The aim of this study was to investigate the possibility of using bio-oil obtained from pine cones, olive mill pomace, and wheat straw as rejuvenators for the reuse of aged asphalt binders. Additionally, the biomass used for bio-oil production was selected from waste materials. Therefore, it makes great contributions to both the environment and the economy. B50/70 bitumen was selected as the neat binder. The bio-oils used in the study were obtained as a result of pyrolysis. Bio-oil rejuvenators at 5%, 10% and 20% by the weight of the binder were added to the aged binder obtained from recycled asphalt mixtures to obtaine bioregenerated asphalts. The physical and rheological properties of bioregenerated asphalts were investigated and not compared on neat and aged binders through penetration, softening point, rotational viscometer and dynamic shear rheometer tests. In addition, the effects of temperature and biooil content on complex modulus properties were examined using response surface methods. It was foud that while the bio-oils increased the penetration values of the aged binders, they also decreased the softening point and viscosity values. The bio-oils significantly modified rutting resistance of the aged binder. The addition of bio-oil improved the viscous components and can rejuvenate the viscoelastic properties of aged asphalt binders to that of almost the original level. In addition, response surface methods results showed that the interactions between both independent variables were effective. Finally, high coefficient of determination (R2) values indicated good agreement between the actual and predicted values. It was recommended as a result of the study that 20% concentration of bio-oil should be used to rejuvenate the aged asphalt binder for reuse in pavement construction.
Türkiye Bilimsel ve Teknolojik Araştırma Kurumu (TÜBİTAK)
Project Number
122M042
Thanks
This study was carried out within the scope of the Scientific and Technological Research Council of Turkey (TUBITAK). We gratefully acknowledge the financial support provided by TUBITAK to the Research Project 122M042.
References
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Onochie, A., Fini, E., Yang, X., Mills-Beale, J., You, Z.: Transportation research board 92nd annual meeting. Rheological Characterization of Nano-particle based Bio-modified Binder, Washington DC (2013)
Zhang, R., Wang, H., Gao, J., Yang, X., You, Z.: Comprehensive Performance Evaluation and Cost Analysis of SBS-Modified Bioasphalt Binders and Mixtures. J. Mater. Civ. Eng. 29, 04017232 (2017). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002098
Ge, D., Yan, K., You, Z., Xu, H.: Modification mechanism of asphalt binder with waste tire rubber and recycled polyethylene. Constr. Build. Mater. 126, 66–76 (2016). https://doi.org/10.1016/j.conbuildmat.2016.09.014
Zhang, R., Wang, H., Jiang, X., You, Z., Yang, X., Ye, M.: Thermal Storage Stability of Bio-Oil Modified Asphalt. J. Mater. Civ. Eng. 30, 04018054 (2018). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002237
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Zaumanis, M., Mallick, R.B., Poulikakos, L., Frank, R.: Influence of six rejuvenators on the performance properties of Reclaimed Asphalt Pavement (RAP) binder and 100% recycled asphalt mixtures. Constr. Build. Mater. 71, 538–550 (2014). https://doi.org/10.1016/j.conbuildmat.2014.08.073
Xie, Z., Tran, N., Julian, G., Taylor, A., Blackburn, L.D.: Performance of Asphalt Mixtures with High Recycled Contents Using Rejuvenators and Warm-Mix Additive: Field and Lab Experiments. J. Mater. Civ. Eng. 29, 04017190 (2017). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002037
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Yang, X., You, Z.-P., Dai, Q.-L.: Performance evaluation of asphalt binder modified by bio-oil generated from waste wood resources. Int. J. Pavement Res. Technol. 6, 431–439 (2013). https://doi.org/10.6135/ijprt.org.tw/2013.6(4).431
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Asli, H., Ahmadinia, E., Zargar, M., Karim, M.R.: Investigation on physical properties of waste cooking oil – Rejuvenated bitumen binder. Constr. Build. Mater. 37, 398–405 (2012). https://doi.org/10.1016/j.conbuildmat.2012.07.042
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Gong, M., Yang, J., Zhang, J., Zhu, H., Tong, T.: Physical–chemical properties of aged asphalt rejuvenated by bio-oil derived from biodiesel residue. Constr. Build. Mater. 105, 35–45 (2016). https://doi.org/10.1016/j.conbuildmat.2015.12.025
Zargar, M., Ahmadinia, E., Asli, H., Karim, M.R.: Investigation of the possibility of using waste cooking oil as a rejuvenating agent for aged bitumen. J. Hazard. Mater. 233–234, 254–258 (2012). https://doi.org/10.1016/j.jhazmat.2012.06.021
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Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt
The aim of this study was to investigate the possibility of using bio-oil obtained from pine cones, olive mill pomace, and wheat straw as rejuvenators for the reuse of aged asphalt binders. Additionally, the biomass used for bio-oil production was selected from waste materials. Therefore, it makes great contributions to both the environment and the economy. B50/70 bitumen was selected as the neat binder. The bio-oils used in the study were obtained as a result of pyrolysis. Bio-oil rejuvenators at 5%, 10% and 20% by the weight of the binder were added to the aged binder obtained from recycled asphalt mixtures to obtaine bioregenerated asphalts. The physical and rheological properties of bioregenerated asphalts were investigated and not compared on neat and aged binders through penetration, softening point, rotational viscometer and dynamic shear rheometer tests. In addition, the effects of temperature and biooil content on complex modulus properties were examined using response surface methods. It was foud that while the bio-oils increased the penetration values of the aged binders, they also decreased the softening point and viscosity values. The bio-oils significantly modified rutting resistance of the aged binder. The addition of bio-oil improved the viscous components and can rejuvenate the viscoelastic properties of aged asphalt binders to that of almost the original level. In addition, response surface methods results showed that the interactions between both independent variables were effective. Finally, high coefficient of determination (R2) values indicated good agreement between the actual and predicted values. It was recommended as a result of the study that 20% concentration of bio-oil should be used to rejuvenate the aged asphalt binder for reuse in pavement construction.
