Research Article
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E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ

Year 2018, Volume: 57 Issue: 4, 233 - 246, 01.12.2018
https://doi.org/10.30797/madencilik.480060

Abstract

Bu çalışma, alternatif çözücüler kullanarak bakır, altın ve gümüşün geri kazanımı için atık
merkezi işlemci ünitelerinin (CPU) liç süreciyle ilgilidir. Fiziksel ön işlemler (boyut küçültme,
ayıklama) ve hidrometalürjik yöntemler kullanılarak yüksek verimlerle metallerin kazanımı
hedeflenmiştir. Kimyasal liç testleri kapsamında 23 tam faktöriyel tasarım testleri yürütülmüştür.
Metal kazanım verimi üzerine reaktif (I2, H2SO4, NH3) derişimi, oksitleyici (H2O2, (NH4)2S2O8)
derişimi, katı/sıvı oranının etkileri, varyans analizi (ANOVA) ile incelenmiştir, etkin değerlere bağlı
modeller oluşturulmuştur. Metal kazanımlarını arttırmak amacıyla iki aşamalı reaktör liçi testleri
yürütülmüştür. Birinci aşamada H2SO4+H2O2 liçi ile %95,60 bakır, ikinci aşamada I2+H2O2 liçi ile
%99,92 altın, %99,81 gümüş kazanım verimleri elde edilmiştir.

