SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES

A. Seyhun Kıpçak; Tuğba İbroşka; Nurcan Tuğrul; Emek Möröydor Derun; Sabriye Pişkin

SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES

Abstract

The 72% of the World boron reserves are in Turkey. The biggest portion of boron reserves leads the boron studies. Due to its important properties boron usage areas are extending. In this study the chlorine containing magnesium borate synthesis by solid-state method is investigated. The reaction temperatures were set between 500°C - 700°C. Magnesium chloride hexahydrate (MgCl2.6H2O) used as chlorine and magnesium source, magnesium oxide (MgO) used as magnesium source and boric acid (H3BO3) used as boron source. The effect on the synthesis by the molar ratio change of the raw materials was investigated. Synthesized minerals characterization analyses were done by the techniques of X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR). From the results of this study the chlorine containing magnesium borate of boracite (Mg3B7O13Cl) was obtained. The side products of dehydrated magnesium borates namely magnesium borate (MgB4O7) and suanite (Mg2B2O5) were also formed. The formation of boracite was started at the reaction temperature of 500°C and the temperature increase effected the Mg3B7O13Cl formation positively.

Keywords

References

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Details

Primary Language

English

Subjects

-

Journal Section

Research Article

Authors

A. Seyhun Kıpçak This is me
Türkiye

Tuğba İbroşka This is me
Türkiye

Nurcan Tuğrul This is me
Türkiye

Emek Möröydor Derun This is me
Türkiye

Sabriye Pişkin This is me
Türkiye

Publication Date

June 1, 2014

Submission Date

December 29, 2013

Acceptance Date

March 4, 2014

Published in Issue

Year 2014 Volume: 32 Number: 2

IZ

https://izlik.org/JA33XH37AW

Cite

RIS / Bibtex

APA

Kıpçak, A. S., İbroşka, T., Tuğrul, N., Möröydor Derun, E., & Pişkin, S. (2014). SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES. Sigma Journal of Engineering and Natural Sciences, 32(2), 201-210. https://izlik.org/JA33XH37AW

AMA

1.Kıpçak AS, İbroşka T, Tuğrul N, Möröydor Derun E, Pişkin S. SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES. SIGMA. 2014;32(2):201-210. https://izlik.org/JA33XH37AW

Chicago

Kıpçak, A. Seyhun, Tuğba İbroşka, Nurcan Tuğrul, Emek Möröydor Derun, and Sabriye Pişkin. 2014. “SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES”. Sigma Journal of Engineering and Natural Sciences 32 (2): 201-10. https://izlik.org/JA33XH37AW.

EndNote

Kıpçak AS, İbroşka T, Tuğrul N, Möröydor Derun E, Pişkin S (June 1, 2014) SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES. Sigma Journal of Engineering and Natural Sciences 32 2 201–210.

IEEE

[1]A. S. Kıpçak, T. İbroşka, N. Tuğrul, E. Möröydor Derun, and S. Pişkin, “SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES”, SIGMA, vol. 32, no. 2, pp. 201–210, June 2014, [Online]. Available: https://izlik.org/JA33XH37AW

ISNAD

Kıpçak, A. Seyhun - İbroşka, Tuğba - Tuğrul, Nurcan - Möröydor Derun, Emek - Pişkin, Sabriye. “SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES”. Sigma Journal of Engineering and Natural Sciences 32/2 (June 1, 2014): 201-210. https://izlik.org/JA33XH37AW.

JAMA

1.Kıpçak AS, İbroşka T, Tuğrul N, Möröydor Derun E, Pişkin S. SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES. SIGMA. 2014;32:201–210.

MLA

Kıpçak, A. Seyhun, et al. “SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES”. Sigma Journal of Engineering and Natural Sciences, vol. 32, no. 2, June 2014, pp. 201-10, https://izlik.org/JA33XH37AW.

Vancouver

1.A. Seyhun Kıpçak, Tuğba İbroşka, Nurcan Tuğrul, Emek Möröydor Derun, Sabriye Pişkin. SOLID STATE SYNTHESIS OF CHLORINE CONTAINING DEHYDRATED MAGNESIUM BORATES. SIGMA [Internet]. 2014 Jun. 1;32(2):201-10. Available from: https://izlik.org/JA33XH37AW