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Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route

Year 2022, , 1185 - 1189, 01.10.2022
https://doi.org/10.2339/politeknik.824853

Abstract

The paper presents the synthesis and characterization of Copper metal matrix composite reinforced with silica using powder metallurgy route. The 5%wt of silica is reinforced with copper metal as matrix material. 5% wt Magnesium was added as wetting agent as copper shows poor wettability towards silica. The reinforced silica was extracted from agro waste rice husk ash under controlled conditions of sintering temperature and duration of heating from rice husk ash using alkali extraction method. Reflux method was used to extract nanosilica from silica. Silica and the composite were characterized for microstructural studies, elemental composition and surface morphologies using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive X-Ray (EDX) and Transmission Electron Microscopy (TEM). The synthesized copper silica composite was studied for structural, compositional and mechanical properties. The results showed that the copper metal matrix composite reinforced with silica showed improved mechanical behavior and can be used in all such applications where light weight and better mechanical strength from copper metal are expected. As the filler material silica is extracted from green route which partially replaces the expensive metal, this work reports a non-toxic, cost effective, light weight and improved mechanical strength substitute for copper metal applications.

Supporting Institution

UGC-DAE Consortium for Scientific Research, Indore, M.P. India

Project Number

CSR/Acctts/2020-21/326

Thanks

I thank Prof. Dr. Hakan Ates for inviting me the the ICMATSE2020 conference and giving the opportunity to present my work.

References

  • [1] Laad M., Jatti V., “Investigation into the effect of Aluminium powder on mechanical , tribological and Electrical properties of Al-ABSComposites”,WseasTransactions on Applied and Theoritical Mechanics , E-ISSN: 2224-3429, 10, 47-53.
  • [2] Mallik S., N. Ekere, C. Best, R. Bhatti, “Investigation of thermal management materials for automotive electronic control units”., Appl ThermEng, 31: 355-362, (2011).
  • [3] A. Molina, T. Wang, C. Zou, Z. Chen, M. Li, W. Wang, et al. “In situ synthesis of TiB2 particulate reinforced copper matrix composite with a rotating magnetic field”., Mater Des, 65: 280-288, (2015).
  • [4] S. Kumari, A. Kumar, P.R. Sengupta, P.K. Dutta, R.B. Mathur “Improving the mechanical and thermal properties of semi-coke based carbon/copper composites reinforced using carbon nanotubes”., J Adv Mater Lett, 5: 265-271, (2014).
  • [5] R. Zitoune, M. El Mansori, K. Vijayan “Tribo-functional design of double cone drill implications in tool wear during drilling of copper mesh/CFRP/woven ply”Wear, 302: 1560-1567, (2013).
  • [6] M. Yusoff, R. Othman, Z. Hussain “Mechanical alloying and sintering of nanostructured tungsten carbide-reinforced copper composite and its characterization” Mater Des, 32: 3293-3298, (2011).
  • [7] A.A. Thakre, S. Soni “Modeling of burr size in drilling of aluminum silicon carbide composites using response surface methodology”Eng Sci Technol, 19: 1199-1205, (2016).
  • [8] Wąsik, Mateusz &Karwan-Baczewska, Joanna. “Copper Metal Matrix Composites Reinforced by Titanium Nitride Particles”. Key Engineering Materials. 682: 270-275, (2016).
  • [9] R. Sathiskumar, N. Murugan, I. Dinaharan, S.J. Vijay “Fabrication and characterization of Cu/B4c surface dispersion strengthened composite using friction stir processing” ., 59: 83-89, (2014).
  • [10] W.V. Sagar, S.L. Samir, W.R. Amit “Modelling of Cu-Al2O3 metal matrix composite prepared by powder metallurgy route”Int. J. Eng. Adv. Technol., 3: 330-332, (2013).
  • [11] M. Yusoff, R. Othman, Z. Hussain “Mechanical alloying and sintering of nanostructured tungsten carbide-reinforced copper composite and its characterization”Mater. Des., 32: 3293-3298, (2011).
  • [12]Q. Kang, X. He, S. Ren, L. Zhang, M. Wu, C. Guo, W. Cui, X. Qu “Preparation of copper–diamond composites with chromium carbide coatings on diamond particles for heat sink applications”Appl. Therm. Eng., 60: 423-429, (2013).
  • [13] . Zhang, X.H. Qu, X.B. He, B.H. Duan, S.B. Ren, M.L. Qin “Thermo-physical and mechanical properties of high volume fraction SiCp/Cu composites prepared by pressureless infiltration”Mater. Sci. Eng., A, 489: 285-293, (2008).
  • [14] B..M. Girish, B.R. Basawaraj, B.M. Satish, D.R. “SomashElectrical resistivity and mechanical properties of tungsten carbide reinforced copper alloy composites” Int. J. Comput. Mater., 2 (3): 37-42, (2012).
  • [15] V. Aleksandar, R. Viseslava, Z. FatimaFriction and wear properties of copper based composites reinforced with micro and nano-sized Al2O3 particles 8th Int. conf. Tribol., 30th Oct-1st Nov. 2014, Sinaia, Romania, 357-358, (2014).
  • [16] A.A. Thakre, S. Soni “Modeling of burr size in drilling of aluminum silicon carbide composites using response surface methodology”Eng. Sci. Technol., 19: 1199-1205, (2016).
  • [17] I. Dinaharan, N. Murugan, A. Thangarasu “Development of empirical relationships for prediction of mechanical and wear properties of AA6082 aluminum matrix composites produced using friction stir processing”Eng. Sci. Technol., 19: 1132-1144, (2016).
  • [18] M. Laad, “Extraction and Characterization of silica from agro-waste for energy applications”, IEEE International Conference on Energy, Communication, Data Analytics and Soft Computing (ICECDS-2017), 1(V): 233-239.
  • [19] R.W.G.Wyckoff, Am.J.Sci.,1925,9,448-459.
  • [20] B. T. Ferreira, L.J. Silva, T. H. Panzera, J. C. Santos, R. T. Freire, F. “Scarpa,Sisal-glass hybrid composites reinforced with silica microparticles”, Polymer Testing, 74: 57-62, ISSN 0142-9418, 2019.
  • [21] S. Choi, J. Changwoon, B. “Properties of natural rubber composites reinforced with silica or carbon black: influence of cure accelerator content and filler dispersion”. Polymer International, 52: 1382 - 1389, 2003.
  • [22] H.H.Xu,J.B.Quinn, A.A.Giuseppetti, F.C.Eichmiller, E.E.Parry, G.E.Schumacher, “Three-body wear of dental resin composites reinforced with silica-fused whisker”, Dent Mater.2004, 20(3): 220-227.

Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route

Year 2022, , 1185 - 1189, 01.10.2022
https://doi.org/10.2339/politeknik.824853

Abstract

The paper presents the synthesis and characterization of Copper metal matrix composite reinforced with silica using powder metallurgy route. The 5%wt of silica is reinforced with copper metal as matrix material. 5% wt Magnesium was added as wetting agent as copper shows poor wettability towards silica. The reinforced silica was extracted from agro waste rice husk ash under controlled conditions of sintering temperature and duration of heating from rice husk ash using alkali extraction method. Reflux method was used to extract nanosilica from silica. Silica and the composite were characterized for microstructural studies, elemental composition and surface morphologies using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive X-Ray (EDX) and Transmission Electron Microscopy (TEM). The synthesized copper silica composite was studied for structural, compositional and mechanical properties. The results showed that the copper metal matrix composite reinforced with silica showed improved mechanical behavior and can be used in all such applications where light weight and better mechanical strength from copper metal are expected. As the filler material silica is extracted from green route which partially replaces the expensive metal, this work reports a non-toxic, cost effective, light weight and improved mechanical strength substitute for copper metal applications.

Project Number

CSR/Acctts/2020-21/326

References

  • [1] Laad M., Jatti V., “Investigation into the effect of Aluminium powder on mechanical , tribological and Electrical properties of Al-ABSComposites”,WseasTransactions on Applied and Theoritical Mechanics , E-ISSN: 2224-3429, 10, 47-53.
  • [2] Mallik S., N. Ekere, C. Best, R. Bhatti, “Investigation of thermal management materials for automotive electronic control units”., Appl ThermEng, 31: 355-362, (2011).
  • [3] A. Molina, T. Wang, C. Zou, Z. Chen, M. Li, W. Wang, et al. “In situ synthesis of TiB2 particulate reinforced copper matrix composite with a rotating magnetic field”., Mater Des, 65: 280-288, (2015).
  • [4] S. Kumari, A. Kumar, P.R. Sengupta, P.K. Dutta, R.B. Mathur “Improving the mechanical and thermal properties of semi-coke based carbon/copper composites reinforced using carbon nanotubes”., J Adv Mater Lett, 5: 265-271, (2014).
  • [5] R. Zitoune, M. El Mansori, K. Vijayan “Tribo-functional design of double cone drill implications in tool wear during drilling of copper mesh/CFRP/woven ply”Wear, 302: 1560-1567, (2013).
  • [6] M. Yusoff, R. Othman, Z. Hussain “Mechanical alloying and sintering of nanostructured tungsten carbide-reinforced copper composite and its characterization” Mater Des, 32: 3293-3298, (2011).
  • [7] A.A. Thakre, S. Soni “Modeling of burr size in drilling of aluminum silicon carbide composites using response surface methodology”Eng Sci Technol, 19: 1199-1205, (2016).
  • [8] Wąsik, Mateusz &Karwan-Baczewska, Joanna. “Copper Metal Matrix Composites Reinforced by Titanium Nitride Particles”. Key Engineering Materials. 682: 270-275, (2016).
  • [9] R. Sathiskumar, N. Murugan, I. Dinaharan, S.J. Vijay “Fabrication and characterization of Cu/B4c surface dispersion strengthened composite using friction stir processing” ., 59: 83-89, (2014).
  • [10] W.V. Sagar, S.L. Samir, W.R. Amit “Modelling of Cu-Al2O3 metal matrix composite prepared by powder metallurgy route”Int. J. Eng. Adv. Technol., 3: 330-332, (2013).
  • [11] M. Yusoff, R. Othman, Z. Hussain “Mechanical alloying and sintering of nanostructured tungsten carbide-reinforced copper composite and its characterization”Mater. Des., 32: 3293-3298, (2011).
  • [12]Q. Kang, X. He, S. Ren, L. Zhang, M. Wu, C. Guo, W. Cui, X. Qu “Preparation of copper–diamond composites with chromium carbide coatings on diamond particles for heat sink applications”Appl. Therm. Eng., 60: 423-429, (2013).