References

  • Akcil, A., Erust, C., Gahan, C.S., Ozgun, M., Sahin, M., Tuncuk, A., 2015. Precious Metal Recovery from Waste Printed Circuit Boards using Cyanide and Non-Cyanide Lixiviants–A Review. Waste Management, 45, 258-271.
  • Akcil, A., 2016. WEEE: Booming for Sustainable Recycling. Waste Management, 57, 1-2.
  • Alzate, A., López, M.E., Serna, C., 2016. Recovery of Gold from Waste Electrical and Electronic Equipment (WEEE) using Ammonium Persulfate. Waste Management, 57, 113-120.
  • Babu, M.N., Sahu, K.K., Pandey, B.D., 2002. Zinc Recovery from Sphalerite Concentrate by Direct Oxidative Leaching with Ammonium, Sodium and Potassium Persulphates. Hydrometallurgy, 64, 119-129.
  • Betts, K, 2008. Producing Usable Materials from E-Waste. Environmental Science and Technology, 42, 6782-6783. Bidini, G., Fantozzi, F., Bartocci, P., Alessandro, B.D., Amico, M.D., Laranci, P., Scozza, E., Zagaroli, M., 2015. Recovery of Precious Metals from Scrap Printed Circuit Boards through Pyrolysis. Journal of Analytical and Applied Pyrolysis, 111, 140–147.
  • Birloaga, I., Michelis, I.D., Ferella, F., Buzatu, M., Vegliò, F., 2013. Study on the Influence of Various Factors in the Hydrometallurgical Processing of Waste Printed Circuit Boards for Copper and Gold Recovery. Waste Management, 33, 935–941.
  • Block, P.A., Brown, R.A., Robinson, D., 2004. Novel Activation Technologies for Sodium Persulfate in situ Chemical Oxidation. In: Proceedings of the 4th International Conference on the Remediation of Chlorinated and Recalcitrant Compounds. Erüst, C., Akcil, A., Gahan, C.S., Tuncuk, A., Deveci, H., 2013. Biohydrometallurgy of Secondary Metal Resources: A Potential Alternative Approach for Metal Recovery. Journal of Chemical Technology and Biotechnology, 88 (12), 2115-2132.
  • Furman, O.S., Teel, A.L., Watts, R.J., 2010. Mechanism of Base Activation of Persulfate. Environmental Science Technology, 44 (16), 6423- 6428. Goosey, M., Kellner, R., 2003. Recycling Technologies for the Treatment of End of Life Printed Circuit Boards (PCBs). Circuit World, 29 (3), 33-37.
  • Goosey, M., 2004. End-of-Life Electronics Legislation — an Industry Perspective. Circuit World, 30, 41-45. Hischier, R., Wager, P., Gauglhofer, J., 2005. Does WEEE Recycling Make Sense from an Environmental Perspective? The Environmental Impacts of the Swiss Take-Back and Recycling Systems for Waste Electrical and Electronic Equipment (WEEE). Environmental Impact Assessment Review, 25, 525-539.
  • Huisman, J., Magalini, F., Kuehr, R., Maurer, C., Ogilvie, S., Poll, J., Delgado, C., Artim, E., Szlezak, J., Stevels, A., 2007. 2008 Review of Directive 2002/96 on Waste Electrical and Electronic Equipment. ENV.G.4/ETU/2006/0032, United Nations University, Bonn, Germany, s. 347.
  • Hyk, W., Kitka, K., 2017. Highly Efficient and Selective Leaching of Silver from Electronic Scrap in the Base-Activated Persulfate – Ammonia System. Waste Management, 60, 601-608. Ji, Z.Y., Zhao, M.Y., Zhao, Y.Y., Liu, J., Peng, J.L., Yuan, J.S., 2017. Lithium Extraction Process on Spinel-Type LiMn2O4 and Characterization based on the Hydrolysis of Sodium Persulfate. Solid State Ionics, 301, 116-124.
  • Kang, H-Y., Schoenung, J., 2005. Electronic Waste Recycling: A Review of U.S. Infrastructure and Technology Options. Resources. Conservation and Recycling, 45 (4), 368-400.
  • Konyratbekova, S.S., Baikonurova, A., Ussoltseva, G.A., Erust, C., Akcil, A., 2015a. Thermodynamic and Kinetic of Iodine–Iodide Leaching in Gold Hydrometallurgy. Transactions of Nonferrous Metals Society of China, 25 (11), 3774-3783.
  • Konyratbekova, S.S., Baikonurova, A., Akcil, A., 2015b. Non-Cyanide Leaching Processes in Gold Hydrometallurgy and Iodine-Iodide Applications: A Review. Mineral Processing and Extractive Metallurgy Review, 36: 198–212.
  • Liang, H., Zhang, Y., Huang, S., Hussain, I., 2013. Oxidative Degradation of Pchloroaniline by Copper Oxidate Activated Persulfate. Chemical Engineering Journal, 218, 384-391.
