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Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy

Year 2025, Volume: 14 Issue: 3, 165 - 171, 26.09.2025
https://doi.org/10.46810/tdfd.1738630

Abstract

The machinability of copper-nickel-based alloys, such as Cupral 4M, is known to be quite challenging in the manufacturing industry due to their high thermal conductivity, sticky chip formation, and susceptibility to tool wear. Conventional cooling and lubrication methods are insufficient for improving the machinability of these materials, resulting in a negative impact on machinability metrics such as production quality and tool life. In this study, the effects of adding 0.5 wt% CNC nanopowder to the MQL fluid on the milling process of Cupral 4M material were investigated. The experiments were conducted under two different cutting speeds (125-150 m/min), two different feed rates (0.04-0.06 mm/rev), and three different cooling/lubrication conditions (dry, pure MQL, and CNC nanoparticle MQL). As a result of the experiment, surface roughness, tool wear, and energy consumption were measured, and the obtained data were compared. The addition of CNC nanopowder to MQL fluid provided significant improvements (up to 66% in surface quality, 39% in tool wear, and 10% in energy consumption) in all three results compared to dry and MQL conditions. These results indicate that the addition of CNC nanoparticles has a friction-reducing and tribofilm-protecting effect in the cutting zone. This study fills one of the essential gaps in the literature on improving the sustainable millability of Cupral 4M material and reveals the effectiveness of nanoparticle-added MQL fluids.