  • [13] . Zhang, X.H. Qu, X.B. He, B.H. Duan, S.B. Ren, M.L. Qin “Thermo-physical and mechanical properties of high volume fraction SiCp/Cu composites prepared by pressureless infiltration”Mater. Sci. Eng., A, 489: 285-293, (2008).
  • [14] B..M. Girish, B.R. Basawaraj, B.M. Satish, D.R. “SomashElectrical resistivity and mechanical properties of tungsten carbide reinforced copper alloy composites” Int. J. Comput. Mater., 2 (3): 37-42, (2012).
  • [15] V. Aleksandar, R. Viseslava, Z. FatimaFriction and wear properties of copper based composites reinforced with micro and nano-sized Al2O3 particles 8th Int. conf. Tribol., 30th Oct-1st Nov. 2014, Sinaia, Romania, 357-358, (2014).
  • [16] A.A. Thakre, S. Soni “Modeling of burr size in drilling of aluminum silicon carbide composites using response surface methodology”Eng. Sci. Technol., 19: 1199-1205, (2016).
  • [17] I. Dinaharan, N. Murugan, A. Thangarasu “Development of empirical relationships for prediction of mechanical and wear properties of AA6082 aluminum matrix composites produced using friction stir processing”Eng. Sci. Technol., 19: 1132-1144, (2016).
  • [18] M. Laad, “Extraction and Characterization of silica from agro-waste for energy applications”, IEEE International Conference on Energy, Communication, Data Analytics and Soft Computing (ICECDS-2017), 1(V): 233-239.
  • [19] R.W.G.Wyckoff, Am.J.Sci.,1925,9,448-459.
  • [20] B. T. Ferreira, L.J. Silva, T. H. Panzera, J. C. Santos, R. T. Freire, F. “Scarpa,Sisal-glass hybrid composites reinforced with silica microparticles”, Polymer Testing, 74: 57-62, ISSN 0142-9418, 2019.
  • [21] S. Choi, J. Changwoon, B. “Properties of natural rubber composites reinforced with silica or carbon black: influence of cure accelerator content and filler dispersion”. Polymer International, 52: 1382 - 1389, 2003.
  • [22] H.H.Xu,J.B.Quinn, A.A.Giuseppetti, F.C.Eichmiller, E.E.Parry, G.E.Schumacher, “Three-body wear of dental resin composites reinforced with silica-fused whisker”, Dent Mater.2004, 20(3): 220-227.
There are 22 citations in total.

Details

Primary Language English
Subjects Engineering
Journal Section Research Article
Authors

Meena Laad 0000-0003-4857-0670

Project Number CSR/Acctts/2020-21/326
Publication Date October 1, 2022
Submission Date November 12, 2020
Published in Issue Year 2022

Cite

APA Laad, M. (2022). Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route. Politeknik Dergisi, 25(3), 1185-1189. https://doi.org/10.2339/politeknik.824853
AMA Laad M. Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route. Politeknik Dergisi. October 2022;25(3):1185-1189. doi:10.2339/politeknik.824853
Chicago Laad, Meena. “Synthesis and Characterization of Copper Metal Matrix Composite Reinforced With Ceramic Oxide Extracted By The Green Route”. Politeknik Dergisi 25, no. 3 (October 2022): 1185-89. https://doi.org/10.2339/politeknik.824853.
EndNote Laad M (October 1, 2022) Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route. Politeknik Dergisi 25 3 1185–1189.
IEEE M. Laad, “Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route”, Politeknik Dergisi, vol. 25, no. 3, pp. 1185–1189, 2022, doi: 10.2339/politeknik.824853.
ISNAD Laad, Meena. “Synthesis and Characterization of Copper Metal Matrix Composite Reinforced With Ceramic Oxide Extracted By The Green Route”. Politeknik Dergisi 25/3 (October 2022), 1185-1189. https://doi.org/10.2339/politeknik.824853.
JAMA Laad M. Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route. Politeknik Dergisi. 2022;25:1185–1189.
MLA Laad, Meena. “Synthesis and Characterization of Copper Metal Matrix Composite Reinforced With Ceramic Oxide Extracted By The Green Route”. Politeknik Dergisi, vol. 25, no. 3, 2022, pp. 1185-9, doi:10.2339/politeknik.824853.
Vancouver Laad M. Synthesis and Characterization of Copper Metal Matrix Composite Reinforced with Ceramic Oxide Extracted By The Green Route. Politeknik Dergisi. 2022;25(3):1185-9.
 
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