INVESTIGATION OF NATURAL ANALCIME-RICH ZEOLITE TUFF FROM TURKEY: A COMBINED XRD, XRF, FT-IR AND SEM STUDY

Yıl 2021, Cilt: 9 Sayı: Iconat Special Issue 2021, 36 - 41, 24.12.2021

Meryem Akbelen

https://doi.org/10.20290/estubtdb.1010189

Öz

In this study, chemical and structural properties of natural analcime-rich zeolite tuff from Turkey and that of ion-exchanged forms investigated. The microporous structure and the presence of extra-framework cations are of great importance for characterizing the unique properties of zeolites. Ion-exchanged forms (K+, H+ and Ca2+) of analcime zeolite were prepared with 1 M KNO3,1 M Ca(NO3)2 and 1 M HCl solutions in a shaker for 6 hours at 80 °C. The obtained samples were characterized by X-ray diffraction (XRD), X-ray fluorescence (XRF), Fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM) techniques. Quantitative XRD analysis showed that the major component of the natural zeolite was analcime, together with varying amounts of quartz, feldspar and clay mineral.

Anahtar Kelimeler

Natural zeolite, Analcime, XRF, XRD, FT-IR

Destekleyen Kurum

Eskişehir Teknik Üniversitesi Bilimsel Araştırma Projesi

Proje Numarası

20ADP231

Teşekkür

Financial support by Eskişehir Teknik University via Scientific Research Projects (No. 20ADP231 ) is acknowledged.

INVESTIGATION OF NATURAL ANALCIME-RICH ZEOLITE TUFF FROM TURKEY: A COMBINED XRD, XRF, FT-IR AND SEM STUDY

Öz

In this study, chemical and structural properties of natural analcime-rich zeolite tuff from Turkey and that of ion-exchanged forms investigated. The microporous structure and the presence of extra-framework cations are of great importance for characterizing the unique properties of zeolites. Ion-exchanged forms (K+, H+ and Ca2+) of analcime zeolite were prepared with 1 M KNO3,1 M Ca(NO3)2 and 1 M HCl solutions in a shaker for 6 hours at 80 °C. The obtained samples were characterized by X-ray diffraction (XRD), X-ray fluorescence (XRF), Fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM) techniques. Quantitative XRD analysis showed that the major component of the natural zeolite was analcime, together with varying amounts of quartz, feldspar and clay mineral.

Anahtar Kelimeler

Natural zeolite, Analcime, XRF, XRD, FT-IR

Proje Numarası

20ADP231

Kaynakça

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