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A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light

Year 2017, Volume: 20 Issue: 1, 25 - 36, 01.03.2017

Meral Dükkancı

Abstract

In this study the oxidation of Bisphenol-A (BPA) was investigated using heterogeneous photo-Fenton-like oxidation under visible light irradiation over iron containing TiO2 catalysts. The catalysts were prepared by the incipient wetness impregnation method with different iron contents (1 and 5 wt%) and characterized by XRD, SEM, FT-IR, nitrogen adsorption, UV-Vis DRS, and ICP-AES measurements. Among the prepared catalysts the 1 wt% iron containing the TiO2 catalyst showed better catalytic activity (with a chemical oxygen demand (COD) reduction of 65.4% at the end of 6h of oxidation) than the other catalysts. The effects of the parameters such as the initial BPA concentration, H2O2 amount, catalyst amount, the pH of the initial BPA solution, and reaction temperature were studied with that catalyst on the heterogeneous photo-Fenton-like oxidation of an aqueous BPA solution. The small amount of iron that leached to the solution and the reusability of the catalyst illustrates that the process is mainly the heterogeneous photo-Fenton-like process, instead of the homogeneous photo-Fenton-like process. The degradation of BPA was described by the first order kinetics with an activation energy of 22.5 kJ/Mol.

Keywords

Photo-Fenton-like Oxidation Bisphenol-A Fe/TiO2 Catalysts

References

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A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light

Year 2017, Volume: 20 Issue: 1, 25 - 36, 01.03.2017

Meral Dükkancı

Abstract

In this study the oxidation of Bisphenol-A (BPA) was investigated using heterogeneous photo-Fenton-like oxidation under visible light irradiation over iron containing TiO2 catalysts. The catalysts were prepared by the incipient wetness impregnation method with different iron contents (1 and 5 wt%) and characterized by XRD, SEM, FT-IR, nitrogen adsorption, UV-Vis DRS, and ICP-AES measurements. Among the prepared catalysts the 1 wt% iron containing the TiO2 catalyst showed better catalytic activity (with a chemical oxygen demand (COD) reduction of 65.4% at the end of 6h of oxidation) than the other catalysts. The effects of the parameters such as the initial BPA concentration, H2O2 amount, catalyst amount, the pH of the initial BPA solution, and reaction temperature were studied with that catalyst on the heterogeneous photo-Fenton-like oxidation of an aqueous BPA solution. The small amount of iron that leached to the solution and the reusability of the catalyst illustrates that the process is mainly the heterogeneous photo-Fenton-like process, instead of the homogeneous photo-Fenton-like process. The degradation of BPA was described by the first order kinetics with an activation energy of 22.5 kJ/Mol.