Chailleux, E., Audo, M., Bujoli, B., Queffelec, C., Legrand, J., Lepine, O.: Workshop alternative binders for sustainable asphalt pavements. In: Alternative Binder from Microalgae: Algoroute Project. pp. 7–14 (2012)
Zhang, R., Wang, H., Gao, J., You, Z., Yang, X.: High temperature performance of SBS modified bio-asphalt. Constr. Build. Mater. 144, 99–105 (2017). https://doi.org/10.1016/j.conbuildmat.2017.03.103
Lv, S., Liu, C., Yao, H., Zheng, J.: Comparisons of synchronous measurement methods on various moduli of asphalt mixtures. Constr. Build. Mater. 158, 1035–1045 (2018). https://doi.org/10.1016/j.conbuildmat.2017.09.193
Lee, K.W., Brayton, T.E., Mueller, M., Singh, A.: Rational Mix-Design Procedure for Cold In-Place Recycling Asphalt Mixtures and Performance Prediction. J. Mater. Civ. Eng. 28, 04016008 (2016). https://doi.org/10.1061/(ASCE)MT.1943-5533.0001492
Onochie, A., Fini, E., Yang, X., Mills-Beale, J., You, Z.: Transportation research board 92nd annual meeting. Rheological Characterization of Nano-particle based Bio-modified Binder, Washington DC (2013)
Zhang, R., Wang, H., Gao, J., Yang, X., You, Z.: Comprehensive Performance Evaluation and Cost Analysis of SBS-Modified Bioasphalt Binders and Mixtures. J. Mater. Civ. Eng. 29, 04017232 (2017). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002098
Ge, D., Yan, K., You, Z., Xu, H.: Modification mechanism of asphalt binder with waste tire rubber and recycled polyethylene. Constr. Build. Mater. 126, 66–76 (2016). https://doi.org/10.1016/j.conbuildmat.2016.09.014
Zhang, R., Wang, H., Jiang, X., You, Z., Yang, X., Ye, M.: Thermal Storage Stability of Bio-Oil Modified Asphalt. J. Mater. Civ. Eng. 30, 04018054 (2018). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002237
Wang, H., Zhang, R., Chen, Y., You, Z., Fang, J.: Study on microstructure of rubberized recycled hot mix asphalt based X-ray CT technology. Constr. Build. Mater. 121, 177–184 (2016). https://doi.org/10.1016/j.conbuildmat.2016.05.166
Bell, C.A., Wieder, A.J., Fellin, M.J.: Laboratory aging of asphalt-aggregate mixtures, Field Validation. , Washington, DC (1994)
Said, S.: Aging Effect on Mechanical Characteristics of Bituminous Mixtures. Transp. Res. Rec. J. Transp. Res. Board. 1901, 1–9 (2005). https://doi.org/10.3141/1901-01
Ramadan, K.Z., Saad, A.A.: Effect of Superpave Short-Term Aging on Binder and Asphalt Mixture Rheology. Period. Polytech. Transp. Eng. 45, 196 (2017). https://doi.org/10.3311/PPtr.10477
G. Holleran, T. Wieringa, T. Tailby: Rejuvenation treatments for aged pavements. In: Transit New Zealand and New Zealand Institute of Highway Technology (NZIHT) Annual Conference. , Auckland, New Zealand (2006)
Zhang, R.H., Zhao, T.S., Tan, P., Wu, M.C., Jiang, H.R.: Ruthenium dioxide-decorated carbonized tubular polypyrrole as a bifunctional catalyst for non-aqueous lithium-oxygen batteries. Electrochim. Acta. 257, 281–289 (2017). https://doi.org/10.1016/j.electacta.2017.10.097
Nahar, S.N., Qiu, J., Schmets, A.J.M., Schlangen, E., Shirazi, M., van de Ven, M.F.C., Schitter, G., Scarpas, A.: Turning Back Time. Transp. Res. Rec. J. Transp. Res. Board. 2444, 52–62 (2014). https://doi.org/10.3141/2444-06
Yu, X., Zaumanis, M., dos Santos, S., Poulikakos, L.D.: Rheological, microscopic, and chemical characterization of the rejuvenating effect on asphalt binders. Fuel. 135, 162–171 (2014). https://doi.org/10.1016/j.fuel.2014.06.038