  • Liu, C.S., Shih, K., Sun, C.X., Wang, F., 2012. Oxidative Degradation of Propachlor by Ferrous and Copper Ion Activated Persulfate”, Science of the Total Environment, 416, 507-512.
  • Lu, Y., Xu, Z., 2017. Recycling Non-Leaching Gold from Gold-Plated Memory Cards: Parameters Optimization, Experimental Verification, and Mechanism Analysis. Journal of Cleaner Production, 162, 1518-1526.
  • Milton, J., Arnold, J,. 1995. Introduction to Probability and Statistics. McGraw-Hill, 505p, NewYork. Minitab. 2004. Statistical Software. Minitab Inc., Deneme sürümü 14.12.0., USA.
  • Montgomery, D. C., 2001. Design and Analysis of Experiments. 5th ed., Wiley, New York, USA. Ozturk, T., 2015. Generation and Management of Electrical–Electronic Waste (E-Waste) in Turkey. Journal of Material Cycles and Waste Management, 17, 411-421.
  • Özensoy, E,. 1982. Teknolojik ve Bilimsel Araştırmalarda Modern Deney Tasarımcılığı ve Optimizasyon Yöntemleri. M.T.A. Enstitüsü Yayınları, 24, Ankara, s. 118.
  • Park, K.H., Mohapatra, D., Reddy, B.R., Nam, C.W., 2007. A Study on the Oxidative Ammonia- Ammonium Sulfate Leaching of a Complex (Cu− Ni−Co−Fe) Matte. Hydrometallurgy, 86 (3−4), 164-171. Reed, W.A., Garnov, Y.A., Rao, L., Nash, K.L., Bond, A.H., 2005. Oxidative Alkaline Leaching of Americium from Simulated High-Level Nuclear Waste Sludges. Separation Science and Technology, 40 (5), 1029-1046.
  • Resmi Gazete. Atık Elektrikli ve Elektronik Eşyaların Kontrolü Yönetmeliği. http://www.resmigazete. gov.tr/eskiler/2012/05/20120522-5.htm, Son erişim tarihi: 25 Aralık 2015.
  • Sahin, M., Akcil, A., Erust, C., Altynbek, S., Gahan, C.S., Tuncuk, A., 2015. A Potential Alternative for Precious Metal Recovery from E-Waste: Iodine Leaching. Separation Science and Technology, 50 (16), 2587-2595.
  • Sahu, S.K., Asselin, E., 2012. Effect of Oxidizing Agents on the Hydrometallurgical Purification of Metallurgical Grade Silicon. Hydrometallurgy, 121-124, 120-125.
  • Syed, S., 2006. A Green Technology for Recovery of Gold from Non-Metallic Secondary Sources. Hydrometallurgy, 82 (1-2), 48-53.
  • Tuncuk, A., Stazi, V., Akcil A., Yazici, E.Y., Deveci, H., 2012. Aqueous Metal Recovery Techniques from E-Scrap: Hydrometallurgy in Recycling. Minerals Engineering, 25, 28-37.
  • USGS, 2001. Obsolete Computers, Gold Mine or High-Tech Trash? – Resource Recovery from Recycling, USGS (US Geological Survey), Fact Sheet, July.
  • Widmer, R., Oswald-Krapf, H., Sinha-Khetriwal, D., Schnellmann, M., Boni, H., 2005. Global Perspectives on E-Waste. Environmental Impact Assessment Review, 25, 436-458.
  • Yazıcı , E., Deveci, H., Alp, I., Akcil, A., Yazıcı, R., 2010. Characterisation of Computer Printed Circuit Boards for Hazardous Properties and Beneficiation Studies. XXV International Mineral Processing Congress (IMPC) Bribane, Qld, Australia, 6 - 10 September, 4009-4015. Yu, J., Williams, E., Ju, M., 2009. Review and Prospects of Recycling Methods for Waste Printed Circuit Boards, Sustainable Systems and Technology. ISSST ‘09. IEEE International Symposium.
  • Zhang, Y., Liu, S., Xie, S., Zeng, X., Li, J., 2012. Current Status on Leaching Precious Metals from Waste Printed Circuit Boards. The 7th International Conference on Waste Management and Technology, Procedia Environmental Sciences, 16, 560-568.
  • Zhong, H., Tian, Y., Yang, Q., Brusseau, M.L., Yang, L., Zeng, G., 2017. Degradation of Landfill Leachate Compounds by Persulfate for Groundwater Remediation. Chemical Engineering Jounal, 307, 399-407. Zhu, C., Fang, G., Dionysiou, D.D., Liu, C., Gao, J., Qin, W., Zhou, D., 2016. Efficient Transformation of DDTs with Persulfate Activation by Zero-Valent Iron Nanoparticles: A Mechanistic Study. Journal of Hazardous Materials, 316, 232-241.
Year 2018, Volume: 57 Issue: 4, 233 - 246, 01.12.2018
https://doi.org/10.30797/madencilik.480060

