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Al 2024 Alaşımı Üzerine Mikro Ark Oksidasyon Yöntemiyle B4C İlaveli Kompozit Kaplamaların Büyütülmesi

Year 2023, , 1107 - 1117, 29.12.2023
https://doi.org/10.53433/yyufbed.1284780

Abstract

Al alaşımı üzerinde Mikro ark Oksidasyon (MAO) yöntemiyle büyütülen kaplamaların yapısı ve özellikleri üzerine Bor karbür (B4C) katılmasının etkisi, sodyum fosfat, sodyum silikat ve potasyum hidroksitten oluşan bir çözelti içerisinde gerçekleştirilerek araştırılmıştır. MAO, B4C parçacıkları eklenmiş ve eklenmemiş çözeltilerde Al 2024 alaşımı üzerine uygulanmıştır. MAO kaplamalarının faz bileşimi ve mikro yapısı X-ışını kırınımı difraktometresi (XRD) ve taramalı elektron mikroskobu (SEM) kullanılarak değerlendirilmiştir. Ayrıca kaplamaların, mikrosertlik değerleri mikrosertlik test cihazı kullanılarak tespit edilmiştir. Al alaşımı üzerindeki oksit kaplamaların birincil olarak γ- Al2O3'ten oluştuğu gözlenmiştir. Solüsyona ilave edilen B4C partiküllerinin eklenmesi, MAO kaplamalarının Al alaşımları üzerindeki oluşum hızını ve kompaktlığını iyileştirdiği ve X-ışını kırınımı yoluyla kaplamalarda B4C varlığı tespit edilmiştir. Yüksek sertlik ve iyi kimyasal stabiliteye sahip B4C parçacıkları, MAO kaplamalarında eşit olarak dağıldığı gözlenmiştir. Bu nedenle, B4C takviyeli MAO kaplamaların sertlik değeri, Al alaşımları üzerindeki B4C ilave edilmeyen oksit kaplamalardan belirgin şekilde yüksek olduğu gözlenmiştir.

References

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Deposition of B4C Doped Composite Coatings on Al 2024 Alloy by Micro-Arc Oxidation Method

Year 2023, , 1107 - 1117, 29.12.2023
https://doi.org/10.53433/yyufbed.1284780

Abstract

The effect of boron carbide (B4C) addition on the structure and properties of coatings grown by the Microarc Oxidation (MAO) method on Al alloy was investigated by performing it in a solution consisting of sodium phosphate, sodium silicate and potassium hydroxide. MAO was applied on Al 2024 alloy in solutions with and without added B4C particles. The phase composition and microstructure of the MAO coatings were evaluated using X-ray diffraction diffractometry (XRD) and scanning electron microscopy (SEM). In addition, the microhardness values of the coatings were determined using a microhardness tester. It has been observed that the oxide coatings on the Al alloy are primarily composed of γ-Al2O3. The addition of B4C particles to the solution improved the formation rate and compactness of MAO coatings on Al alloys, and the presence of B4C in the coatings was detected by X-ray diffraction. B4C particles with high hardness and good chemical stability were observed to be evenly dispersed in MAO coatings. Therefore, it has been observed that the hardness value of B4C reinforced MAO coatings is significantly higher than that of oxide coatings without B4C on Al alloys.

