Research Article
BibTex RIS Cite

Developing Natural Shampoo Formulation Against Hair Loss with Microbiologically Tested Herbal Extracts and Essential Oils

Year 2024, Volume: 9 Issue: 1, 12 - 23, 30.04.2024
https://doi.org/10.58854/jicm.1402811

Abstract

Objectives: Shampoo is the most frequently used cosmetic product. Given the importance placed on cleanliness for hair health and the increasing importance placed on hair beauty and care, it is evident that synthetic shampoos damage hair when used regularly. In this context, the objective was to produce a natural shampoo and conduct antimicrobial analysis using Urtica dioica (nettle), wheat germ oil, Rosa damascena Mill (Isparta rose), and Allium sativum (garlic).

Material and Methods: All necessary processes, including formulation design, characterization, and final product tests, were carried out within the scope of the study until the product was packaged and became the final product. Physicochemical tests (pH, viscosity, dandruff effect, microbiological tests) and stability tests (color, odor, appearance, and pH control) were performed on the developed formulation.

Results: The analysis revealed that the pH value of the formulations was approximately 5.5, which is suitable for the skin. The selected NI-S-7 exhibited high viscosity (26.43 ± 0.75), foaming index (250), and high cleaning efficiency among all formulations. This led to developing a shampoo containing active herbal ingredients that nourish and repair hair. Furthermore, the microbiological analysis of the resulting formulation product was conducted and found to comply with the established limit values.

Conclusion: The transformation of agricultural products into commercial products has the potential to bolster the economy. The shampoo in development will be derived from naturally sourced plants cultivated in Turkey and utilized for medical conditions with an aromatherapeutic effect while preserving the typical scent of the rose plant.

Ethical Statement

not applicable

Thanks

I would like to thank Dr Ahmet Arif Kurt for her support in the study.

