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CrVMoO7: MICROWAVE SYNTHESIS AND STRUCTURAL CHARACTERIZATION

Year 2018, Volume: 5 Issue: 2, 881 - 884, 01.01.2018
https://doi.org/10.18596/jotcsa.315212

Abstract

In this study, microwave
synthesis method was operated to obtain CrVMoO7. Structural
characterization of the compound was realized by powder X-ray diffraction (XRD)
and fourier transform infrared spectrum (FTIR). Morphological property and
elemental composition were determined via scanning electron microscopy (SEM)
and energy dispersive X-ray analysis (EDS). Thermal nature of the sample was
identified by thermogravimetric analyzer (TGA). 

References

  • 1. Walczak J, Filipek E. In Sofia, Bulgaria: IUPAC; 1987. p. 171.
  • 2. Walczak J, Filipek E. The CrVO4-MoO3 system. Thermochimica Acta. 1989 Sep;150(1):125–31.
  • 3. Walczak J, Filipek E. Phase equilibria in the Cr2V4O13-CrVMoO7 system. Thermochimica Acta. 1990 May;161(2):239–45.
  • 4. Walczak J, Filipek E. Studies on the V2O5-CrVMoO7 system. Thermochimica Acta. 1990 Dec;173:235–40.
  • 5. Walczak J, Filipek E. Zeszyty Naukowe Politechniki Slaskiej. Seria: Chemia. 1988;119(958):380. 6. Walczak J, Filipek E. Reactivity of MoO3 towards Cr2V4O13. Thermochimica Acta. 1988 Oct;133:67–72.
  • 7. Kuriata J, Sadłowski L, Walczak J, Filipek E. Temperature Dependence of the EPR Linewidth of CrVO4. physica status solidi (b). 1987 Jul 1;142(1):K73–7.
  • 8. Walczak J, Filipek E, Tabero P. CrVMoO7 and phase equilibria in the V9Mo6O40-CrVMoO7 system. Thermochimica Acta. 1992 Sep;206:279–84.
  • 9. Walczak J, Filipek E. Studies on the CrVMoO7-Cr2(MoO4)3 system. Thermochimica Acta. 1993 Nov;228:127–30.
  • 10. Walczak J, Rychiowska-Himmel I, Tabero P. Iron(III) tungstate and its modifications. Journal of Materials Science. 1992;27(13):3680–4.
  • 11. Plasova L, Kefeli L. Inorganic Materials. Vol. 3. 1967. 906 p.
  • 12. Baykal A, Kizilyalli M, Kniep R. X-ray powder diffraction and IR study of NaMg (H2O) 2 [BP2O8]· H2O and NH4Mg (H2O) 2 [BP2O8]· H2O. Journal of materials science. 2000;35(18):4621–4626.
  • 13. Gözel G, Kizilyalli M, Kniep R. Characterization of a new calcium ultraphosphate, Ca3 (P5O14) 2. Journal of Solid State Chemistry. 1997;129(2):196–199.
  • 14. Gözel G, Baykal A, Kizilyalli M, Kniep R. Solid-State Synthesis, X-ray Powder Investigation and IR Study of α-Mg3[BPO7]. Journal of the European Ceramic Society. 1998 Dec;18(14):2241–6.
Year 2018, Volume: 5 Issue: 2, 881 - 884, 01.01.2018
https://doi.org/10.18596/jotcsa.315212

Abstract

References

  • 1. Walczak J, Filipek E. In Sofia, Bulgaria: IUPAC; 1987. p. 171.
  • 2. Walczak J, Filipek E. The CrVO4-MoO3 system. Thermochimica Acta. 1989 Sep;150(1):125–31.
  • 3. Walczak J, Filipek E. Phase equilibria in the Cr2V4O13-CrVMoO7 system. Thermochimica Acta. 1990 May;161(2):239–45.
  • 4. Walczak J, Filipek E. Studies on the V2O5-CrVMoO7 system. Thermochimica Acta. 1990 Dec;173:235–40.
  • 5. Walczak J, Filipek E. Zeszyty Naukowe Politechniki Slaskiej. Seria: Chemia. 1988;119(958):380. 6. Walczak J, Filipek E. Reactivity of MoO3 towards Cr2V4O13. Thermochimica Acta. 1988 Oct;133:67–72.
  • 7. Kuriata J, Sadłowski L, Walczak J, Filipek E. Temperature Dependence of the EPR Linewidth of CrVO4. physica status solidi (b). 1987 Jul 1;142(1):K73–7.
  • 8. Walczak J, Filipek E, Tabero P. CrVMoO7 and phase equilibria in the V9Mo6O40-CrVMoO7 system. Thermochimica Acta. 1992 Sep;206:279–84.
  • 9. Walczak J, Filipek E. Studies on the CrVMoO7-Cr2(MoO4)3 system. Thermochimica Acta. 1993 Nov;228:127–30.
  • 10. Walczak J, Rychiowska-Himmel I, Tabero P. Iron(III) tungstate and its modifications. Journal of Materials Science. 1992;27(13):3680–4.
  • 11. Plasova L, Kefeli L. Inorganic Materials. Vol. 3. 1967. 906 p.
  • 12. Baykal A, Kizilyalli M, Kniep R. X-ray powder diffraction and IR study of NaMg (H2O) 2 [BP2O8]· H2O and NH4Mg (H2O) 2 [BP2O8]· H2O. Journal of materials science. 2000;35(18):4621–4626.
  • 13. Gözel G, Kizilyalli M, Kniep R. Characterization of a new calcium ultraphosphate, Ca3 (P5O14) 2. Journal of Solid State Chemistry. 1997;129(2):196–199.
  • 14. Gözel G, Baykal A, Kizilyalli M, Kniep R. Solid-State Synthesis, X-ray Powder Investigation and IR Study of α-Mg3[BPO7]. Journal of the European Ceramic Society. 1998 Dec;18(14):2241–6.
There are 13 citations in total.

Details

Primary Language English
Subjects Chemical Engineering
Journal Section Articles
Authors

Gülşah Çelik Gül

Publication Date January 1, 2018
Submission Date May 22, 2017
Acceptance Date July 16, 2018
Published in Issue Year 2018 Volume: 5 Issue: 2

Cite

Vancouver Çelik Gül G. CrVMoO7: MICROWAVE SYNTHESIS AND STRUCTURAL CHARACTERIZATION. JOTCSA. 2018;5(2):881-4.