Araştırma Makalesi
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Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories

Yıl 2023, , 143 - 148, 01.04.2023
https://doi.org/10.34248/bsengineering.1263291

Öz

High-quality alumina raw materials allow corundum-based brick and monolithics to perform to the full potential of alumina as a refractory material. Dense packing of the matrix to a submicron range and reduction of water demand of castables can be facilitated by a new family of multimodal reactive alumina. Dispersing aluminas ensure uniform mixing of dispersion and setting adjustment additives. In this study, fine reactive alumina powder production was investigated using Bayer gibbsite as a starting material. Experimental studies consist of two steps; in the first step, the soda content was reduced by means of boric acid and distilled water and then the powders obtained optimum conditions were ground in an attritor ball mill using distilled water for 8 hours. In the second step, physical characteristics such as rheological behaviours, bulk density, open porosity and thermal shock resistance, bending and compressive strength and fracture toughness in accordance with ASTM E399 standard were determined. Finally, KIC values of the refractory samples which was prepared with the reactive alumina produced from Seydişehir gibbsite were higher than that of the refractory mixture containing commercial reactive alumina obtained from a refractory company.

Destekleyen Kurum

Afyon Kocatepe Üniversitesi

Proje Numarası

BAPK-09.MUH.10.

Teşekkür

Bu çalışma Afyon Kocatepe Üniversitesi Bilimsel Araştırma Projeleri Koordinasyon Birimi tarafından BAPK-09.MUH.10 nolu proje ile desteklenmiştir. Çalışmaya olan önemli desteklerinden dolayı Prof. Dr. Ö. Faruk Emrullahoğlu'na teşekkür ederiz. Ayrıca dispersiyon alüminaları sağlayan Alisan firmasından Sayın İlker Bahçe'ye de teşekkürlerimizi sunarız.

Kaynakça

  • Akselrod MS, Bruni FJ. 2012. Modern trends in crystal growth and new applications of sapphire. J Crystal Growth, 360: 134-145.
  • Buhr A, Laurich J O. 2000. Synthetic alumina raw materials--key elements for innovative refractories. Metallurg Plant Technol Inter (Germany), 23(3): 62-64.
  • Chang PL, Wu YC, Lai SJ, Yen FS. 2009. Size effects on χ-to α-Al2O3 phase transformation. J European Ceramic Soc, 29(16): 3341-3348.
  • Fu X, Tang W, Ji L, Chen S. 2012. V2O5/Al2O3 composite photocatalyst: preparation, characterization, the role of Al2O3. Chem Engin J, 180:170-177.
  • Gogtas C, Lopez HF, Sobolev K. 2014. Role of cement content on the properties of self-flowing Al2O3 refractory castables. J European Ceramic Soc, 34(5): 1365-1373.
  • Göğtaş C, Ünlü N, Odabaşı A, Sezer L, Cınar F, Güner Ş, Göller G, Eruslu N. 2010. Preparation and characterisation of self-flowing refractory material containing 971U type microsilica. Advan Applied Ceramics, 109(1): 6-11.
  • Gürel SB, Altun A. 2009. Reactive alumina production for the refractory industry. Powder Technol, 196(2): 115-121.
  • Lee JS, Kim HS, Park NK, Lee TJ, Kang M. 2013. Low temperature synthesis of α-alumina from aluminum hydroxide hydrothermally synthesized using [Al(C2O4) x(OH) y] complexes. Chem Engin J, 230:351-360.
  • Lee W, Vieira W, Zhang S, Ahari KG, Sarpoolaky H, Parr C. 2001. Castable refractory concretes. Inter Materials Rev, 46(3): 145-167.
  • Luz A, Gabriel A, Consoni L, Aneziris C, Pandolfelli V. 2018. Self-reinforced high-alumina refractory castables. Ceramics Inter, 44(2): 2364-2375.
  • Ma W, Brown PW. 1999. Mechanisms of reaction of hydratable aluminas. J American Ceramic Soc, 82(2): 453-456.
  • Madono M. 1999. Alumina raw materials for the refractory industry. CN-Refractories, 6(3): 54-63.
  • Otroj S, Sagaeian A, Daghighi A, Nemati ZA. 2010. The effect of nano-size additives on the electrical conductivity of matrix suspension and properties of self-flowing low-cement high alumina refractory castables. Ceramics Inter, 36(4): 1411-1416.
  • Schnabel M, Buhr A, Kockegey-Lorenz R, Schmidtmeier D, Dutton J. 2014. Benefit of matrix alumina and modern dispersing systems in low cement castables. Interceram-Inter Ceramic Rev, 63:281-285.
  • Silva AP, Segadães AM, Pinto DG, Oliveira LA, Devezas TC. 2012. Effect of particle size distribution and calcium aluminate cement on the rheological behaviour of all-alumina refractory castables. Powder Technol, 226:107-113.
  • Xie ZP, Lu JW, Huang Y, Cheng YB. 2003. Influence of α-alumina seed on the morphology of grain growth in alumina ceramics from Bayer aluminum hydroxide. Materials Letters, 57(16-17): 2501-2508.
  • Zhu L, Liu L, Sun C, Zhang X, Zhang L, Gao Z, Ye G, Li H. 2020. Low temperature synthesis of polyhedral α-Al2O3 nanoparticles through two different modes of planetary ball milling. Ceramics Inter, 46(18): 28414-28421.

Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories

Yıl 2023, , 143 - 148, 01.04.2023
https://doi.org/10.34248/bsengineering.1263291

Öz

High-quality alumina raw materials allow corundum-based brick and monolithics to perform to the full potential of alumina as a refractory material. Dense packing of the matrix to a submicron range and reduction of water demand of castables can be facilitated by a new family of multimodal reactive alumina. Dispersing aluminas ensure uniform mixing of dispersion and setting adjustment additives. In this study, fine reactive alumina powder production was investigated using Bayer gibbsite as a starting material. Experimental studies consist of two steps; in the first step, the soda content was reduced by means of boric acid and distilled water and then the powders obtained optimum conditions were ground in an attritor ball mill using distilled water for 8 hours. In the second step, physical characteristics such as rheological behaviours, bulk density, open porosity and thermal shock resistance, bending and compressive strength and fracture toughness in accordance with ASTM E399 standard were determined. Finally, KIC values of the refractory samples which was prepared with the reactive alumina produced from Seydişehir gibbsite were higher than that of the refractory mixture containing commercial reactive alumina obtained from a refractory company.

Proje Numarası

BAPK-09.MUH.10.

Kaynakça

  • Akselrod MS, Bruni FJ. 2012. Modern trends in crystal growth and new applications of sapphire. J Crystal Growth, 360: 134-145.
  • Buhr A, Laurich J O. 2000. Synthetic alumina raw materials--key elements for innovative refractories. Metallurg Plant Technol Inter (Germany), 23(3): 62-64.
  • Chang PL, Wu YC, Lai SJ, Yen FS. 2009. Size effects on χ-to α-Al2O3 phase transformation. J European Ceramic Soc, 29(16): 3341-3348.
  • Fu X, Tang W, Ji L, Chen S. 2012. V2O5/Al2O3 composite photocatalyst: preparation, characterization, the role of Al2O3. Chem Engin J, 180:170-177.
  • Gogtas C, Lopez HF, Sobolev K. 2014. Role of cement content on the properties of self-flowing Al2O3 refractory castables. J European Ceramic Soc, 34(5): 1365-1373.
  • Göğtaş C, Ünlü N, Odabaşı A, Sezer L, Cınar F, Güner Ş, Göller G, Eruslu N. 2010. Preparation and characterisation of self-flowing refractory material containing 971U type microsilica. Advan Applied Ceramics, 109(1): 6-11.
  • Gürel SB, Altun A. 2009. Reactive alumina production for the refractory industry. Powder Technol, 196(2): 115-121.
  • Lee JS, Kim HS, Park NK, Lee TJ, Kang M. 2013. Low temperature synthesis of α-alumina from aluminum hydroxide hydrothermally synthesized using [Al(C2O4) x(OH) y] complexes. Chem Engin J, 230:351-360.
  • Lee W, Vieira W, Zhang S, Ahari KG, Sarpoolaky H, Parr C. 2001. Castable refractory concretes. Inter Materials Rev, 46(3): 145-167.
  • Luz A, Gabriel A, Consoni L, Aneziris C, Pandolfelli V. 2018. Self-reinforced high-alumina refractory castables. Ceramics Inter, 44(2): 2364-2375.
  • Ma W, Brown PW. 1999. Mechanisms of reaction of hydratable aluminas. J American Ceramic Soc, 82(2): 453-456.
  • Madono M. 1999. Alumina raw materials for the refractory industry. CN-Refractories, 6(3): 54-63.
  • Otroj S, Sagaeian A, Daghighi A, Nemati ZA. 2010. The effect of nano-size additives on the electrical conductivity of matrix suspension and properties of self-flowing low-cement high alumina refractory castables. Ceramics Inter, 36(4): 1411-1416.
  • Schnabel M, Buhr A, Kockegey-Lorenz R, Schmidtmeier D, Dutton J. 2014. Benefit of matrix alumina and modern dispersing systems in low cement castables. Interceram-Inter Ceramic Rev, 63:281-285.
  • Silva AP, Segadães AM, Pinto DG, Oliveira LA, Devezas TC. 2012. Effect of particle size distribution and calcium aluminate cement on the rheological behaviour of all-alumina refractory castables. Powder Technol, 226:107-113.
  • Xie ZP, Lu JW, Huang Y, Cheng YB. 2003. Influence of α-alumina seed on the morphology of grain growth in alumina ceramics from Bayer aluminum hydroxide. Materials Letters, 57(16-17): 2501-2508.
  • Zhu L, Liu L, Sun C, Zhang X, Zhang L, Gao Z, Ye G, Li H. 2020. Low temperature synthesis of polyhedral α-Al2O3 nanoparticles through two different modes of planetary ball milling. Ceramics Inter, 46(18): 28414-28421.
Toplam 17 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Research Articles
Yazarlar