References

  • Uzun M, Usca ÜA, Kuntoglu M, Gupta MK. Influence of tool path strategies on machining time, tool wear, and surface roughness during milling of AISI X210Cr12 steel. Int J Adv Manuf Tech. 2022;119(3-4):2709-20.
  • Kar BC, Panda A, Kumar R, Sahoo AK, Mishra RR. Research trends in high speed milling of metal alloys: A short review. Mater Today-Proc. 2020;26:2657-62.
  • Polo S, Rubio EM, Marín MM, de Pipaón JMS. Evolution and Latest Trends in Cooling and Lubrication Techniques for Sustainable Machining: A Systematic Review. Processes. 2025;13(2).
  • Sap S. Understanding the Machinability and Energy Consumption of Al-Based Hybrid Composites under Sustainable Conditions. Lubricants. 2023;11(3).
  • Sap E, Usca ÜA, Degirmenci Ü, Sap S, Uzun M. Evaluation of Machinability and Energy Consumption of CK45 Steel Using Synthetic-Based Nanofluid and Minimum Quantity Lubrication Cutting Fluid. Metals-Basel. 2025;15(1).
  • Sap E, Usca ÜA, Uzun M. Machining and optimization of reinforced copper composites using different cooling-lubrication conditions. J Braz Soc Mech Sci. 2022;44(9).
  • Sap E, Usca ÜA, Sap S, Polat H, Giasin K, Kalyoncu M. Understanding the effects of machinability properties of Incoloy 800 superalloy under different machining conditions using artificial intelligence methods. Mater Today Commun. 2024;38.
  • Sap S, Acar E, Degirmenci U, Usca UA, Memis S, Sener R. Machinability of different Cu-Gr composites in milling: Performance parameters prediction via machine learning models. Expert Syst Appl. 2025;272.
  • Dogan MA, Yazman S, Gemi L, Yildiz M, Yapici A. A review on drilling of FML stacks with conventional and unconventional processing methods under different conditions. Compos Struct. 2022;297.
  • Dambatta YS, Li CH, Yang M, Beikai LI, Gao T, Liu MZ, et al. Grinding with minimum quantity lubrication: a comparative assessment. Int J Adv Manuf Tech. 2023;128(3-4):955-1014.
  • Sap E, Usca ÜA, Sap S. Impacts of Environmentally Friendly Milling of Inconel-800 Superalloy on Machinability Parameters and Energy Consumption. Int J Pr Eng Man-Gt. 2024;11(3):781-97.
  • Usca UA, Sap S, Uzun M, Degirmenci U. Assessment of the machinability and energy consumption characteristics of Cu-6Gr hybrid composites under sustainable operating. J Braz Soc Mech Sci. 2024;46(4).
  • Degirmenci Ü, Usca ÜA, Sap S. Machining characterization and optimization under different cooling/lubrication conditions of Al-4Gr hybrid composites fabricated by vacuum sintering. Vacuum. 2023;208.
  • Chinchanikar S, Kore SS, Hujare P. A review on nanofluids in minimum quantity lubrication machining. J Manuf Process. 2021;68:56-70.
  • Bai XF, Li CH, Dong L, Yin QA. Experimental evaluation of the lubrication performances of different nanofluids for minimum quantity lubrication (MQL) in milling Ti-6Al-4V. Int J Adv Manuf Tech. 2019;101(9-12):2621-32.
  • Abellán-Nebot JV, Ameen KH, Khan AM, Mondragón R. Application of Hybrid Nanofluids in MQL Assisted Machining Operations: Exploring Synergies and Establishing Guidelines. Int J Pr Eng Man-Gt. 2025;12(2):657-89.
  • Zhang YB, Li CH, Jia DZ, Li BK, Wang YG, Yang M, et al. Experimental study on the effect of nanoparticle concentration on the lubricating property of nanofluids for MQL grinding of Ni-based alloy. J Mater Process Tech. 2016;232:100-15.
  • Günay M, Korkmaz ME. Understanding the Relationship between Surface Quality and Chip Morphology under Sustainable Cutting Environments. Materials. 2024;17(8).
  • Pal A, Chatha SS, Sidhu HS. Tribological characteristics and drilling performance of nano-MoS-enhanced vegetable oil-based cutting fluid using eco-friendly MQL technique in drilling of AISI 321 stainless steel. J Braz Soc Mech Sci. 2021;43(4).
  • Wang Y, Liu CF. State-of-the-art on minimum quantity lubrication in green machining. J Clean Prod. 2023;429.
  • Usca UA. The Effect of Cellulose Nanocrystal-Based Nanofluid on Milling Performance: An Investigation of Dillimax 690T. Polymers-Basel. 2023;15(23).
  • Şap S. Effects on Machinability of Minimum Quantity Lubrication Strategy during Milling of ST52 Steel. Türk Doğa ve Fen Dergisi. 2023;12(1):82-90.
  • Yildirim ÇV. Investigation of hard turning performance of eco-friendly cooling strategies: Cryogenic cooling and nanofluid based MQL. Tribol Int. 2020;144.
  • Abellán-Nebot JV, Pastor CV, Siller HR. A Review of the Factors Influencing Surface Roughness in Machining and Their Impact on Sustainability. Sustainability-Basel. 2024;16(5).
  • Liao ZR, la Monaca A, Murray J, Speidel A, Ushmaev D, Clare A, et al. Surface integrity in metal machining - Part I: Fundamentals of surface characteristics and formation mechanisms. Int J Mach Tool Manu. 2021;162.
  • Zerooglu T, Degirmenci Ü, Sap S. A Study on the Machinability and Environmental Effects of Milling AISI 5140 Steel in Sustainable Cutting Environments. Machines. 2024;12(7).
  • Sap S, Usca A, Tarih YS, Yar A, Kuntoglu M, Gupta MK. Novel Use of Cellulose Based Biodegradable Nano Crystals in the Machining of PPS Composites: An Approach Towards Green Machining. Int J Pr Eng Man-Gt. 2024;11(1):1-19.
  • Sap S. Machining and Energy Aspect Assessment with Sustainable Cutting Fluid Strategies of Al-12Si Based Hybrid Composites. Int J Pr Eng Man-Gt. 2024;11(1):33-53.
  • Salur E. Understandings the tribological mechanism of Inconel 718 alloy machined under different cooling/lubrication conditions. Tribol Int. 2022;174.
  • Hsu SM, Shen MC, Ruff AW. Wear prediction for metals. Tribol Int. 1997;30(5):377-83.
  • Mughal K, Mughal MP, Farooq MU, Anwar S, Ammarullah MI. Using Nano-Fluids Minimum Quantity Lubrication (NF-MQL) to Improve Tool Wear Characteristics for Efficient Machining of CFRP/Ti6Al4V Aeronautical Structural Composite. Processes. 2023;11(5).
  • Dağılgan G. Kayit Dişi Ekonomi̇ Özeli̇nde Diş Ti̇caret Ve Ekonomi̇k Büyümeni̇n Enerji̇ Tüketi̇mi̇ Üzeri̇ndeki̇ Etki̇si̇: G20 Ülkeleri̇ Örneği̇. Toplum Ekonomi Ve Yönetim Dergisi. 2023;4(2):214-27.
  • Eren N, Hayat F, Günay M. Sertleştirilmiş 1.2367 Takım Çeliğinin İşlenmesinde Enerji Tüketiminin Analizi ve Modellenmesi. Manufacturing Technologies and Applications. 2020;1(3):41-9.
  • Li PN, Chen M, Kang XJ, Zhang L, Zhou M. The Optimization of Cutting Parameters for Surface Roughness in High Speed Milling based on Taguchi Method. Mater Sci Forum. 2012;723:196-+.
  • Liu ZQ, Zhang F, Jiang FL. Investigations of Transient Machined Workpiece Surface Temperature in High Speed Peripheral Milling Using Inverse Method. Mater Sci Forum. 2012;723:14-9.
  • Yogeswaran M, Kadirgama K, Rahman MM, Devarajan R. Temperature Analysis When Using Ethylene-Glycol-Based Tio as a New Coolant for Milling. Int J Automo Mech E. 2015;11:2272-81.
  • Storchak M, Hlembotska L, Melnyk O. Generation of Mechanical Characteristics in Workpiece Subsurface Layers through Milling. Materials. 2024;17(7).Carlson BM. Human embryology and developmental biology. 4th ed. St. Louis: Mosby; 2009.