Zaumanis, M., Mallick, R.B., Poulikakos, L., Frank, R.: Influence of six rejuvenators on the performance properties of Reclaimed Asphalt Pavement (RAP) binder and 100% recycled asphalt mixtures. Constr. Build. Mater. 71, 538–550 (2014). https://doi.org/10.1016/j.conbuildmat.2014.08.073
Xie, Z., Tran, N., Julian, G., Taylor, A., Blackburn, L.D.: Performance of Asphalt Mixtures with High Recycled Contents Using Rejuvenators and Warm-Mix Additive: Field and Lab Experiments. J. Mater. Civ. Eng. 29, 04017190 (2017). https://doi.org/10.1061/(ASCE)MT.1943-5533.0002037
Tran, N., Xie, Z., Julian, G., Taylor, A., Willis, R., Robbins, M., Buchanan, S.: Effect of a Recycling Agent on the Performance of High-RAP and High-RAS Mixtures: Field and Lab Experiments. J. Mater. Civ. Eng. 29, 04016178 (2017). https://doi.org/10.1061/(ASCE)MT.1943-5533.0001697
Lei, Z., Bahia, H., Yi-qiu, T.: Effect of bio-based and refined waste oil modifiers on low temperature performance of asphalt binders. Constr. Build. Mater. 86, 95–100 (2015). https://doi.org/10.1016/j.conbuildmat.2015.03.106
Yang, X., You, Z.-P., Dai, Q.-L.: Performance evaluation of asphalt binder modified by bio-oil generated from waste wood resources. Int. J. Pavement Res. Technol. 6, 431–439 (2013). https://doi.org/10.6135/ijprt.org.tw/2013.6(4).431
López, S., Davies, D.R., Giráldez, F.J., Dhanoa, M., Dijkstra, J., France, J.: Assessment of nutritive value of cereal and legume straws based on chemical composition andin vitro digestibility. J. Sci. Food Agric. 85, 1550–1557 (2005). https://doi.org/10.1002/jsfa.2136
Wang, M., Hettiarachchy, N.S., Qi, M., Burks, W., Siebenmorgen, T.: Preparation and Functional Properties of Rice Bran Protein Isolate. J. Agric. Food Chem. 47, 411–416 (1999). https://doi.org/10.1021/jf9806964
Wang, J., Sun, B., Cao, Y., Wang, C.: In vitro fermentation of xylooligosaccharides from wheat bran insoluble dietary fiber by Bifidobacteria. Carbohydr. Polym. 82, 419–423 (2010). https://doi.org/10.1016/j.carbpol.2010.04.082
Ortiz de Zárate, I., Ezcurra, A., Lacaux, J.P., Van Dinh, P., de Argandoña, J.D.: Pollution by cereal waste burning in Spain. Atmos. Res. 73, 161–170 (2005). https://doi.org/10.1016/j.atmosres.2004.07.006
Ayrilmis, N., Buyuksari, U., Dundar, T.: Waste pine cones as a source of reinforcing fillers for thermoplastic composites. J. Appl. Polym. Sci. 117, 2324–2330 (2010). https://doi.org/10.1002/app.32076
McCready, N.S., Williams, R.C.: The Utilization of Agriculturally Derived Lignin as an Antioxidant in Asphalt Binder. In: Proceedings of the 2007 Mid-Continent Transportation Research Symposium. , Ames (2007)
Li, Y., Xing, B., Ding, Y., Han, X., Wang, S.: A critical review of the production and advanced utilization of biochar via selective pyrolysis of lignocellulosic biomass. Bioresour. Technol. 312, 123614 (2020). https://doi.org/10.1016/j.biortech.2020.123614
Akhtar, J., Kuang, S.K., Amin, N.S.: Liquefaction of empty palm fruit bunch (EPFB) in alkaline hot compressed water. Renew. Energy. 35, 1220–1227 (2010). https://doi.org/10.1016/j.renene.2009.10.003
Bridgwater, A.: Fast pyrolysis processes for biomass. Renew. Sustain. Energy Rev. 4, 1–73 (2000). https://doi.org/10.1016/S1364-0321(99)00007-6
Mohan, D., Pittman, C.U., Steele, P.H.: Pyrolysis of Wood/Biomass for Bio-oil: A Critical Review. Energy & Fuels. 20, 848–889 (2006). https://doi.org/10.1021/ef0502397