Hatice Şule Çoban Tetik 0000-0002-4775-9706

Cemile Betül Emrullahoğlu Abi 0000-0003-0326-6122

Proje Numarası BAPK-09.MUH.10.
Yayımlanma Tarihi 1 Nisan 2023
Gönderilme Tarihi 10 Şubat 2023
Kabul Tarihi 29 Mart 2023
Yayımlandığı Sayı Yıl 2023

Kaynak Göster

APA Çoban Tetik, H. Ş., & Emrullahoğlu Abi, C. B. (2023). Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories. Black Sea Journal of Engineering and Science, 6(2), 143-148. https://doi.org/10.34248/bsengineering.1263291
AMA Çoban Tetik HŞ, Emrullahoğlu Abi CB. Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories. BSJ Eng. Sci. Nisan 2023;6(2):143-148. doi:10.34248/bsengineering.1263291
Chicago Çoban Tetik, Hatice Şule, ve Cemile Betül Emrullahoğlu Abi. “Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories”. Black Sea Journal of Engineering and Science 6, sy. 2 (Nisan 2023): 143-48. https://doi.org/10.34248/bsengineering.1263291.
EndNote Çoban Tetik HŞ, Emrullahoğlu Abi CB (01 Nisan 2023) Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories. Black Sea Journal of Engineering and Science 6 2 143–148.
IEEE H. Ş. Çoban Tetik ve C. B. Emrullahoğlu Abi, “Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories”, BSJ Eng. Sci., c. 6, sy. 2, ss. 143–148, 2023, doi: 10.34248/bsengineering.1263291.
ISNAD Çoban Tetik, Hatice Şule - Emrullahoğlu Abi, Cemile Betül. “Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories”. Black Sea Journal of Engineering and Science 6/2 (Nisan 2023), 143-148. https://doi.org/10.34248/bsengineering.1263291.
JAMA Çoban Tetik HŞ, Emrullahoğlu Abi CB. Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories. BSJ Eng. Sci. 2023;6:143–148.
MLA Çoban Tetik, Hatice Şule ve Cemile Betül Emrullahoğlu Abi. “Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories”. Black Sea Journal of Engineering and Science, c. 6, sy. 2, 2023, ss. 143-8, doi:10.34248/bsengineering.1263291.
Vancouver Çoban Tetik HŞ, Emrullahoğlu Abi CB. Production of Reactive Alumina from Domestic Sources and Its Use in Alumina-Based Self-Flowing Castable Refractories. BSJ Eng. Sci. 2023;6(2):143-8.

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