in Issue Year 2021 Volume: 5 Issue: 3

Cite

APA Öksüzcan, İ., Çakan, D., Yılmaz, M. S., Ertuğrul, O. (2021). INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING. International Journal of 3D Printing Technologies and Digital Industry, 5(3), 654-662. https://doi.org/10.46519/ij3dptdi.1024485
AMA Öksüzcan İ, Çakan D, Yılmaz MS, Ertuğrul O. INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING. IJ3DPTDI. December 2021;5(3):654-662. doi:10.46519/ij3dptdi.1024485
Chicago Öksüzcan, İlkgül, Derya Çakan, Mustafa Safa Yılmaz, and Onur Ertuğrul. “INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING”. International Journal of 3D Printing Technologies and Digital Industry 5, no. 3 (December 2021): 654-62. https://doi.org/10.46519/ij3dptdi.1024485.
EndNote Öksüzcan İ, Çakan D, Yılmaz MS, Ertuğrul O (December 1, 2021) INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING. International Journal of 3D Printing Technologies and Digital Industry 5 3 654–662.
IEEE İ. Öksüzcan, D. Çakan, M. S. Yılmaz, and O. Ertuğrul, “INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING”, IJ3DPTDI, vol. 5, no. 3, pp. 654–662, 2021, doi: 10.46519/ij3dptdi.1024485.
ISNAD Öksüzcan, İlkgül et al. “INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING”. International Journal of 3D Printing Technologies and Digital Industry 5/3 (December 2021), 654-662. https://doi.org/10.46519/ij3dptdi.1024485.
JAMA Öksüzcan İ, Çakan D, Yılmaz MS, Ertuğrul O. INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING. IJ3DPTDI. 2021;5:654–662.
MLA Öksüzcan, İlkgül et al. “INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING”. International Journal of 3D Printing Technologies and Digital Industry, vol. 5, no. 3, 2021, pp. 654-62, doi:10.46519/ij3dptdi.1024485.
Vancouver Öksüzcan İ, Çakan D, Yılmaz MS, Ertuğrul O. INVESTIGATION OF THE EFFECT OF HEAT TREATMENT CONDITIONS ON HARDNESS PROPERTIES OF MARAGING STEELS PRODUCED BY ADDITIVE MANUFACTURING. IJ3DPTDI. 2021;5(3):654-62.

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