Coating of Graphene on the Spunbond Non-Woven Textile Surface Via Electrospinning Method in Nano Size and its Characterization

Year 2017, Volume: 24 Issue: 108, 243 - 253, 31.12.2017

M. Hakkı Alma Mustafa Yazıcı Behzat Yıldırım , İsmail Tiyek

Abstract

 In this study, reduced graphene oxide (RGO) was produced via chemical
method using graphene oxide (GO) obtained by modified Hummer's method. Produced
RGO was dispersed in deionized water, dimethylformamide (DMF), N-methyl-2-pyrrolidone
(NMP), tetrahydrofuran (THF), DMF/THF (1/1, wt%) solvents at different
concentrations. These mixtures were spun on nonwoven spunbond surface using multi-needle
electrospinning method at different spinning parameters. It was determined that
RGO in DMF could be coated in nano size without any polymer addition using
electrospinning method. According to results from spectroscopic, morphological
and thermal analyses, it was determined that RGO was successfully coated on
spunbond surface and changed the properties.

Keywords

Graphene oxide, reduced graphene oxide, multi-needle electrospinning, nano surface

Spunbond Dokusuz Tekstil Yüzeyi Üzerine Elektro Çekim Yöntemi ile Nano Boyutta Grafen Kaplanması ve Karakterizasyonu

Abstract

Bu çalışmada, modifiye Hummers
yöntemi ile elde edilen grafen oksitten (GO) kimyasal yöntemle indirgenmiş grafen
oksit (RGO) üretilmiştir. Üretilen RGO, farklı konsantrasyonlarda deiyonize su,
dimetilformamid (DMF), N-metil-2-pirolidon
(NMP), Tetrahidrofuran (THF), DMF/THF  (1/1, ağ.%) çözücüleri içerisinde dispers
edilmiştir. Bu karışımlar çok iğneli elektro çekim yöntemiyle farklı parametrelerde
spunbond dokusuz yüzey üzerine çekilmiştir. RGO’nun kullanılan çözücüler
arasından DMF ile herhangi bir polimere gerek duyulmadan elektro çekim yöntemi
kullanılarak nano boyutta kaplanmasının mümkün olduğu belirlenmiştir. Elde
edilen yüzeylere yapılan spektroskopik, morfolojik ve termal analiz
sonuçlarından RGO’nun başarılı bir şekilde spunbond yüzeye kaplanarak özelliklerini
değiştirdiği tespit edilmiştir.

 

Keywords

Grafen oksit, İndirgenmiş grafen oksit, çok iğneli elektroçekim, nano yüzey

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