A new glassy carbon surface covered with 1-(2-benzothiazolyl)-3-methyl pyrazol-5-one and its characterization

Abstract

1- (2-benzotiazolil) -3-metil 5-pirazolon (B3MP), susuz ortamda camsı karbon (GC) elektrot yüzeyine elektrokimyasal olarak kaplandı. B3MP filminin özellikleri dönüşümlü voltametri (CV) ve elektrokimyasal impedans spektroskopisi (EIS) ile araştırıldı. Transfer olan elektron sayısı hesaplandı ve GC elektrot yüzeyine B3MP molekülünün elektrokimyasal yükseltgenme yoluyla  modifikasyon mekanizması önerildi.

Keywords

• Electrochemical modification,Impedance spectroscopy,Glassy carbon electrode

References

1. K. Brune, “The early history of non-opioid analgesics,” Acute Pain, vol. 1, pp. 33–40, 1997.
2. S. M. Sondhi, S. Kumar, N. Kumar, P. Roy, “Synthesis anti-inflammatory and anticancer activity evaluation of some pyrazole and oxadiazole derivatives,” Medicinal Chemistry Research, vol. 21, no. 10, pp. 3043–3052, 2012.
3. A. Zaoui, L. Hammal, N. Bennamane, S. Merabtene, B. Nedjar-Kolli, “A catalytic method for the synthesis of pyrazolone derivatives using heteropolyacids and study of the antibacterial activity,” International Journal of Pharmaceutical, Chemical and Biological Sciences,” vol. 3, no. 3, pp. 732–737, 2013.
4. E. Bagdatli, E. Altuntas, U. Sayin, “Synthesis and structural characterization of new oxovanadium(IV) complexes derived from azo-5-pyrazolone with prospective medical importance,” Journal of Molecular Structure, vol. 1127, pp. 653–661, 2017.
5. N.V. Trofimov, N.N. Nekhaer, N.A. Kanaev, A.I. Busev, “Pyrazolone derivatives as analytical redox-reagents. Determination of cerium and hydrogen peroxide with bis-(1- phenyl-3-methylpyrazolone-5),” Zhurnal Analiticheskoj Khimii, vol. 37, pp.1445–1451, 1982.
6. E. Aktan, B. Çatıkkaş, “Infrared and Raman spectra, DFT investigation of the tautomerism, conformational equilibrium, structure and vibrational assignment of 1-(2-benzothiazolyl)- 3-methyl pyrazol-5-one,” Vibrational Spectroscopy, vol. 67, pp. 92– 100, 2013.
7. T. Ito, C. Goto, K. Noguchi, “Lanthanoid ion-selective solvent polymeric membrane electrode based on 1-phenyl-3-methyl-4-octadecanoyl-5-pyrazolone,” Analytica Chimica Acta, vol. 443, pp. 41–51, 2001.
8. V. Kumar Gupta, S. Jain, S. Chandra, “Chemical sensor for lanthanum(III) determination using aza-crown as ionophore in poly(vinyl chloride) matrix,” Analytica Chimica Acta, vol. 486, pp. 199–207, 2003.

9. D. Morales-Martínez, F. J. González, “Reversible reorganization of alkyl ester groups grafted on glassy carbon electrode: Induction by a redox probe,” Electrochemistry Communications, vol. 62, pp. 21–23, 2016.
10. V. Georgakilas, M. Otyepka, A. B. Bourlinos, V. Chandra, N. Kim, K. C. Kemp, P. Hobza, R. Zboril, K. S. Kim, “Functionalization of graphene: Covalent and non-covalent approaches, derivatives and applications,” Chemical Reviews, vol. 112, pp. 6156−6214, 2012.
11. L. Arrue, T. Barra, M. B. Camarada, X. Zarate, E. Schott, “Electrochemical and theoretical characterization of the electro-oxidation of dimethoxycurcumin,” Chemical Physics Letters, vol. 677, pp. 35–40, 2017.
12. E. Laviron, “Adsorption, autoinhibition and autocatalysis in polarography and in linear potential sweep voltammetry,” Journal of Electroanalytical Chemistry and Interfacial Electrochemistry, vol. 52, no. 3, pp. 355-393, 1974.
13. S. M. Ghoreishi, M. Behpour, M. Delshad, A. Khoobi, “Electrochemical determination of tyrosine in the presence of uric acid at a carbon paste electrode modified with multi-walled carbon nanotubes enhanced by sodium dodecyl sulfate,” Central European Journal of Chemistry, vol. 10, 1824–1829, 2012.
14. S. Bouden, G. Trippé-Allard, J. Ghilane, H. Randriamahazaka, “Electrochemical immobilization of redox active molecule based ionic liquid,” Electrochemistry Communications, vol. 58, pp. 65–68, 2015.
15. D. Uzun, H. Arslan, A. Balaban Gündüzalp, E. Hasdemir, “Preparation of modified glassy carbon surface with N-(1-H-indole-3yl) methylene thiazole-2-amine and its characterization,” Surface & Coatings Technology, vol. 239, pp. 108–115, 2014.
16. R. S. Deinhammer, M. Ho, J. W. Anderegg, M. D. Porter, “Electrochemical oxidation of amine-containing compounds: A route to the surface modification of glassy carbon electrodes,” Langmuir, vol. 10, pp. 1306–1313, 1994.
17. Y. Li, X. Lin, “Simultaneous electroanalysis of dopamine, ascorbic acid and uric acid by poly (vinyl alcohol) covalently modified glassy carbon electrode,” Sensors and Actuators B, vol. 115, pp. 134–139, 2006.
18. V. K. Gupta, M. L. Yolac, N. Atar, A. Osman Solak, L. Uzun, Z. Üstündağ, “Electrochemically modified sulfisoxazole nanofilm on glassy carbon for determination of cadmium(II) in water samples,” Electrochimica Acta, vol. 105, pp. 149– 156, 2013.
19. H. Chen, J.-H. Jiang, Y. Huang, T. Deng, J.-S. Li, G.-L. Shen, R.-Q. Yu, “An electrochemical impedance immunosensor with signal amplification based on Au-colloid labeled antibody complex,” Sensors and Actuators B, vol. 117, pp. 211–218, 2006.
20. M. Khoshroo, A. A. Rostami, “Characterization of the organic molecules deposited at gold surface by the electrochemical reaction of diazonium salts,” Journal of Electroanalytical Chemistry, vol. 647, pp. 117–122, 2010.
21. R. Zhang, G.-D. Jin, D. Chen, X.-Y. Hu, “Simultaneous electrochemical determination of dopamine, ascorbic acid and uric acid using poly(acid chrome blue K) modified glassy carbon electrode,” Sensors and Actuators B, vol. 138, pp. 174–181, 2009.