Altın otu (Helichrysum italicum) esansiyel yağının mikrokapsüle edilmesi ve karakterizasyonu
Year 2022,
, 669 - 684, 31.12.2022
Gözde K. Erdoğan
,
Fethiye Göde
Abstract
Amaç: Bu çalışmanın amacı altın otu esansiyel yağı ve argan yağı karışımının yanıt yüzey metodolojisi (YYM) koşullarında mikrokapsüle edilmesi ve uygun krem formülasyonundaki antioksidan aktivitesinin belirlenmesidir.
Materyal ve Yöntem: YYM deney tasarımı kullanılarak, kompleks koaservasyon yöntemi ile mikrokapsül üretilmiştir.
Araştırma Bulguları: Altın otu esansiyel yağı ve argan yağı karışımlı, jelatin/arap zamkı duvarlı mikrokapsüller üretilmiş ve karakterize edilmiştir. Oluşturulan deney tasarımına verilerimiz işlenerek ANOVA sonuçları elde edilmiştir. Mikrokapsül içeren kremin antioksidan kapasitesi yüksek bulunmuştur.
Sonuç: YYM ile üç farklı parametrede, kompleks koaservasyon yöntemiyle mikrokapsül üretilip, karakterize edilmiştir. Mikrokapsüllerin morfolojik görüntüleri için SEM (taramalı elektron mikroskobu) ve optik mikroskoptan yararlanılmış olup, yapıyı aydınlatmak için GC-MS (gaz kromatografisi-kütle spektroskopisi) ve FT-IR (Fourier dönüşümlü kızılötesi spektroskopisi) kullanılmıştır. Mikrokapsüller kreme eklenip, kremin antioksidan kapasitesi CUPRAC metoduyla yorumlanmıştır. Tüm veriler değerlendirildiğinde altın otu ve argan yağı karışımı kompleks koaservasyon yöntemi kullanılarak başarılı bir şekilde mikrokapsüle edilmiştir. Mikrokapsül içeren kozmetik kremin etkin bir şekilde antioksidan kapasiteye sahip olduğu görülmüştür.
Supporting Institution
SDÜ-Bilimsel Araştırma Projeleri Koordinasyon Birimi
Project Number
FYL-2022-8645
Thanks
Bu çalışma, Süleyman Demirel Üniversitesi Bilimsel Araştırma Projeleri Koordinasyon Birimi tarafından ‘FYL-2022-8645 ’kodlu proje ile desteklenmiştir.
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Microencapsulation and characterization of immortelle (Helichrysum italicum) essential oil
Year 2022,
, 669 - 684, 31.12.2022
Gözde K. Erdoğan
,
Fethiye Göde
Abstract
Objective: The objective of this study was to microencapsulation of a mixture of immortelle essential oil and argan oil under response surface methodology (RSM) conditions and determination of antioxidant activity in the appropriate cream formulation.
Material and Methods: Microcapsule was produced by complex coacervation method using RSM experimental design.
Results: Microcapsules with a mixture of immortelle essential oil and argan oil, with gelatin/gum arabic walls were produced and characterized. ANOVA results were obtained by processing the data obtained in this study. The antioxidant capacity of the cream containing microcapsules was found to be high.
Conclusion: Microcapsules were produced and characterized by complex coacervation method in three different parameters with RSM. SEM (scanning electron microscope) and optical microscope were used for morphological images of microcapsules, and GC-MS (gas chromatography-mass spectroscopy) and FT-IR (Fourier transform infrared spectroscopy) were used to elucidate the structure. Microcapsules were added to the cream and the antioxidant capacity of the cream was interpreted by the CUPRAC method. When all data were evaluated, a mixture of immortelle and argan oil was successfully microencapsulated using the complex coacervation method. It was found that the cosmetic cream containing microcapsules has an effective antioxidant capacity.
Project Number
FYL-2022-8645
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- Andjić, M., B. Božin, N. Draginić, A. Kočović, J.N. Jeremić, M. Tomović & J. V. Bradić, 2021. Formulation and evaluation of Helichrysum italicum essential oil-based topical formulations for wound healing in diabetic rats. Pharmaceuticals, 14 (8): 813. https://doi.org/10.3390/ph14080813
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- Arenas-Jal, M., J.M. Suñé-Negre & E. García-Montoya, 2020. An overview of microencapsulation in the food industry: opportunities, challenges and innovations. European Food Research and Technology, 246 (7): 1371-1382. https: //doi.org/10.1007/s00217-020-03496-x
- Bayram, O., E. Köksal & F. Göde, 2020. Yanıt yüzey metodolojisi şartlarında karabaş otu yağının kompleks koaservasyon yöntemi ile enkapsülasyonu. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 24 (2): 508-515. https: //doi.org/10.19113/sdufenbed.687943
- Boukhobza, M. & N. Pichon-Prun, 1988. L’arganier ressource économique et médicinale pour le Maroc. Phytothérapie, 27: 21-26.
- Charrouf, Z. & D. Guillaume, 2014. Argan oil, the 35‐years‐of‐research product. European Journal of Lipid Science and Technology, 116 (10): 1316-1321. https: //doi.org/10.1002/ejlt.201400261
- Charrouf, Z. & D. Guillaume, 2018. The argan oil project: going from utopia to reality in 20 years. OCL, 25 (2): D209. https: //doi.org/10.1051/ocl/2018006
- Charrouf, Z., D. Guillaume & A. Driouich, 2002. The argan tree, an asset for Morocco. Biofutur, 220: 54-57.
- Costa, P., J.M. Loureiro, M.A. Teixeira & A.E. Rodrigues, 2015. Extraction of aromatic volatiles by hydrodistillation and supercritical fluid extraction with CO2 from Helichrysum italicum subsp. picardii growing in Portugal. Industrial Crops and Products, 77: 680-683. https: //doi.org/10.1016/j.indcrop.2015.09.042
- Erdoğan, Ü. & E.H. Gökçe, 2021. Fig seed oil‐loaded nanostructured lipid carriers: Evaluation of the protective effects against oxidation. Journal of Food Processing & Preservation, 45 (10): e15835. https: //doi.org/10.1111/jfpp.15835
- Erdoğan, Ü., 2022. Antioxidant activities and chemical composition of essential oil of rhizomes of Zingiber officinale (ginger) and Curcuma longa L.(turmeric). International Journal of Secondary Metabolite, 9 (2): 137-148. https://doi.org/10.21448/ijsm.993906
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