BibTex RIS Kaynak Göster

Gold Nanoparticle Synthesis and Characterisation

Yıl 2009, Cilt: 37 Sayı: 3, 217 - 226, 01.08.2009

Öz

The aim of this study is to synthesize and characterize gold nanoparticles. For this purpose, the reduction reaction between tetrachloroauric acid and sodium citrate was used. At the end of the reduction reaction, gold nanoparticles with narrow size distribution were obtained. The initial gold concentration, trisodium citrate concentration and mixing rate were changed and their effects on particle size and size distribution were investigated. The optimal gold salt concentration, trisodium citrate concentration and mixing rate were found 0.06 mM, 0.17 mM and 450 rpm, respectively. Zeta sizer has been used to characterize and determine the size and size distribution of the synthesized gold nanoparticles.

Kaynakça

  • 1. Nanosystems, Molecular, Machinery, Manufacturing and Computation (Ed.: K. E. Drexler), Wiley, New York, 1992.
  • 2. DeSilva, A.P., Gunaratne, H.Q.N., McCoy, C.P., A molecular photoionic and gate based on fluorescent signalling, Nature, 364, 42, 1993.
  • 3. Göpel, W. Bioelectronics and nanotechnologies, Biosensors and Bioelectronics, 13, 723, 1998.
  • 4. Clusters and colloids. From Theory to Applications. Schmid, G. (Ed.), VCH Verlagsgesellschaft, Weinheim, 1994.
  • 5. Khairutdinov, R. F. Physical chemistry of nanocrystalline semiconductors, Colloid J. 59 (5), 535-548, 1997.
  • 6. Mulvaney, P., Surface Plasmon Spectroscopy of Nanosized Metal Particles, Langmuir, 12, 788-800, 1996.
  • 7. Lewis, L.N., Chemical catalysis by colloids and clusters, Chem. Rev., 93, 2693-2730, 1993.
  • 8. Fu-Ken, L., Aqueous-Organic Phase Transfer of Gold Nanoparticles and Gold Nanorods Using an Ionic Liquid J. Am. Chem. Soc., 126, 5036-5037, 2004.
  • 9. Meldrum, F.C., Flath, J., Knoll, W., Chemical Deposition of PbS on a Series of w-Functionalised Self-Assembled Monolayers, J. Mater. Chem., 9, 711-723, 1999.
  • 10. Link, S., Size and Temperature Dependence of the Plasmon Absorption of Colloidal Gold Nanoparticles, J. Phys. Chem. B, 103, 4212-4217, 1999.
  • 11. Han, S., Lin, J., Satjapipat, M., Baca, A.J., and Zhou, F., A Three-dimensional Heterogeneous DNA Sensing Surface Formed by Attaching OligodeoxynucleotideCapped Gold Nanoparticles onto a Gold Coated Quartz Crystal, Chem. Commun., 7, 609–610. 2001.
  • 12. Yamaguchi, S., and Shimomura, T., Adsorption, Immobilization, and Hybridization of DNA Studied by the Use of Quartz Crystal Oscillators, Anal. Chem., 65, 1925- 1927, 1999.
  • 13. Zhou, X.C., Huang, L.Q., Li, S.F.Y., Microgravimetric DNA sensor based on quartz crystal microbalance: comparison of oligonucleotide immobilization methods and the application in genetic diagnosis, Biosens. Bioelectron., 16(1-2), 85-95, 2001.
  • 14. Huang, H., Yang, X., Chitosan Mediated Assembly of Gold Nanoparticles Multilayer, Coll. Surf. A: Physicochem. Eng. Aspects, 226, 77–86, 2003.
  • 15. Shipway, A.N., Katz, E., Willner, I., Nanoparticle Arrays on Surfaces for Electronic, Optical, and Sensor Applications, ChemPhysChem, 1, 18-52, 2000.
  • 16. Nagasaki, Y., Kataoka, K., Ligand-installed PEGylated Bionanosphere. IEEE Proc.-Nanobiotechnol., 152(2), 89- 96, 2005.
  • 17. Xiao, Y., Ju, X., Chen, Y., Hydrogen Peroxide Sensor Based on Horseradish Peroxidase-Labeled Au Colloids Immobilized on Gold Electrode Surface by Cysteamine Monolayer. Anal. Chim. Acta, 391, 73-82, 1999.
  • 18. Turkevich, J., Colloidal Gold. Part I, Historical and Preparative Aspects, Morphology and Structure, Gold Bull., 18(3), 86-91, 1985.
  • 19. Liu, F.K., Hsieh, S.Y., Ko, F.H., Chu, T.C., Dai, B.T., Synthesis of Nanometer-Sized Poly(methyl methacrylate) Polymer Network by Gold Nanoparticle Template, Jpn. J. Appl. Phys. 42, 4147–4151, 2003.
  • 20. Hostettler, M.J., Wingate, J.E., Zhong, J., Alkanethiolate Gold Cluster Molecules with Core Diameters from 1.5 to 5.2 nm: Core and Monolayer Properties as a Function of Core Size, Langmuir, 14, 17-30, 1998.
  • 21. Tabrizi, Amir P.F., Production of Gold Nanoparticle and it is use in Quartz Crystal Microbalance System, M.Sc. Thesis, Hacettepe University, Bioengineering Dept., Beytepe, Ankara, Turkey, 2005.
Yıl 2009, Cilt: 37 Sayı: 3, 217 - 226, 01.08.2009