References

  • Ahmed Y, Jamil SS, Hashimi A, Siraj MB, Jahangir U. Rosa Damascene Mill. (Rose): A versatile herb in cosmetology. Humanitas medicine 2019; 9 (4): e2. https://doi.org/ 10.5667/tang.2019.0017
  • Yılmaztekin Y. A Review on Hypoglycemic Effects of the Urtica dioica L. and Punica granatum L. Plants. Anat. J. Pharm. Sci 2022; 1(1): 1-8.
  • Tito A, Minale M, Riccio S, Grieco F, Colucci MG, Apone F. A Triticum vulgare Extract Exhibits Regenerating Activity During the Wound Healing Process. Clin Cosmet Investig Dermatol. 2020; 13: 21–30. https://doi.org/ 10.2147/CCID.S216391
  • Kim HW, Seok YS, Cho TJ, Rhee MS. Risk factors influencing contamination of customized cosmetics made on-the-spot: Evidence from the national pilot project for public health. Sci Rep. 2020; 10: 1561.
  • Döner P, Öztürk İİ. Activities of Amphoteric Surfactants on Shampoo. BSEU Journal of Science 2022; 9(1), 574-582. https://doi.org/10.35193/bseufbd.1106220
  • Adu SA, Naughton PJ, Marchant R, Banat IM.Microbial Biosurfactants in Cosmetic and Personal Skincare Pharmaceutical Formulations. Pharmaceutics. 2020 Nov; 12(11): 1099. doi: 10.3390/pharmaceutics12111099
  • Kabara JJ, Orth DS. Principles for product preservation. In Preservative-Free and Self-Preserving Cosmetics and Drugs: Principles and Practices; Kabara, J.J., Ed.; Marcel Dekker: New York, NY, USA, 1997; pp. 1–14.
  • Huang HY, Lai YC, Chiu CW, Yeh JM. Comparing micellar electrokinetic chromatography and microemulsion electrokinetic chromatography for the analysis of preservatives in pharmaceutical and cosmetic products. J. Chromatogr. A 2003, 993, 153–164.
  • Hoang HT, Moon JY, Lee YC. Natural antioxidants from plant extracts in skincare cosmetics: Recent applications, challenges and perspectives. Cosmetics. 2021;8(4). https://doi.org/10.3390/cosmetics8040106
  • Głaz P, Rosińska A, Woźniak S, Boguszewska-Czubara A, Biernasiuk A, Matosiuk D. Effect of Commonly Used Cosmetic Preservatives on Healthy Human Skin Cells. Cells. 2023;12(7). https://doi.org/10.3390/cells12071076
  • Kurt AA, Aslan I, Duman, G. Next-Generation Natural Baby Barrier Cream Formulations: Physicochemical Analysis and Safety Assessment. Journal of Cosmetic Science, 2021; 72(2).
  • Ali HS, Kadhim RB. Formulation and evaluation of herbal shampoo from Ziziphus spina leaves extract. Int J Res Appl Pharm 2011; 2:1802-6.
  • Lasseuguette, E., Roux, D., & Nishiyama, Y. Rheological properties of microfibrillar suspension of TEMPO-oxidized pulp. Cellulose, 2008; 15, 425-433.
  • Serra-Paraeda F, Tarr´es Q, Sanchez-Salvador JL, et al. Tuning morphology and structure of non-woody nanocellulose: Ranging between nanofibers and nanocrystals. Industrial Crops & Products 2021; 171, 113877. https://doi.org/10.1016/j.indcrop.2021.113877
  • Halla N, Fernandes IP, Heleno SA, Costa P, Boucherit-Otmani Z, Boucherit K, et al. Cosmetics preservation: A review on present strategies. Molecules. 2018;23(7). https://doi.org/10.3390/molecules23071571.
  • Yazıcı EK, Eryilmaz M. Investıgatıon Of The Mıcrobıologıcal Contamınatıon Of Used Lıpstıcks And Mascaras. Ankara Universitesi Eczacilik Fakultesi Dergisi. 2023;47(1):269-276. https://doi.org/10.33483/jfpau.1209451
  • Giacomel CB, Dartora G, Dienfethaeler HS, Haas SE. Investigation on the use of expired make-up and microbiological contamination of mascaras. Int J Cosmet Sci. 2013;35(4):375-380. https://doi.org/ 10.1111/ics.12053
  • Lundov MD, Moesby L, Zacharıae C, et al, Contamination versus preservation of cosmetics: a review on legislation, usage, infections, and contact allergy. Contact Dermatitis 2009: 60: 70–78. https://doi.org/10.1111/j.1600-0536.2008.01501.x
  • Eldesoukey RMM, Alqhtani BS, Alqhtani AS, Alqhtani AH, Alqhtani AM. Comparative microbiological study between traditional and modern cosmetics in Saudi Arabia. Enzyme Engineering, 2016; 5:2.
  • Babalola M, Eze M. Microbiological quality and characterization of potential pathogens associated with selected brands of commercial cosmetic products in Nigeria. Microbiology Research Journal International, 2018; 9, 1-17.
  • Michalek IM, John SM, Caetano dos Santos FL. Microbiological contamination of cosmetic products-observations from Europe, 2005-2018. Journal of European Academy of Dermatology and Venereology, 2019; 33, 2151-2157.
  • Neza E, Centini M. Microbiologically contaminated and over-preserved cosmetic products according apex 2008–2014. Cosmetics, 2016; 3, 3.
  • Skowron K, Budzyńska A, Kaczmarek A, Grudlewska K. Microbiological purity assessment of cosmetics used by one and several persons and cosmetics after their expiry date. Rocz Panstw Zakl Hig. Published online 2017. https://www.researchgate.net/publication/317903586
  • Anand U, Tudu CK, Nandy S, et al. Ethnodermatological use of medicinal plants in India: From ayurvedic formulations to clinical perspectives – A review. Journal of Ethnopharmacology 284, 114744. https://doi.org/10.1016/j.jep.2021.114744

Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi

Year 2024, Volume: 9 Issue: 1, 12 - 23, 30.04.2024
https://doi.org/10.58854/jicm.1402811

Abstract

Amaç: Şampuan en sık kullanılan kozmetik üründür. Saç sağlığı için temizliğe verilen önem nedeniyle saç güzelliğine ve bakımına verilen önem de giderek artmaktadır. Sentetik şampuanlar düzenli kullanıldığında saçlara zarar verir. Bu kapsamda Urtica dioica (ısırgan otu), buğday tohumu yağı, Rosa damascena Mill (Isparta gülü) ve Allium sativum (sarımsak) kullanılarak doğal bir şampuan üretilmesi ve antimikrobiyal analizlerin yapılması amaçlandı.

Gereç ve Yöntem: Ürün paketlenip nihai ürün haline gelinceye kadar gerekli tüm süreçler (formülasyon tasarımı, karakterizasyon ve son ürün testleri) çalışma kapsamında gerçekleştirildi. Geliştirilen formülasyon üzerinde fizikokimyasal testler (pH, viskozite, kepek etkisi, mikrobiyolojik testler) ve stabilite testleri (renk, koku, görünüm ve pH kontrolü) yapıldı.

Bulgular: Analiz sonucunda formülasyonların pH değerinin cilde uygun olan 5,5’e yakın olduğu belirlendi. Seçilen NI-S-7, tüm formülasyonlar arasında yüksek viskozite (26,43± 0,75), köpüklenme indeksi (250) ve yüksek temizleme verimliliği gösterdi. Saçı besleyen ve onaran bitkisel etken maddeler içeren bir şampuan elde edildi. Ayrıca ortaya çıkan formülasyon ürününün mikrobiyolojik analizi yapılmış ve Türkiye İlaç ve Tibbi Cihaz Kurumu (TITCK) tarafından yayınlanan kozmetik ürünlerde güvenlilik kılavuzına göre sınır değerlere uygun olduğu görülmüştür.