Asli, H., Ahmadinia, E., Zargar, M., Karim, M.R.: Investigation on physical properties of waste cooking oil – Rejuvenated bitumen binder. Constr. Build. Mater. 37, 398–405 (2012). https://doi.org/10.1016/j.conbuildmat.2012.07.042
You, Z., Mills-Beale, J., Fini, E., Goh, S.W., Colbert, B.: Evaluation of Low-Temperature Binder Properties of Warm-Mix Asphalt, Extracted and Recovered RAP and RAS, and Bioasphalt. J. Mater. Civ. Eng. 23, 1569–1574 (2011). https://doi.org/10.1061/(ASCE)MT.1943-5533.0000295
Wang, H., Sun, M., Yang, H., Tian, X., Tong, Y., Zhou, T., Zhang, T., Fu, Y., Guo, X., Fan, D., Yu, A., Fan, M., Wu, X., Xiao, W., Chui, D.: Hypoxia-inducible factor-1α mediates up-regulation of neprilysin by histone deacetylase-1 under hypoxia condition in neuroblastoma cells. J. Neurochem. 131, 4–11 (2014). https://doi.org/10.1111/jnc.12795
Yang, X., You, Z.: High temperature performance evaluation of bio-oil modified asphalt binders using the DSR and MSCR tests. Constr. Build. Mater. 76, 380–387 (2015). https://doi.org/10.1016/j.conbuildmat.2014.11.063
Gong, M., Yang, J., Zhang, J., Zhu, H., Tong, T.: Physical–chemical properties of aged asphalt rejuvenated by bio-oil derived from biodiesel residue. Constr. Build. Mater. 105, 35–45 (2016). https://doi.org/10.1016/j.conbuildmat.2015.12.025
Zargar, M., Ahmadinia, E., Asli, H., Karim, M.R.: Investigation of the possibility of using waste cooking oil as a rejuvenating agent for aged bitumen. J. Hazard. Mater. 233–234, 254–258 (2012). https://doi.org/10.1016/j.jhazmat.2012.06.021
Ržek, L., Ravnikar Turk, M., Tušar, M.: Increasing the rate of reclaimed asphalt in asphalt mixture by using alternative rejuvenator produced by tire pyrolysis. Constr. Build. Mater. 232, 117177 (2020). https://doi.org/10.1016/j.conbuildmat.2019.117177
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Yalçın, B. F., & Yilmaz, M. (2024). Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt. Turkish Journal of Civil Engineering, 35(3), 95-123. https://doi.org/10.18400/tjce.1320185
AMA
Yalçın BF, Yilmaz M. Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt. tjce. May 2024;35(3):95-123. doi:10.18400/tjce.1320185
Chicago
Yalçın, Beyza Furtana, and Mehmet Yilmaz. “Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes As Rejuvenators for Recycled Asphalt”. Turkish Journal of Civil Engineering 35, no. 3 (May 2024): 95-123. https://doi.org/10.18400/tjce.1320185.
EndNote
Yalçın BF, Yilmaz M (May 1, 2024) Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt. Turkish Journal of Civil Engineering 35 3 95–123.
IEEE
B. F. Yalçın and M. Yilmaz, “Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt”, tjce, vol. 35, no. 3, pp. 95–123, 2024, doi: 10.18400/tjce.1320185.
ISNAD
Yalçın, Beyza Furtana - Yilmaz, Mehmet. “Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes As Rejuvenators for Recycled Asphalt”. Turkish Journal of Civil Engineering 35/3 (May 2024), 95-123. https://doi.org/10.18400/tjce.1320185.
JAMA
Yalçın BF, Yilmaz M. Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt. tjce. 2024;35:95–123.
MLA
Yalçın, Beyza Furtana and Mehmet Yilmaz. “Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes As Rejuvenators for Recycled Asphalt”. Turkish Journal of Civil Engineering, vol. 35, no. 3, 2024, pp. 95-123, doi:10.18400/tjce.1320185.
Vancouver
Yalçın BF, Yilmaz M. Investigation of the Performance of Bio-Oils from Three Different Agricultural Wastes as Rejuvenators for Recycled Asphalt. tjce. 2024;35(3):95-123.