CNC Nanopartikül Katkılı Nanoakışkanların Cupral 4M Alaşımının İşlenebilirliği Üzerine Etkilerinin Araştırılması

Year 2025, Volume: 14 Issue: 3, 165 - 171, 26.09.2025
https://doi.org/10.46810/tdfd.1738630

Abstract

Cupral 4M gibi bakır-nikel esaslı alaşımların işlenebilirliği, yüksek termal iletkenlik, yapışkan talaş oluşumu ve takım aşınmasına yatkınlık nedeniyle imalat endüstrisinde oldukça zorlu işlenebilirliğe sahip olarak bilinir. Geleneksel soğutma ve yağlama yöntemleri bu malzemelerin işlenebilirliğinde yetersiz kalmakla birlikte, üretim kalitesi ve takım ömrü gibi işlenebilirlik metrikleri üzerinde olumsuzluğa neden olmaktadır. Bu çalışmada, ağırlıkça %0.5 CNC nanotozu katkılı MQL sıvısının Cupral 4M malzemesinin frezeleme işlemi üzerindeki etkileri incelenmiştir. Deneyler iki farklı kesme hızı (125-150 m/dk), iki farklı ilerleme hızı (0.04-0.06 mm/dev) ve üç farklı soğutma/yağlama koşulu (kuru, saf MQL, CNC nano parçacık MQL) altında gerçekleştirilmiştir. Deney sonucu olarak yüzey pürüzlülüğü, takım aşınması ve enerji tüketimi ölçülmüş, elde edilen veriler karşılaştırmalı olarak irdelenmiştir. CNC nanotoz ilaveli MQL sıvısı, kuru ve MQL ortamına göre her üç sonuçta da anlamlı iyileşmeler (yüzey kalitesinde %66’ya, takım aşınmasında %39’a, enerji tüketiminde ise %10’a kadar) sağlamıştır. Bu sonuçlar, CNC nano partikül ilavesinin kesme bölgesinde sürtünme azaltıcı ve tribo-film koruyucu bir etki oluşturduğunu göstermiştir. Bu çalışma, Cupral 4M malzemesinin sürdürülebilir frezelenebilirliğini artırmaya yönelik literatürdeki önemli boşluklardan birini doldurmakla birlikte ve nano partikül katkılı MQL sıvılarının etkinliğini ortaya çıkarmıştır.