Sonuç: Ülkemizde yetiştirilen ürünlerin ticari ürüne dönüştürülmesi ekonomiye destek olacaktır. Geliştirilecek şampuan, gül bitkisinin tipik kokusunu koruduğu için Türkiye’de yetişen doğal kaynaklı bitkilerden elde edilecek ve aromaterapi etkisiyle tıbbi rahatsızlıklarda kullanılması beklenmektedir.

References

  • Ahmed Y, Jamil SS, Hashimi A, Siraj MB, Jahangir U. Rosa Damascene Mill. (Rose): A versatile herb in cosmetology. Humanitas medicine 2019; 9 (4): e2. https://doi.org/ 10.5667/tang.2019.0017
  • Yılmaztekin Y. A Review on Hypoglycemic Effects of the Urtica dioica L. and Punica granatum L. Plants. Anat. J. Pharm. Sci 2022; 1(1): 1-8.
  • Tito A, Minale M, Riccio S, Grieco F, Colucci MG, Apone F. A Triticum vulgare Extract Exhibits Regenerating Activity During the Wound Healing Process. Clin Cosmet Investig Dermatol. 2020; 13: 21–30. https://doi.org/ 10.2147/CCID.S216391
  • Kim HW, Seok YS, Cho TJ, Rhee MS. Risk factors influencing contamination of customized cosmetics made on-the-spot: Evidence from the national pilot project for public health. Sci Rep. 2020; 10: 1561.
  • Döner P, Öztürk İİ. Activities of Amphoteric Surfactants on Shampoo. BSEU Journal of Science 2022; 9(1), 574-582. https://doi.org/10.35193/bseufbd.1106220
  • Adu SA, Naughton PJ, Marchant R, Banat IM.Microbial Biosurfactants in Cosmetic and Personal Skincare Pharmaceutical Formulations. Pharmaceutics. 2020 Nov; 12(11): 1099. doi: 10.3390/pharmaceutics12111099
  • Kabara JJ, Orth DS. Principles for product preservation. In Preservative-Free and Self-Preserving Cosmetics and Drugs: Principles and Practices; Kabara, J.J., Ed.; Marcel Dekker: New York, NY, USA, 1997; pp. 1–14.
  • Huang HY, Lai YC, Chiu CW, Yeh JM. Comparing micellar electrokinetic chromatography and microemulsion electrokinetic chromatography for the analysis of preservatives in pharmaceutical and cosmetic products. J. Chromatogr. A 2003, 993, 153–164.
  • Hoang HT, Moon JY, Lee YC. Natural antioxidants from plant extracts in skincare cosmetics: Recent applications, challenges and perspectives. Cosmetics. 2021;8(4). https://doi.org/10.3390/cosmetics8040106
  • Głaz P, Rosińska A, Woźniak S, Boguszewska-Czubara A, Biernasiuk A, Matosiuk D. Effect of Commonly Used Cosmetic Preservatives on Healthy Human Skin Cells. Cells. 2023;12(7). https://doi.org/10.3390/cells12071076
  • Kurt AA, Aslan I, Duman, G. Next-Generation Natural Baby Barrier Cream Formulations: Physicochemical Analysis and Safety Assessment. Journal of Cosmetic Science, 2021; 72(2).
  • Ali HS, Kadhim RB. Formulation and evaluation of herbal shampoo from Ziziphus spina leaves extract. Int J Res Appl Pharm 2011; 2:1802-6.
  • Lasseuguette, E., Roux, D., & Nishiyama, Y. Rheological properties of microfibrillar suspension of TEMPO-oxidized pulp. Cellulose, 2008; 15, 425-433.
  • Serra-Paraeda F, Tarr´es Q, Sanchez-Salvador JL, et al. Tuning morphology and structure of non-woody nanocellulose: Ranging between nanofibers and nanocrystals. Industrial Crops & Products 2021; 171, 113877. https://doi.org/10.1016/j.indcrop.2021.113877
  • Halla N, Fernandes IP, Heleno SA, Costa P, Boucherit-Otmani Z, Boucherit K, et al. Cosmetics preservation: A review on present strategies. Molecules. 2018;23(7). https://doi.org/10.3390/molecules23071571.
  • Yazıcı EK, Eryilmaz M. Investıgatıon Of The Mıcrobıologıcal Contamınatıon Of Used Lıpstıcks And Mascaras. Ankara Universitesi Eczacilik Fakultesi Dergisi. 2023;47(1):269-276. https://doi.org/10.33483/jfpau.1209451
  • Giacomel CB, Dartora G, Dienfethaeler HS, Haas SE. Investigation on the use of expired make-up and microbiological contamination of mascaras. Int J Cosmet Sci. 2013;35(4):375-380. https://doi.org/ 10.1111/ics.12053
  • Lundov MD, Moesby L, Zacharıae C, et al, Contamination versus preservation of cosmetics: a review on legislation, usage, infections, and contact allergy. Contact Dermatitis 2009: 60: 70–78. https://doi.org/10.1111/j.1600-0536.2008.01501.x
  • Eldesoukey RMM, Alqhtani BS, Alqhtani AS, Alqhtani AH, Alqhtani AM. Comparative microbiological study between traditional and modern cosmetics in Saudi Arabia. Enzyme Engineering, 2016; 5:2.
  • Babalola M, Eze M. Microbiological quality and characterization of potential pathogens associated with selected brands of commercial cosmetic products in Nigeria. Microbiology Research Journal International, 2018; 9, 1-17.
  • Michalek IM, John SM, Caetano dos Santos FL. Microbiological contamination of cosmetic products-observations from Europe, 2005-2018. Journal of European Academy of Dermatology and Venereology, 2019; 33, 2151-2157.
  • Neza E, Centini M. Microbiologically contaminated and over-preserved cosmetic products according apex 2008–2014. Cosmetics, 2016; 3, 3.
  • Skowron K, Budzyńska A, Kaczmarek A, Grudlewska K. Microbiological purity assessment of cosmetics used by one and several persons and cosmetics after their expiry date. Rocz Panstw Zakl Hig. Published online 2017. https://www.researchgate.net/publication/317903586
  • Anand U, Tudu CK, Nandy S, et al. Ethnodermatological use of medicinal plants in India: From ayurvedic formulations to clinical perspectives – A review. Journal of Ethnopharmacology 284, 114744. https://doi.org/10.1016/j.jep.2021.114744
There are 24 citations in total.