Öz

Kaynakça

  • 1. Nanosystems, Molecular, Machinery, Manufacturing and Computation (Ed.: K. E. Drexler), Wiley, New York, 1992.
  • 2. DeSilva, A.P., Gunaratne, H.Q.N., McCoy, C.P., A molecular photoionic and gate based on fluorescent signalling, Nature, 364, 42, 1993.
  • 3. Göpel, W. Bioelectronics and nanotechnologies, Biosensors and Bioelectronics, 13, 723, 1998.
  • 4. Clusters and colloids. From Theory to Applications. Schmid, G. (Ed.), VCH Verlagsgesellschaft, Weinheim, 1994.
  • 5. Khairutdinov, R. F. Physical chemistry of nanocrystalline semiconductors, Colloid J. 59 (5), 535-548, 1997.
  • 6. Mulvaney, P., Surface Plasmon Spectroscopy of Nanosized Metal Particles, Langmuir, 12, 788-800, 1996.
  • 7. Lewis, L.N., Chemical catalysis by colloids and clusters, Chem. Rev., 93, 2693-2730, 1993.
  • 8. Fu-Ken, L., Aqueous-Organic Phase Transfer of Gold Nanoparticles and Gold Nanorods Using an Ionic Liquid J. Am. Chem. Soc., 126, 5036-5037, 2004.
  • 9. Meldrum, F.C., Flath, J., Knoll, W., Chemical Deposition of PbS on a Series of w-Functionalised Self-Assembled Monolayers, J. Mater. Chem., 9, 711-723, 1999.
  • 10. Link, S., Size and Temperature Dependence of the Plasmon Absorption of Colloidal Gold Nanoparticles, J. Phys. Chem. B, 103, 4212-4217, 1999.
  • 11. Han, S., Lin, J., Satjapipat, M., Baca, A.J., and Zhou, F., A Three-dimensional Heterogeneous DNA Sensing Surface Formed by Attaching OligodeoxynucleotideCapped Gold Nanoparticles onto a Gold Coated Quartz Crystal, Chem. Commun., 7, 609–610. 2001.
  • 12. Yamaguchi, S., and Shimomura, T., Adsorption, Immobilization, and Hybridization of DNA Studied by the Use of Quartz Crystal Oscillators, Anal. Chem., 65, 1925- 1927, 1999.
  • 13. Zhou, X.C., Huang, L.Q., Li, S.F.Y., Microgravimetric DNA sensor based on quartz crystal microbalance: comparison of oligonucleotide immobilization methods and the application in genetic diagnosis, Biosens. Bioelectron., 16(1-2), 85-95, 2001.
  • 14. Huang, H., Yang, X., Chitosan Mediated Assembly of Gold Nanoparticles Multilayer, Coll. Surf. A: Physicochem. Eng. Aspects, 226, 77–86, 2003.
  • 15. Shipway, A.N., Katz, E., Willner, I., Nanoparticle Arrays on Surfaces for Electronic, Optical, and Sensor Applications, ChemPhysChem, 1, 18-52, 2000.
  • 16. Nagasaki, Y., Kataoka, K., Ligand-installed PEGylated Bionanosphere. IEEE Proc.-Nanobiotechnol., 152(2), 89- 96, 2005.
  • 17. Xiao, Y., Ju, X., Chen, Y., Hydrogen Peroxide Sensor Based on Horseradish Peroxidase-Labeled Au Colloids Immobilized on Gold Electrode Surface by Cysteamine Monolayer. Anal. Chim. Acta, 391, 73-82, 1999.
  • 18. Turkevich, J., Colloidal Gold. Part I, Historical and Preparative Aspects, Morphology and Structure, Gold Bull., 18(3), 86-91, 1985.
  • 19. Liu, F.K., Hsieh, S.Y., Ko, F.H., Chu, T.C., Dai, B.T., Synthesis of Nanometer-Sized Poly(methyl methacrylate) Polymer Network by Gold Nanoparticle Template, Jpn. J. Appl. Phys. 42, 4147–4151, 2003.
  • 20. Hostettler, M.J., Wingate, J.E., Zhong, J., Alkanethiolate Gold Cluster Molecules with Core Diameters from 1.5 to 5.2 nm: Core and Monolayer Properties as a Function of Core Size, Langmuir, 14, 17-30, 1998.
  • 21. Tabrizi, Amir P.F., Production of Gold Nanoparticle and it is use in Quartz Crystal Microbalance System, M.Sc. Thesis, Hacettepe University, Bioengineering Dept., Beytepe, Ankara, Turkey, 2005.
Toplam 21 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Bölüm Research Article
Yazarlar

