TR
EN
Tripodal Schiff Bazlı Ligandın Sentezi ve Üç Merkezli Geçiş Metal Komplekslerinin İncelenmesi
Abstract
Bu çalışmada çıkış maddesi olarak siyanür klorür kullanıldı. Siyanür klorür, sodyum karbonat ve benzenli ortamda 4-hidroksibenzaldehit ile reaksiyona girerek, 2,4,6-tris(p-formilfenoksi)-1,3,5-triazin (TRIPOD) elde edildi. Daha Sonra, Tripodal Schiff bazı literatüre göre TRIPOD ile aminin, kenetleme reaksiyonu ile sentezlendi. Tripodal Schiff bazının sentezi için, 2-(aminometil)piridin kullanıldı. Etanollü ortamda çözülmüş, 2,4,6-tns(2-piridilimino-4-formllfenoksl)-1,3,5-triazin ligandına, etanolde çözülmüş olan Ni(ll), Co(ll) ve Cu(ll) asetat tuzları ilave edilerek renkli kompleksler elde edildi. Sonuç olarak, tripodal Schiff baz ligandı ve kompleksleri izole edildi ve elementel analiz, FT-IR, 1H NMR ve manyetik susseptibilite ile yapıları aydınlatıldı.
Keywords
Details
Primary Language
English
Subjects
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Journal Section
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Publication Date
December 1, 2007
Submission Date
December 1, 2007
Acceptance Date
-
Published in Issue
Year 2007 Volume: 2 Number: 29
APA
Koç, Z. E., & Uçan, H. İ. (2007). Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes. Selcuk University Journal of Science Faculty, 2(29), 135-139. https://izlik.org/JA55JU62HC
AMA
1.Koç ZE, Uçan Hİ. Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes. Selcuk University Journal of Science Faculty. 2007;2(29):135-139. https://izlik.org/JA55JU62HC
Chicago
Koç, Ziya Erdem, and H. İsmet Uçan. 2007. “Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes”. Selcuk University Journal of Science Faculty 2 (29): 135-39. https://izlik.org/JA55JU62HC.
EndNote
Koç ZE, Uçan Hİ (December 1, 2007) Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes. Selcuk University Journal of Science Faculty 2 29 135–139.
IEEE
[1]Z. E. Koç and H. İ. Uçan, “Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes”, Selcuk University Journal of Science Faculty, vol. 2, no. 29, pp. 135–139, Dec. 2007, [Online]. Available: https://izlik.org/JA55JU62HC
ISNAD
Koç, Ziya Erdem - Uçan, H. İsmet. “Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes”. Selcuk University Journal of Science Faculty 2/29 (December 1, 2007): 135-139. https://izlik.org/JA55JU62HC.
JAMA
1.Koç ZE, Uçan Hİ. Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes. Selcuk University Journal of Science Faculty. 2007;2:135–139.
MLA
Koç, Ziya Erdem, and H. İsmet Uçan. “Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes”. Selcuk University Journal of Science Faculty, vol. 2, no. 29, Dec. 2007, pp. 135-9, https://izlik.org/JA55JU62HC.
Vancouver
1.Ziya Erdem Koç, H. İsmet Uçan. Synthesis of Tripodal Schiff Base Ligand and Investigation of Its Trinuclear Transition Metal Complexes. Selcuk University Journal of Science Faculty [Internet]. 2007 Dec. 1;2(29):135-9. Available from: https://izlik.org/JA55JU62HC