References

  • Uzun M, Usca ÜA, Kuntoglu M, Gupta MK. Influence of tool path strategies on machining time, tool wear, and surface roughness during milling of AISI X210Cr12 steel. Int J Adv Manuf Tech. 2022;119(3-4):2709-20.
  • Kar BC, Panda A, Kumar R, Sahoo AK, Mishra RR. Research trends in high speed milling of metal alloys: A short review. Mater Today-Proc. 2020;26:2657-62.
  • Polo S, Rubio EM, Marín MM, de Pipaón JMS. Evolution and Latest Trends in Cooling and Lubrication Techniques for Sustainable Machining: A Systematic Review. Processes. 2025;13(2).
  • Sap S. Understanding the Machinability and Energy Consumption of Al-Based Hybrid Composites under Sustainable Conditions. Lubricants. 2023;11(3).
  • Sap E, Usca ÜA, Degirmenci Ü, Sap S, Uzun M. Evaluation of Machinability and Energy Consumption of CK45 Steel Using Synthetic-Based Nanofluid and Minimum Quantity Lubrication Cutting Fluid. Metals-Basel. 2025;15(1).
  • Sap E, Usca ÜA, Uzun M. Machining and optimization of reinforced copper composites using different cooling-lubrication conditions. J Braz Soc Mech Sci. 2022;44(9).
  • Sap E, Usca ÜA, Sap S, Polat H, Giasin K, Kalyoncu M. Understanding the effects of machinability properties of Incoloy 800 superalloy under different machining conditions using artificial intelligence methods. Mater Today Commun. 2024;38.
  • Sap S, Acar E, Degirmenci U, Usca UA, Memis S, Sener R. Machinability of different Cu-Gr composites in milling: Performance parameters prediction via machine learning models. Expert Syst Appl. 2025;272.
  • Dogan MA, Yazman S, Gemi L, Yildiz M, Yapici A. A review on drilling of FML stacks with conventional and unconventional processing methods under different conditions. Compos Struct. 2022;297.
  • Dambatta YS, Li CH, Yang M, Beikai LI, Gao T, Liu MZ, et al. Grinding with minimum quantity lubrication: a comparative assessment. Int J Adv Manuf Tech. 2023;128(3-4):955-1014.
  • Sap E, Usca ÜA, Sap S. Impacts of Environmentally Friendly Milling of Inconel-800 Superalloy on Machinability Parameters and Energy Consumption. Int J Pr Eng Man-Gt. 2024;11(3):781-97.
  • Usca UA, Sap S, Uzun M, Degirmenci U. Assessment of the machinability and energy consumption characteristics of Cu-6Gr hybrid composites under sustainable operating. J Braz Soc Mech Sci. 2024;46(4).
  • Degirmenci Ü, Usca ÜA, Sap S. Machining characterization and optimization under different cooling/lubrication conditions of Al-4Gr hybrid composites fabricated by vacuum sintering. Vacuum. 2023;208.
  • Chinchanikar S, Kore SS, Hujare P. A review on nanofluids in minimum quantity lubrication machining. J Manuf Process. 2021;68:56-70.
  • Bai XF, Li CH, Dong L, Yin QA. Experimental evaluation of the lubrication performances of different nanofluids for minimum quantity lubrication (MQL) in milling Ti-6Al-4V. Int J Adv Manuf Tech. 2019;101(9-12):2621-32.
  • Abellán-Nebot JV, Ameen KH, Khan AM, Mondragón R. Application of Hybrid Nanofluids in MQL Assisted Machining Operations: Exploring Synergies and Establishing Guidelines. Int J Pr Eng Man-Gt. 2025;12(2):657-89.
  • Zhang YB, Li CH, Jia DZ, Li BK, Wang YG, Yang M, et al. Experimental study on the effect of nanoparticle concentration on the lubricating property of nanofluids for MQL grinding of Ni-based alloy. J Mater Process Tech. 2016;232:100-15.
  • Günay M, Korkmaz ME. Understanding the Relationship between Surface Quality and Chip Morphology under Sustainable Cutting Environments. Materials. 2024;17(8).
  • Pal A, Chatha SS, Sidhu HS. Tribological characteristics and drilling performance of nano-MoS-enhanced vegetable oil-based cutting fluid using eco-friendly MQL technique in drilling of AISI 321 stainless steel. J Braz Soc Mech Sci. 2021;43(4).
  • Wang Y, Liu CF. State-of-the-art on minimum quantity lubrication in green machining. J Clean Prod. 2023;429.
  • Usca UA. The Effect of Cellulose Nanocrystal-Based Nanofluid on Milling Performance: An Investigation of Dillimax 690T. Polymers-Basel. 2023;15(23).
  • Şap S. Effects on Machinability of Minimum Quantity Lubrication Strategy during Milling of ST52 Steel. Türk Doğa ve Fen Dergisi. 2023;12(1):82-90.
  • Yildirim ÇV. Investigation of hard turning performance of eco-friendly cooling strategies: Cryogenic cooling and nanofluid based MQL. Tribol Int. 2020;144.
  • Abellán-Nebot JV, Pastor CV, Siller HR. A Review of the Factors Influencing Surface Roughness in Machining and Their Impact on Sustainability. Sustainability-Basel. 2024;16(5).
  • Liao ZR, la Monaca A, Murray J, Speidel A, Ushmaev D, Clare A, et al. Surface integrity in metal machining - Part I: Fundamentals of surface characteristics and formation mechanisms. Int J Mach Tool Manu. 2021;162.
  • Zerooglu T, Degirmenci Ü, Sap S. A Study on the Machinability and Environmental Effects of Milling AISI 5140 Steel in Sustainable Cutting Environments. Machines. 2024;12(7).
  • Sap S, Usca A, Tarih YS, Yar A, Kuntoglu M, Gupta MK. Novel Use of Cellulose Based Biodegradable Nano Crystals in the Machining of PPS Composites: An Approach Towards Green Machining. Int J Pr Eng Man-Gt. 2024;11(1):1-19.
  • Sap S. Machining and Energy Aspect Assessment with Sustainable Cutting Fluid Strategies of Al-12Si Based Hybrid Composites. Int J Pr Eng Man-Gt. 2024;11(1):33-53.
  • Salur E. Understandings the tribological mechanism of Inconel 718 alloy machined under different cooling/lubrication conditions. Tribol Int. 2022;174.
  • Hsu SM, Shen MC, Ruff AW. Wear prediction for metals. Tribol Int. 1997;30(5):377-83.
  • Mughal K, Mughal MP, Farooq MU, Anwar S, Ammarullah MI. Using Nano-Fluids Minimum Quantity Lubrication (NF-MQL) to Improve Tool Wear Characteristics for Efficient Machining of CFRP/Ti6Al4V Aeronautical Structural Composite. Processes. 2023;11(5).
  • Dağılgan G. Kayit Dişi Ekonomi̇ Özeli̇nde Diş Ti̇caret Ve Ekonomi̇k Büyümeni̇n Enerji̇ Tüketi̇mi̇ Üzeri̇ndeki̇ Etki̇si̇: G20 Ülkeleri̇ Örneği̇. Toplum Ekonomi Ve Yönetim Dergisi. 2023;4(2):214-27.
  • Eren N, Hayat F, Günay M. Sertleştirilmiş 1.2367 Takım Çeliğinin İşlenmesinde Enerji Tüketiminin Analizi ve Modellenmesi. Manufacturing Technologies and Applications. 2020;1(3):41-9.
  • Li PN, Chen M, Kang XJ, Zhang L, Zhou M. The Optimization of Cutting Parameters for Surface Roughness in High Speed Milling based on Taguchi Method. Mater Sci Forum. 2012;723:196-+.
  • Liu ZQ, Zhang F, Jiang FL. Investigations of Transient Machined Workpiece Surface Temperature in High Speed Peripheral Milling Using Inverse Method. Mater Sci Forum. 2012;723:14-9.
  • Yogeswaran M, Kadirgama K, Rahman MM, Devarajan R. Temperature Analysis When Using Ethylene-Glycol-Based Tio as a New Coolant for Milling. Int J Automo Mech E. 2015;11:2272-81.
  • Storchak M, Hlembotska L, Melnyk O. Generation of Mechanical Characteristics in Workpiece Subsurface Layers through Milling. Materials. 2024;17(7).Carlson BM. Human embryology and developmental biology. 4th ed. St. Louis: Mosby; 2009.
There are 37 citations in total.