Keywords

Photo-Fenton-like Oxidation Bisphenol-A Fe/TiO2 Catalysts

References

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  • 2. Er B. and Sarımehmetoğlu B., “Evaluation of presence of Bisphenol-A in foods”, Vet. Hekim Der., 82: 69-74, (2011).
  • 3. Zhang K., Gao N., Deng Y., Lin T.F., Ma Y., Li L. and Sui M., “Degradation of Bisphnol-A using ultrasonic irradiation assisted by low-concentration hydrogen peroxide”, J. Environ. Sci., 23: 31-36, (2011).
  • 4. Gültekin I. and İnce N.H., “Ultrasonic destruction of Bisphenol-A: The operating parameters”, Ultrason. Sonochem., 15: 524-529, (2008).
  • 5. Torres R.A., Petrier C., Combet E., Carrıer M. And Pulgarın C., “Ultrasonic cavitation applied to the treatment of Bisphenol A. Effect of sonochemical parameters and analysis of BPA by-products”, Ultrason. Sonochem., 15: 605-611, (2008).
  • 6. Inoue M., Masuda Y., Okada F., Sakurai A., Takahashi I. and Sakakibara, M., “Degradation of Bisphenol A using sonochemical reactions”, Water Res., 42: 1379-1386, (2008).
  • 7. Guo Z. and Feng R., “Ultrasonic irradiation-induced degradation of low-concentration Bisphenol A in aqueous solution”, J. Hazard. Mater., 163: 855-860, (2009).
  • 8. Petrier C., Torres-Palma R., Combet E., Sarantakos G., Baup S. and Pulgarın, C., “Enhanced sonochemical degradation of Bisphenol-A by biocarbonate ions”, Ultrason. Sonochem., 17: 111-115, (2010).
  • 9. Son Y., Lım M., Khım J., Kım L.H. and Ashokkumar, M., “Comparison of calorimetric energy and cavitation energy for the removal of bisphenol-A: The effects of frequency and liquid height”, Chem. Eng. J., 183: 39-45 (2012).
  • 10. Torres R.A., Abdelmalek F., Combet E., Petrıer C. and Pulgarin, C., “A Comparative Study of Ultrasonic Cavitation and Fenton’s Reagent for Bisphenol A Degradation in Deionized and Natural Waters”, J. Hazard. Mater., 146: 546-551, (2007).
  • 11. Ioan I., Wılson S., Lundanes E. And Neculai, A., “Comparison of Fenton and sono-Fenton Bisphenol A degradation”, J. Hazard. Mater., 142: 559-563, (2007).
  • 12. Mohapatra D.P., Brar S.K., Tyagı, R.D. and Surampallı R.Y., “Concominant degradation of Bisphenol A during ultrasonication and Fenton oxidation and production of biofertilizer from wastewater sludge”, Ultrason. Sonochem., 18: 1018-1027, (2011).
  • 13. Huang R., Fang Z., Yan X. and Cheng, W., “Heterogeneous sono-Fenton catalytic degradation of Bisphenol A by Fe3O4 magnetic nanoparticles under neutral condition”, Chem. Eng. J., 197: 242-249, (2012).
  • 14. Katsumata H., Kawabe S., Kaneco S., Suzuki T. and Ohta, K., “Degradation of Bisphenol A in water by the Photo-Fenton reaction”, J. Photoch. Photobio. A., 162: 297-305, (2004).
  • 15. Lin K., Ding J., Wang H., Huang X. and Gan J., “Goethite-Mediated transformation of Bisphenol A”, Chemosphere, 89: 789-795, (2012).
  • 16. Zhou D., Wu F., Deng N. and Xıang, W., “Photooxidation of Bisphenol A (BPA) in water in the presence of ferric and carboxylate salts”, Water Res., 38: 4107-4116, (2004).
  • 17. Neamtu M. and Frımmel F.H., “Degradation of endocrine disrupting Bisphenol A by 254 nm irradiation in different water matrices and effect on yeast celss”, Water Res., 40: 3745-3750, (2006).
  • 18. Ohko Y., Ando I., Chısa N., Tatsuma T., Yamamura T., Nakashıma T., Kubota Y. and Fujıshıma A., “Degradation of Bisphenol A in water by TiO2 photocatalyst”, Environ. Sci. Technol., 35: 2365-2368, (2001).
  • 19. Chiang K., Lım T.M., Tsen L. and Lee, C.C. “Photocatalytic degradation and mineralization of Bisphenol A by TiO2 and platinized TiO2”, Appl Catal A-Gen., 261: 225-237, (2004).
  • 20. Wang G., Wu F., Zhang X., Luo M. and Deng N., “Enhanced TiO2 photocatalytic degradation of Bisphenol A by β-cyclodextrin in suspended solutions”, J. Photoch. Photobio. A., 179: 49-56, (2006).
  • 21. Tsai W.T., Lee M.K. Su T.Y. and Chang Y.M., “Photodegradation of Bisphenol A in a batch TiO2 suspension reactor”. J. Hazard. Mater., 168: 269-275, (2009).
  • 22. Wang R., Ren D., Xıa S., Zhang Y. and Zhao, J., “Photocatalytic degradation of Bisphenol A (BPA) using immobilized TiO2 and UV illumination in a horizontal circulating bed photocatalytic reactor (HCBPR)”, J. Hazard. Mater., 169: 926-932, (2009).
  • 23. Gao B., Lim T.M., Subagio D.P. and Lim T., “Zr-doped TiO2 for enhanced photocatalytic degradation of Bisphenol A”., Appl Catal A-Gen., 375: 107-115, (2010).
  • 24. Kuo C., Wu C. and Lin H., “Photocatalytic degradation of Bisphenol A in a visible light/TiO2 system”, Desalination, 256: 37-42, (2010).
  • 25. Wan X. and Lim, T., “Solvothermal synthesis of C-N codoped TiO2 and photocatalytic evaluation for Bisphenol A degradation using a visible-light irradiated LED photoreactor”, Appl. Catal. B-Environ., 100: 355-364, (2010).
  • 26. Qing Z., Jınhua L., Hongchong C., Quanpeng C., Baoxue Z., Shuchuan S. and Weımın, C., “Characterization and mechanism of the photoelectrocatalytic oxidation of organic pollutants in a thin-layer reactor”, Chinese J. Catal., 32: 1357-1363, (2011).
  • 27.Yang J., Dai J. and Li, J., “Synthesis, characterization and degradation of Bisphenol A using Pr, N co-doped TiO2 with highly visible light activity”, Appl. Surf. Sci., 257: 8965-8973, (2011).
  • 28. Li F.B., Lı X.Z., Lıu C.S. and Lıu, T.X., “Effect of alumina on photocatalytic activity of iron oxides for Bisphenol A degradation”, J. Hazard. Mater., 149: 199-207, (2007).
  • 29. Wang C., Zhu L., Song C., Shan G. and Chen P., “Characterization of photocatalyst Bi3.84W0.16O6.24 and its photodegradation on Bisphenol A under simulated solar light irradiation”, Appl. Catal. B-Environ., 105: 229-236, (2011).
  • 30. Wang C., Zhu L., Wei M., Chen P. and Shan, G., “Photolytic reaction mechanism and impacts of coexisting substances on photodegradation of Bisphenol A by Bi2WO6 in water”, Water Res., 46: 845-853, (2012).
  • 31. Wang C., Zhu L., Chang C., Fu Y. and Chu X., “Preparation of magnetic composite photocatalyst Bi2WO6/CoFe2O4 by two-step hydrothermal methos and its photocatalytic degradation”, Catal. Commun., 37: 92-95, (2013).
  • 32. Katsumata H., Taniguchi M., Kaneco S. and Suzuki T., “Photocatalytic degradation of Bisphenol A by Ag3PO4 under visible light”, Catal. Commun., 34: 30-34, (2013).
  • 33. Yang X., Tian P., Zhang C., Deng Y., Xu J., Gong J. and Han Y., “Au/Carbon as Fenton-like catalysts for oxidative degradation of Bisphenol A”, Appl. Catal. B-Environ., 134-135: 145-152, (2013).
  • 34.Irmak S., Erbatur O. and Akgerman, A., “Degradation of 17 β-estradiol and Bisphenol A in aqueous medium by using ozone and ozone/UV techniques”, J. Hazard. Mater., B126: 54-62, (2005).
  • 35. Deborde M., Rabouan S., Mazellier P., Duguet J.P. and Legube, B., “ Oxidation of Bisphenol A by ozone in aqueous solution”, Water Res., 42: 4299-4308, (2008).
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Details

