Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu

Bedrettin Savaş; Temel Öztürk; Ergül Meyvacı

doi:10.17798/bitlisfen.930943

Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu

Abstract

Poli(4-vinilbenzil-g-stiren) [poli(VB-g-S)] aşı kopolimeri tersinir katılmalı/ayrışmalı zincir transfer (RAFT) ve serbest radikal polimerizasyon (FRP) teknikleri kullanılarak sentez edildi. Bu amaç için, 4-vinilbenzil klorür monomeri kullanılarak FRP yöntemiyle poli(4-vinilbenzil klorür) [poli-4-VBC] polimeri sentezlendi. İkinci aşamada, poli-4-VBC polimeri ile potasyum etil ksantat reaksiyona sokularak makro-RAFT ajanı oluşturuldu. Son aşamada, RAFT tekniğiyle makro-RAFT ajanı varlığında stiren monomeriyle poli(VB-g-S) aşı kopolimeri sentez edildi. Sentezlenen ürünler 1H-NMR, FT-IR, TGA, SEM ve Dinamik Işık Saçılım (DLS) cihazları gibi spektroskopik ve termal analiz teknikleri kullanılarak karakterize edildi.

Keywords

References

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Details

Primary Language

Turkish

Subjects

Engineering

Journal Section

Research Article

Authors

Bedrettin Savaş ^*
0000-0002-6620-5493
Türkiye

Temel Öztürk
0000-0002-7856-9809
Türkiye

Ergül Meyvacı
0000-0003-3530-1316
Türkiye

Publication Date

September 17, 2021

Submission Date

May 1, 2021

Acceptance Date

September 1, 2021

Published in Issue

Year 2021 Volume: 10 Number: 3

DOI

https://doi.org/10.17798/bitlisfen.930943

IZ

https://izlik.org/JA48CT62GJ

Cite

RIS / Bibtex

APA

Savaş, B., Öztürk, T., & Meyvacı, E. (2021). Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi, 10(3), 849-857. https://doi.org/10.17798/bitlisfen.930943

AMA

1.Savaş B, Öztürk T, Meyvacı E. Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi. 2021;10(3):849-857. doi:10.17798/bitlisfen.930943

Chicago

Savaş, Bedrettin, Temel Öztürk, and Ergül Meyvacı. 2021. “Poli(4-Vinilbenzil-G-Stiren) Aşı Kopolimerinin RAFT Ve SRP Yöntemleriyle Sentezi Ve Karakterizasyonu”. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi 10 (3): 849-57. https://doi.org/10.17798/bitlisfen.930943.

EndNote

Savaş B, Öztürk T, Meyvacı E (September 1, 2021) Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi 10 3 849–857.

IEEE

[1]B. Savaş, T. Öztürk, and E. Meyvacı, “Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu”, Bitlis Eren Üniversitesi Fen Bilimleri Dergisi, vol. 10, no. 3, pp. 849–857, Sept. 2021, doi: 10.17798/bitlisfen.930943.

ISNAD

Savaş, Bedrettin - Öztürk, Temel - Meyvacı, Ergül. “Poli(4-Vinilbenzil-G-Stiren) Aşı Kopolimerinin RAFT Ve SRP Yöntemleriyle Sentezi Ve Karakterizasyonu”. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi 10/3 (September 1, 2021): 849-857. https://doi.org/10.17798/bitlisfen.930943.

JAMA

1.Savaş B, Öztürk T, Meyvacı E. Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi. 2021;10:849–857.

MLA

Savaş, Bedrettin, et al. “Poli(4-Vinilbenzil-G-Stiren) Aşı Kopolimerinin RAFT Ve SRP Yöntemleriyle Sentezi Ve Karakterizasyonu”. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi, vol. 10, no. 3, Sept. 2021, pp. 849-57, doi:10.17798/bitlisfen.930943.

Vancouver

1.Bedrettin Savaş, Temel Öztürk, Ergül Meyvacı. Poli(4-vinilbenzil-g-stiren) Aşı Kopolimerinin RAFT ve SRP Yöntemleriyle Sentezi ve Karakterizasyonu. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi. 2021 Sep. 1;10(3):849-57. doi:10.17798/bitlisfen.930943

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