rGO/SnSbS Nanokompozitlerin Farklı Depolama Sıcaklığına Bağlı Elektriksel, Yapısal ve Yüzeysel Değerlendirmesi

Year 2022, Volume: 14 Issue: 2, 907 - 916, 31.07.2022

Necmi Serkan Tezel , Afşin Kariper

https://doi.org/10.29137/umagd.1062439

Abstract

Bu çalışmada indirgenmiş grafen oksit/sülfosalt (rGO/SnSbS) nanokompozit yapıları ticari cam taban malzemeler üzerine kimyasal banyo depolama (CBD) metodu ile 20 °C, 40 °C, 60 °C ve 80 °C sıcaklıklarda üretilmiştir. Yapısal olarak düşük sıcaklık değerlerinde amorf yapıya sahiptir ancak 80 °C sıcaklıkta Sn2Sb2S5 kristallenmeleri gözlenmiştir. Artan depolama sıcaklığına bağlı 125,22 nm, 126,27nm, 132,95 nm ve 157,16 nm kalınlıklı nanokompozit yapıların daha homojen ve yoğun yapışkan kıvama geldiği görülmüştür. Elektriksel dirençleri ise four-point probe metodu ile film kalınlığına bağlı olarak I-V ölçümlerinden hesaplanmıştır ve sıcaklığın artması ile elektriksel dirençlerin düştüğü görülmüştür. Elde edilen verilere göre sıcaklığın etkisi ve kullanım alanları tartışılmıştır.

Keywords

İnce film, CBD, Sülfosalt, Elektrik direnci, Depolama sıcaklığı

Supporting Institution

Karabük Üniversitesi Bilimsel Araştırma Projeleri Birimi

Project Number

KBÜBAP-21-DS-012

Thanks

Bu çalışma Karabük Üniversitesi Bilimsel Araştırma Projeleri Birimi tarafından KBÜBAP-21-DS-012 nolu proje ile desteklenmiştir. Finansal desteklerinden dolayı KBU-BAP birimine teşekkür ederiz.

Electrical, Structural, Surface Evaluation Depends on the Different Deposition Temperature of rGO/SnSbS Nanocomposite

Abstract

In this study, reduced graphene oxide/sulfosalt (rGO/SnSbS) nanocomposite structures were produced at temperatures of 20 °C, 40 °C, 60 °C and 80°C with chemical bath deposition (CBD) method on commercial glass substrates. Structurally, it has an amorphous structure at low temperature values, but crystallizations of Sn2Sb2S5 have been observed at the temperature of 80 °C. It has been observed that nanocomposite structures with thickness of 125.22 nm, 126.27nm, 132.95 nm and 157.16 nm due to increased deposition temperatures have a more homogeneous and dense adhesive consistency. Their electrical resistance was calculated from I-V measurements depending on the film thickness using the four-point probe method, and it was observed that the electrical resistance decreased with increasing temperature. According to the obtained results, the effect of temperature and their usage applications have been discussed.

Keywords

Thin film; CBD, Sulfosalt, Electrical resistivity, Deposition Temperature

Project Number

KBÜBAP-21-DS-012

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