Primary Language English
Subjects Engineering
Journal Section Research Article
Authors

Meral Dükkancı This is me

Publication Date March 1, 2017
Submission Date February 18, 2016
Published in Issue Year 2017 Volume: 20 Issue: 1

Cite

APA Dükkancı, M. (2017). A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light. Politeknik Dergisi, 20(1), 25-36.
AMA Dükkancı M. A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light. Politeknik Dergisi. March 2017;20(1):25-36.
Chicago Dükkancı, Meral. “A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light”. Politeknik Dergisi 20, no. 1 (March 2017): 25-36.
EndNote Dükkancı M (March 1, 2017) A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light. Politeknik Dergisi 20 1 25–36.
IEEE M. Dükkancı, “A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light”, Politeknik Dergisi, vol. 20, no. 1, pp. 25–36, 2017.
ISNAD Dükkancı, Meral. “A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light”. Politeknik Dergisi 20/1 (March 2017), 25-36.
JAMA Dükkancı M. A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light. Politeknik Dergisi. 2017;20:25–36.
MLA Dükkancı, Meral. “A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light”. Politeknik Dergisi, vol. 20, no. 1, 2017, pp. 25-36.
Vancouver Dükkancı M. A Parametric Study on the Heterogeneous Photo-Fenton-Like Oxidation of Bisphenol-A over an Fe/TiO2 Catalyst under Visible Light. Politeknik Dergisi. 2017;20(1):25-36.

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