Details

Primary Language English
Subjects Experimental Methods in Fluid Flow, Heat and Mass Transfer
Journal Section Articles
Authors

Üsame Ali Usca 0000-0001-5160-5526

Publication Date September 26, 2025
Submission Date July 9, 2025
Acceptance Date September 3, 2025
Published in Issue Year 2025 Volume: 14 Issue: 3

Cite

APA Usca, Ü. A. (2025). Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy. Türk Doğa Ve Fen Dergisi, 14(3), 165-171. https://doi.org/10.46810/tdfd.1738630
AMA Usca ÜA. Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy. TJNS. September 2025;14(3):165-171. doi:10.46810/tdfd.1738630
Chicago Usca, Üsame Ali. “Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy”. Türk Doğa Ve Fen Dergisi 14, no. 3 (September 2025): 165-71. https://doi.org/10.46810/tdfd.1738630.
EndNote Usca ÜA (September 1, 2025) Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy. Türk Doğa ve Fen Dergisi 14 3 165–171.
IEEE Ü. A. Usca, “Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy”, TJNS, vol. 14, no. 3, pp. 165–171, 2025, doi: 10.46810/tdfd.1738630.
ISNAD Usca, Üsame Ali. “Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy”. Türk Doğa ve Fen Dergisi 14/3 (September2025), 165-171. https://doi.org/10.46810/tdfd.1738630.
JAMA Usca ÜA. Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy. TJNS. 2025;14:165–171.
MLA Usca, Üsame Ali. “Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy”. Türk Doğa Ve Fen Dergisi, vol. 14, no. 3, 2025, pp. 165-71, doi:10.46810/tdfd.1738630.
Vancouver Usca ÜA. Investigation of the Effects of CNC Nanoparticle-Added Nanofluids on the Machinability of Cupral 4M Alloy. TJNS. 2025;14(3):165-71.

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