Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract

Faruk Aslan; Ahmet Ekicibil

TR EN

Çam Kabuğu Ekstraktı Kullanılarak ZnO Nanopartiküllerinin Yeşil Sentezi

Öz

Bu çalışmada, çinko oksit (ZnO) nanoparçacıkları (NPs) çam kabuğu özütü kullanılarak yeşil sentez tekniği ile üretilmiştir. İndirgeyici ve dengeleyici bir madde olarak görev alan çam kabuğu özütü üç farklı oranda kullanılarak ZnO NP’leri sentezlenmiştir. Üretilen ZnO NP'leri X-ışını kırınımı (XRD), taramalı elektron mikroskobu (SEM), enerji dağılımlı X-ışını spektrum analizi (EDS) ve ultraviyole-görünür ışık spektroskopisi (UV-VIS) kullanılarak karakterize edildi. XRD kırınım piklerinin ZnO’nun karakteristik pikleriyle uyumlu olduğu ve hekzagonal wurtzit kristal fazında üretildiği belirlendi. SEM görüntülerinden numunelerin homojen bir şekilde üretildiği, parçacıkların hemen hemen küresel geometriye sahip olduğu ve ortalama parçacık boyutunun 20-30 nm aralığında olduğu belirlendi. Elementel analizde sadece Zn ve O elementleri gözlenerek, safsızlık atomlarının bulunmadığı tespit edildi. Ayrıca, ZnO NP’lerinin fotokatalitik aktivitesinin belirlenmesi için UV ışığı altında metilen mavisi (MB) boyasının bozunma performansı incelendi. Çam kabuğu özütü kullanarak sentezlenen ZnO NP’lerinin 80 dakikalık UV aydınlatması sonrasında MB’yi yaklaşık %66 oranında bozunma aktivitesine ulaştırdığı belirlendi.

Anahtar Kelimeler

ZnO , Yeşil sentez , Çam kabuğu özütü , Optik özellikler , Fotokatalitik aktivite

Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract

Abstract

In this study, zinc oxide (ZnO) nanoparticles (NPs) were synthesized by green synthesis technique using pine bark extract. ZnO NPs were synthesized in three different pine bark extract ratios, which acts as a reducing and stabilizing agent. The produced ZnO NPs were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectrum analysis (EDS) and ultraviolet-visible light spectroscopy (UV-VIS).It was determined that the XRD diffraction peaks were consistent with the characteristic peaks of ZnO, and ZnO NPs were produced in the hexagonal wurtzite crystal phase. It was determined from the SEM images that the samples were produced homogeneously which have almost spherical geometry and the average particles were in the range of 20-30 nm. In the elemental analysis, only Zn and O elements were observed without any impurity atoms. Also, the degradation performance of methylene blue (MB) dye under UV light was determined to determine the photocatalytic activities of ZnO NPs. It was determined that MB reached almost 66% degradation efficiency after 80 minutes of UV illumination of ZnO NPs synthesized by using pine bark extract.

Keywords

ZnO , Green synthesis , Pine bark , Optical properties , Photocatalytic activity

Kaynakça

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Ayrıntılar

Birincil Dil

İngilizce

Konular

Malzeme Fiziği

Bölüm

Araştırma Makalesi

Yazarlar

Faruk Aslan ^*
0009-0007-5012-8941
Türkiye

Ahmet Ekicibil
0000-0003-3071-0444
Türkiye

Yayımlanma Tarihi

20 Haziran 2025

Gönderilme Tarihi

18 Şubat 2025

Kabul Tarihi

11 Nisan 2025

Yayımlandığı Sayı

Yıl 2025 Cilt: 1 Sayı: 1

IZ

https://izlik.org/JA98GH96EM

APA

Aslan, F., & Ekicibil, A. (2025). Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract. Adana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi Bilim Dergisi, 1(1), 19-27. https://izlik.org/JA98GH96EM

AMA

1.Aslan F, Ekicibil A. Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract. ATUJSCIENCE. 2025;1(1):19-27. https://izlik.org/JA98GH96EM

Chicago

Aslan, Faruk, ve Ahmet Ekicibil. 2025. “Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract”. Adana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi Bilim Dergisi 1 (1): 19-27. https://izlik.org/JA98GH96EM.

EndNote

Aslan F, Ekicibil A (01 Haziran 2025) Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract. Adana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi Bilim Dergisi 1 1 19–27.

IEEE

[1]F. Aslan ve A. Ekicibil, “Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract”, ATUJSCIENCE, c. 1, sy 1, ss. 19–27, Haz. 2025, [çevrimiçi]. Erişim adresi: https://izlik.org/JA98GH96EM

ISNAD

Aslan, Faruk - Ekicibil, Ahmet. “Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract”. Adana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi Bilim Dergisi 1/1 (01 Haziran 2025): 19-27. https://izlik.org/JA98GH96EM.

JAMA

1.Aslan F, Ekicibil A. Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract. ATUJSCIENCE. 2025;1:19–27.

MLA

Aslan, Faruk, ve Ahmet Ekicibil. “Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract”. Adana Alparslan Türkeş Bilim ve Teknoloji Üniversitesi Bilim Dergisi, c. 1, sy 1, Haziran 2025, ss. 19-27, https://izlik.org/JA98GH96EM.

Vancouver

1.Faruk Aslan, Ahmet Ekicibil. Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract. ATUJSCIENCE [Internet]. 01 Haziran 2025;1(1):19-27. Erişim adresi: https://izlik.org/JA98GH96EM

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Çam Kabuğu Ekstraktı Kullanılarak ZnO Nanopartiküllerinin Yeşil Sentezi

Öz

Anahtar Kelimeler

Green Synthesis of ZnO Nanoparticles Using Pine Bark Extract

Abstract

Keywords

Kaynakça

Ayrıntılar

Birincil Dil

Konular

Bölüm

Yazarlar

Yayımlanma Tarihi

Gönderilme Tarihi

Kabul Tarihi

Yayımlandığı Sayı

IZ

Kaynak Göster