Amir Tabrizi Bu kişi benim

Fatma Ayhan Bu kişi benim

Hakan Ayhan Bu kişi benim

Yayımlanma Tarihi 1 Ağustos 2009
Yayımlandığı Sayı Yıl 2009 Cilt: 37 Sayı: 3

Kaynak Göster

APA Tabrizi, A., Ayhan, F., & Ayhan, H. (2009). Gold Nanoparticle Synthesis and Characterisation. Hacettepe Journal of Biology and Chemistry, 37(3), 217-226.
AMA Tabrizi A, Ayhan F, Ayhan H. Gold Nanoparticle Synthesis and Characterisation. HJBC. Ağustos 2009;37(3):217-226.
Chicago Tabrizi, Amir, Fatma Ayhan, ve Hakan Ayhan. “Gold Nanoparticle Synthesis and Characterisation”. Hacettepe Journal of Biology and Chemistry 37, sy. 3 (Ağustos 2009): 217-26.
EndNote Tabrizi A, Ayhan F, Ayhan H (01 Ağustos 2009) Gold Nanoparticle Synthesis and Characterisation. Hacettepe Journal of Biology and Chemistry 37 3 217–226.
IEEE A. Tabrizi, F. Ayhan, ve H. Ayhan, “Gold Nanoparticle Synthesis and Characterisation”, HJBC, c. 37, sy. 3, ss. 217–226, 2009.
ISNAD Tabrizi, Amir vd. “Gold Nanoparticle Synthesis and Characterisation”. Hacettepe Journal of Biology and Chemistry 37/3 (Ağustos 2009), 217-226.
JAMA Tabrizi A, Ayhan F, Ayhan H. Gold Nanoparticle Synthesis and Characterisation. HJBC. 2009;37:217–226.
MLA Tabrizi, Amir vd. “Gold Nanoparticle Synthesis and Characterisation”. Hacettepe Journal of Biology and Chemistry, c. 37, sy. 3, 2009, ss. 217-26.
Vancouver Tabrizi A, Ayhan F, Ayhan H. Gold Nanoparticle Synthesis and Characterisation. HJBC. 2009;37(3):217-26.

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