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  • Alizadeh, A., Taheri-Nassaj, E., & Baharvandi, H.R. (2011). Preperation and investigation of Al4wt.%B4C nanocomposite powders using mechanical milling. Bulletin of Materials Science, 34, 1039-1048. doi:10.1007/s12034-011-0158-5
  • Arrabal, R., Pardo, A., Merino, M. C., Mohedano, M., Casajús, P., Matykina, E., Skeldon, P., & Thompson, G. E. (2010). Corrosion behaviour of a magnesium matrix composite with a silicate plasma electrolytic oxidation coating. Corrosion Science, 52, 3738–3749, doi:10.1016/j.corsci.2010.07.024
  • Atapour, M., Blawert, C., & Zheludkevich, M.L. (2019). The wear characteristics of CeO2 containing nanocomposite coating made by aluminate-based PEO on AM 50 magnesium alloy. Surface and Coatings Technology, 357, 626-637. doi:10.1016/j.surfcoat.2018.10.033
  • Bahador, R., Hosseinabadi, N., & Yaghtin, A. (2021). Effect of power duty cycle on plasma electrolytic oxidation of A356-Nb2O5 metal matrix composites. Journal of Materials Engineering and Performance, 30, 2586–2604. doi:10.1007/s11665-021-05597-4
  • Becerik, D. A., Ayday, A., Kumruoğlu, L. C., Kurnaz, C., & Özel, A. (2012). The effects of Na2SiO3 concentration on the properties of plasma electrolytic oxidation coatings on 6060 aluminum alloy. Journal of Materials Engineering and Performance, 21, 1426-1430. doi:10.1007/s11665-011-0022-1
  • Chen, J., Shi, Y., Wang, L., Yan, F., & Zhang, F. (2006). Preparation and properties of hydroXyapatite-containing titania coating by micro-arc oxidation. Materials Letters, 60, 20, 2538-2543. doi:10.1016/j.matlet.2006.01.035
  • Clyne, T. W., & Troughton, S. C. (2019). A review of recent work on discharge characteristics during plasma electrolytic oxidation of various metals. International Materials Reviews, 64, 127–162. doi:10.1080/09506608.2018.1466492
  • Cui, S., Han, J., Du, Y., & Li, W. (2007). Corrosion resistance and wear resistance of plasma electrolytic oxidation coatings on metal matrix composites. Surface and Coatings Technology, 201, 5306–5309. doi:10.1016/j.surfcoat.2006.07.126
  • Darband, G. B., Aliofkhazraei, M., Hamghalam, P., & Valizade, N. (2017). Plasma electrolytic oxidation of magnesium and its alloys: Mechanism, properties and applications. Journal of Magnesium and Alloys, 5, 1, 74-132. doi:10.1016/j.jma.2017.02.004
  • Dou, J., Chen, Y., Yu, H., & Chen, C. (2017). Research status of magnesium alloys by micro-arc oxidation: a review. Surface Engineering, 33, 731-738. doi:10.1080/02670844.2017.1278642
  • Fattah-Alhosseini, A., Vakili-Azghandi, M., & Keshavarz, M. K. (2016). Influence of concentrations of KOH and Na2SiO3 electrolytes on the electrochemical behavior of ceramic coatings on 6061 Al alloy processed by plasma electrolytic oxidation. Acta Metallurgica Sinica (English Letters), 29, 274-281. doi:10.1007/s40195-016-0384-3
  • Fattah-Alhosseini, A., Gashti, S. O., & Molaie, M. (2018). Effects of disodium phosphate concentration (Na2HPO4⋅2H2O) on microstructure and corrosion resistance of plasma electrolytic oxidation (PEO) coatings on 2024 Al alloy. Journal of Materials Engineering and Performance, 27, 825-834. doi:10.1007/s11665-018-3124-1
  • Fattah-Alhosseini, A., Chaharmahali, R., & Babaei, K. (2020). Effect of particles addition to solution of plasma electrolytic oxidation (PEO) on the properties of PEO coatings formed on magnesium and its alloys: A review. Journal of Magnesium and Alloys, 8, 3, 799-818. doi:10.1016/j.jma.2020.05.001
  • Feng, X., Shi, R., Lu, X., Xu, Y., Huang, X., & Chen, D. (2017). The corrosion inhibition efficiency of aluminum tripolyphosphate on carbon steel in carbonated concrete pore solution. Corrosion Science, 124, 150–159. doi:10.1016/j.corsci.2017.05.018
  • Gu, Y., Bandopadhyay, S., Chen, C. F., Guo, Y., & Ning, C. (2012). Effect of oxidation time on the corrosion behavior of micro-arc oxidation produced AZ31 magnesium alloys in simulated body fluid. Journal of Alloys and Compounds, 543, 109–17. doi:10.1016/j.jallcom.2012.07.130
  • Guo, Q., Xu, D., Yang, W., Guo, Y., Yang, Z., Li, J., & Gao, P. (2020). Synthesis, corrosion, and wear resistance of a black microarc oxidation coating on pure titanium. Surface and Coatings Technology, 386, 125454. doi:10.1016/j.surfcoat.2020.125454
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There are 63 citations in total.

Details

Primary Language Turkish
Subjects Engineering
Journal Section Engineering and Architecture / Mühendislik ve Mimarlık
Authors

Süleyman Şüküroğlu 0000-0003-4291-6378

Publication Date December 29, 2023
Submission Date April 17, 2023
Published in Issue Year 2023

Cite

APA Şüküroğlu, S. (2023). Al 2024 Alaşımı Üzerine Mikro Ark Oksidasyon Yöntemiyle B4C İlaveli Kompozit Kaplamaların Büyütülmesi. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 28(3), 1107-1117. https://doi.org/10.53433/yyufbed.1284780