Abstract

References

  • Akcil, A., Erust, C., Gahan, C.S., Ozgun, M., Sahin, M., Tuncuk, A., 2015. Precious Metal Recovery from Waste Printed Circuit Boards using Cyanide and Non-Cyanide Lixiviants–A Review. Waste Management, 45, 258-271.
  • Akcil, A., 2016. WEEE: Booming for Sustainable Recycling. Waste Management, 57, 1-2.
  • Alzate, A., López, M.E., Serna, C., 2016. Recovery of Gold from Waste Electrical and Electronic Equipment (WEEE) using Ammonium Persulfate. Waste Management, 57, 113-120.
  • Babu, M.N., Sahu, K.K., Pandey, B.D., 2002. Zinc Recovery from Sphalerite Concentrate by Direct Oxidative Leaching with Ammonium, Sodium and Potassium Persulphates. Hydrometallurgy, 64, 119-129.
  • Betts, K, 2008. Producing Usable Materials from E-Waste. Environmental Science and Technology, 42, 6782-6783. Bidini, G., Fantozzi, F., Bartocci, P., Alessandro, B.D., Amico, M.D., Laranci, P., Scozza, E., Zagaroli, M., 2015. Recovery of Precious Metals from Scrap Printed Circuit Boards through Pyrolysis. Journal of Analytical and Applied Pyrolysis, 111, 140–147.
  • Birloaga, I., Michelis, I.D., Ferella, F., Buzatu, M., Vegliò, F., 2013. Study on the Influence of Various Factors in the Hydrometallurgical Processing of Waste Printed Circuit Boards for Copper and Gold Recovery. Waste Management, 33, 935–941.
  • Block, P.A., Brown, R.A., Robinson, D., 2004. Novel Activation Technologies for Sodium Persulfate in situ Chemical Oxidation. In: Proceedings of the 4th International Conference on the Remediation of Chlorinated and Recalcitrant Compounds. Erüst, C., Akcil, A., Gahan, C.S., Tuncuk, A., Deveci, H., 2013. Biohydrometallurgy of Secondary Metal Resources: A Potential Alternative Approach for Metal Recovery. Journal of Chemical Technology and Biotechnology, 88 (12), 2115-2132.
  • Furman, O.S., Teel, A.L., Watts, R.J., 2010. Mechanism of Base Activation of Persulfate. Environmental Science Technology, 44 (16), 6423- 6428. Goosey, M., Kellner, R., 2003. Recycling Technologies for the Treatment of End of Life Printed Circuit Boards (PCBs). Circuit World, 29 (3), 33-37.
  • Goosey, M., 2004. End-of-Life Electronics Legislation — an Industry Perspective. Circuit World, 30, 41-45. Hischier, R., Wager, P., Gauglhofer, J., 2005. Does WEEE Recycling Make Sense from an Environmental Perspective? The Environmental Impacts of the Swiss Take-Back and Recycling Systems for Waste Electrical and Electronic Equipment (WEEE). Environmental Impact Assessment Review, 25, 525-539.
  • Huisman, J., Magalini, F., Kuehr, R., Maurer, C., Ogilvie, S., Poll, J., Delgado, C., Artim, E., Szlezak, J., Stevels, A., 2007. 2008 Review of Directive 2002/96 on Waste Electrical and Electronic Equipment. ENV.G.4/ETU/2006/0032, United Nations University, Bonn, Germany, s. 347.
  • Hyk, W., Kitka, K., 2017. Highly Efficient and Selective Leaching of Silver from Electronic Scrap in the Base-Activated Persulfate – Ammonia System. Waste Management, 60, 601-608. Ji, Z.Y., Zhao, M.Y., Zhao, Y.Y., Liu, J., Peng, J.L., Yuan, J.S., 2017. Lithium Extraction Process on Spinel-Type LiMn2O4 and Characterization based on the Hydrolysis of Sodium Persulfate. Solid State Ionics, 301, 116-124.
  • Kang, H-Y., Schoenung, J., 2005. Electronic Waste Recycling: A Review of U.S. Infrastructure and Technology Options. Resources. Conservation and Recycling, 45 (4), 368-400.
  • Konyratbekova, S.S., Baikonurova, A., Ussoltseva, G.A., Erust, C., Akcil, A., 2015a. Thermodynamic and Kinetic of Iodine–Iodide Leaching in Gold Hydrometallurgy. Transactions of Nonferrous Metals Society of China, 25 (11), 3774-3783.
  • Konyratbekova, S.S., Baikonurova, A., Akcil, A., 2015b. Non-Cyanide Leaching Processes in Gold Hydrometallurgy and Iodine-Iodide Applications: A Review. Mineral Processing and Extractive Metallurgy Review, 36: 198–212.
  • Liang, H., Zhang, Y., Huang, S., Hussain, I., 2013. Oxidative Degradation of Pchloroaniline by Copper Oxidate Activated Persulfate. Chemical Engineering Journal, 218, 384-391.
  • Liu, C.S., Shih, K., Sun, C.X., Wang, F., 2012. Oxidative Degradation of Propachlor by Ferrous and Copper Ion Activated Persulfate”, Science of the Total Environment, 416, 507-512.
  • Lu, Y., Xu, Z., 2017. Recycling Non-Leaching Gold from Gold-Plated Memory Cards: Parameters Optimization, Experimental Verification, and Mechanism Analysis. Journal of Cleaner Production, 162, 1518-1526.
  • Milton, J., Arnold, J,. 1995. Introduction to Probability and Statistics. McGraw-Hill, 505p, NewYork. Minitab. 2004. Statistical Software. Minitab Inc., Deneme sürümü 14.12.0., USA.
  • Montgomery, D. C., 2001. Design and Analysis of Experiments. 5th ed., Wiley, New York, USA. Ozturk, T., 2015. Generation and Management of Electrical–Electronic Waste (E-Waste) in Turkey. Journal of Material Cycles and Waste Management, 17, 411-421.
  • Özensoy, E,. 1982. Teknolojik ve Bilimsel Araştırmalarda Modern Deney Tasarımcılığı ve Optimizasyon Yöntemleri. M.T.A. Enstitüsü Yayınları, 24, Ankara, s. 118.
  • Park, K.H., Mohapatra, D., Reddy, B.R., Nam, C.W., 2007. A Study on the Oxidative Ammonia- Ammonium Sulfate Leaching of a Complex (Cu− Ni−Co−Fe) Matte. Hydrometallurgy, 86 (3−4), 164-171. Reed, W.A., Garnov, Y.A., Rao, L., Nash, K.L., Bond, A.H., 2005. Oxidative Alkaline Leaching of Americium from Simulated High-Level Nuclear Waste Sludges. Separation Science and Technology, 40 (5), 1029-1046.
  • Resmi Gazete. Atık Elektrikli ve Elektronik Eşyaların Kontrolü Yönetmeliği. http://www.resmigazete. gov.tr/eskiler/2012/05/20120522-5.htm, Son erişim tarihi: 25 Aralık 2015.
  • Sahin, M., Akcil, A., Erust, C., Altynbek, S., Gahan, C.S., Tuncuk, A., 2015. A Potential Alternative for Precious Metal Recovery from E-Waste: Iodine Leaching. Separation Science and Technology, 50 (16), 2587-2595.
  • Sahu, S.K., Asselin, E., 2012. Effect of Oxidizing Agents on the Hydrometallurgical Purification of Metallurgical Grade Silicon. Hydrometallurgy, 121-124, 120-125.
  • Syed, S., 2006. A Green Technology for Recovery of Gold from Non-Metallic Secondary Sources. Hydrometallurgy, 82 (1-2), 48-53.
  • Tuncuk, A., Stazi, V., Akcil A., Yazici, E.Y., Deveci, H., 2012. Aqueous Metal Recovery Techniques from E-Scrap: Hydrometallurgy in Recycling. Minerals Engineering, 25, 28-37.
  • USGS, 2001. Obsolete Computers, Gold Mine or High-Tech Trash? – Resource Recovery from Recycling, USGS (US Geological Survey), Fact Sheet, July.
  • Widmer, R., Oswald-Krapf, H., Sinha-Khetriwal, D., Schnellmann, M., Boni, H., 2005. Global Perspectives on E-Waste. Environmental Impact Assessment Review, 25, 436-458.
  • Yazıcı , E., Deveci, H., Alp, I., Akcil, A., Yazıcı, R., 2010. Characterisation of Computer Printed Circuit Boards for Hazardous Properties and Beneficiation Studies. XXV International Mineral Processing Congress (IMPC) Bribane, Qld, Australia, 6 - 10 September, 4009-4015. Yu, J., Williams, E., Ju, M., 2009. Review and Prospects of Recycling Methods for Waste Printed Circuit Boards, Sustainable Systems and Technology. ISSST ‘09. IEEE International Symposium.
  • Zhang, Y., Liu, S., Xie, S., Zeng, X., Li, J., 2012. Current Status on Leaching Precious Metals from Waste Printed Circuit Boards. The 7th International Conference on Waste Management and Technology, Procedia Environmental Sciences, 16, 560-568.
  • Zhong, H., Tian, Y., Yang, Q., Brusseau, M.L., Yang, L., Zeng, G., 2017. Degradation of Landfill Leachate Compounds by Persulfate for Groundwater Remediation. Chemical Engineering Jounal, 307, 399-407. Zhu, C., Fang, G., Dionysiou, D.D., Liu, C., Gao, J., Qin, W., Zhou, D., 2016. Efficient Transformation of DDTs with Persulfate Activation by Zero-Valent Iron Nanoparticles: A Mechanistic Study. Journal of Hazardous Materials, 316, 232-241.
There are 31 citations in total.