Details

Primary Language Turkish
Subjects Medical Bacteriology
Journal Section Research Articles
Authors

Bashar Ibrahım 0000-0003-3086-0995

Ahmet Arif Kurt 0000-0002-3490-0192

Publication Date April 30, 2024
Submission Date December 10, 2023
Acceptance Date April 17, 2024
Published in Issue Year 2024 Volume: 9 Issue: 1

Cite

APA Ibrahım, B., & Kurt, A. A. (2024). Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi. Journal of Immunology and Clinical Microbiology, 9(1), 12-23. https://doi.org/10.58854/jicm.1402811
AMA Ibrahım B, Kurt AA. Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi. J Immunol Clin Microbiol. April 2024;9(1):12-23. doi:10.58854/jicm.1402811
Chicago Ibrahım, Bashar, and Ahmet Arif Kurt. “Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar Ve Esansiyel Yağlar Ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi”. Journal of Immunology and Clinical Microbiology 9, no. 1 (April 2024): 12-23. https://doi.org/10.58854/jicm.1402811.
EndNote Ibrahım B, Kurt AA (April 1, 2024) Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi. Journal of Immunology and Clinical Microbiology 9 1 12–23.
IEEE B. Ibrahım and A. A. Kurt, “Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi”, J Immunol Clin Microbiol, vol. 9, no. 1, pp. 12–23, 2024, doi: 10.58854/jicm.1402811.
ISNAD Ibrahım, Bashar - Kurt, Ahmet Arif. “Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar Ve Esansiyel Yağlar Ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi”. Journal of Immunology and Clinical Microbiology 9/1 (April 2024), 12-23. https://doi.org/10.58854/jicm.1402811.
JAMA Ibrahım B, Kurt AA. Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi. J Immunol Clin Microbiol. 2024;9:12–23.
MLA Ibrahım, Bashar and Ahmet Arif Kurt. “Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar Ve Esansiyel Yağlar Ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi”. Journal of Immunology and Clinical Microbiology, vol. 9, no. 1, 2024, pp. 12-23, doi:10.58854/jicm.1402811.
Vancouver Ibrahım B, Kurt AA. Mikrobiyolojik Olarak Test Edilmiş Bitkisel Ekstraktlar ve Esansiyel Yağlar ile Saç Dökülmesine Karşı Doğal Şampuan Formülasyon Geliştirilmesi. J Immunol Clin Microbiol. 2024;9(1):12-23.

88x31.png 

Creative Commons Attribution Non-Commercial License: The articles in the Journal of Immunology and Clinical Microbiology are open access articles licensed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-sa/4.0/) which permits unrestricted, non-commercial use, distribution and reproduction in any medium, provided the work is properly cited.

JICM is a product of QMEL® medicine & publishing