Details

Primary Language Turkish
Journal Section Research Article
Authors

Ayşenur Tuncuk 0000-0001-9424-0758

Publication Date December 1, 2018
Submission Date June 7, 2018
Published in Issue Year 2018 Volume: 57 Issue: 4

Cite

APA Tuncuk, A. (2018). E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ. Bilimsel Madencilik Dergisi, 57(4), 233-246. https://doi.org/10.30797/madencilik.480060
AMA Tuncuk A. E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ. Mining. December 2018;57(4):233-246. doi:10.30797/madencilik.480060
Chicago Tuncuk, Ayşenur. “E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ”. Bilimsel Madencilik Dergisi 57, no. 4 (December 2018): 233-46. https://doi.org/10.30797/madencilik.480060.
EndNote Tuncuk A (December 1, 2018) E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ. Bilimsel Madencilik Dergisi 57 4 233–246.
IEEE A. Tuncuk, “E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ”, Mining, vol. 57, no. 4, pp. 233–246, 2018, doi: 10.30797/madencilik.480060.
ISNAD Tuncuk, Ayşenur. “E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ”. Bilimsel Madencilik Dergisi 57/4 (December 2018), 233-246. https://doi.org/10.30797/madencilik.480060.
JAMA Tuncuk A. E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ. Mining. 2018;57:233–246.
MLA Tuncuk, Ayşenur. “E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ”. Bilimsel Madencilik Dergisi, vol. 57, no. 4, 2018, pp. 233-46, doi:10.30797/madencilik.480060.
Vancouver Tuncuk A. E-ATIKLARDAN METAL KAZANIMINDA ÇÖZÜCÜLERİN VE OKSİTLEYİCİLERİN ETKİLERİ. Mining. 2018;57(4):233-46.

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