Araştırma Makalesi
PDF Zotero Mendeley EndNote BibTex Kaynak Göster

Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film

Yıl 2021, Cilt 7, Sayı 1, 9 - 12, 31.03.2021
https://doi.org/10.22399/ijcesen.727304

Öz

The sol-gel process is an innovative advanced method, initially developed to synthesize glass and ceramics at low temperature. Sol-gel process can be used to synthesis materials with a variety of shapes, such as porous membranes, thin fibers, nano-size powders and thin films. In this study, epoxy and methacrylate based silane coupling agents are used together with zirconium oxide to form a hybrid coating system on glass surface. In the experimental study, an organic–inorganic molecular hybrid compound was prepared by sol-gel method. First glasses were cleaned by traditional piranha solution (3:1 H2SO4 : H2O2) to remove contaminants. Silanization was applied to increase the adhesion of hybrid coatings on glass substrates. Glass substrate was coated with this solution by a homemade dip-coater. In this study, (3-Glycidoxypropyltrimethoxysilane, GLYMO and 3-(trimethoxysilyl)propylmethacrylate, TMSPM) were chosen as a silane. Zirconia is inorganic component of hybrid materails. Coated samples were characterized by Fouirer Transform Infrared Spectrophotometer (FTIR), Scanning Electron Microscope with Energy Dispersive X-ray Spectroscopy (SEM-EDX) and Contact Angle Goniometer.

Kaynakça

  • [1] Garcia J. C., Scolfaro L. M. R., Lino A. T., Freire V. N., Farias G. A., Silva C. C., Leite Alves H. W., Rodrigues S. C. P. and da Silva Jr E. F.. “Structural, electronic, and optical properties of ZrO2 from ab initio calculations” Journal of Applied Physics 100, 104103 (2006) Doi:10.1063/1.2386967 [2] Ciuparu D., Ensuque A., Shafeev G., Bozon-Verduraz F. “Synthesis and apparent bandgap of nanophase zirconia” Journal Of Materials Science Letters 19 (2000) 931– 933. Doi:10.1023/A:1006799701474 [3] Patel U.S., Patel K.H., Chauhan K.V., Chawla A.K., Rawal S.K. “Investigation of various properties for zirconium oxide films synthesized by sputtering” Procedia Technology 23 ( 2016 ) 336 – 343. Doi:10.1016/j.protcy.2016.03.035 [4] Adnan M. M., Dalod A. R. M., Balci M.H., Glaum J. and Einarsrud M.A. “In Situ Synthesis of Hybrid Inorganic–Polymer Nanocomposites” Polymers 10 (2018) 1129. Doi:10.3390/polym10101129 [5] Yedikardeş F.B. “Preparation And Characterization Of Anti Bacterial, Anti Scratch And Easy To Clean Multifunctional Coatings By Sol Gel Method”, M.Sc. Thesis, ITU, June 2016 [6] Bezir N. Çiçek, Evcin A., Kayali R., Özen M.K., Balyaci G. “Comparison of Pure and Doped TiO2 Thin Films Prepared by Sol-Gel Spin-Coating Method” ACTA PHYSICA POLONICA A, 132 (2017) page 620-624 Doi:10.12693/APhysPolA.132.620 [7] Adamczyk A., “The influence of ZrO2 precursor type on the structure of ZrO2-TiO2-SiO2 gels and selected thin films”, Journal of Molecular Structure 1171 (2018) 706-716 Doi:10.1016/j.molstruc.2018.06.068 [8] Halbus A.F., Horozov T.S. and Paunov V.N. “Self-grafting copper oxide nanoparticles show a strong enhancement of their anti-algal and anti-yeast action” Nanoscale Advances 1 (2019) 2323-2336 Doi:10.1039/c9na00099b [9] Vengadaesvaran B., Arun N., Chanthiriga R., Bushroa A. R., Ramis Rau S., Ramesh K., Vikneswaran R., Alshabeeb G. H. E., Ramesh S. and Arof A. K., “Scratch resistance enhancement of 3-glycidyloxypropyltrimethoxysilane coating incorporated with silver nanoparticles” Surface Engineering 30 (2014) 177-182 Doi:10.1179/1743294413Y.0000000238 [10] Lee M.H., Min B.K., Son J.S. and Kwon T.Y. “Influence of Different Post-Plasma Treatment Storage Conditions on the Shear Bond Strength of Veneering Porcelain to Zirconia” Materials 9:43 (2016) 2-12. Doi:10.3390/ma9010043 [11] Bezir N. Çiçek, Evcin A., Kayali R., Kaşikçi Özen M., Esen K., Cambaz E.B. “Characteristic Properties of Dy-Eu-Ce Co-Doped ZrO2 Nanofibers Fabricated via Electrospinning”, Acta Physica Polonica A, 130, 1 (2016) 300-303 Doi:10.12693/APhysPolA.130.300 [12] Hassanien A.S., Akl A.A. “Effect of Se addition on optical and electrical properties of chalcogenide CdSSe thin films” Superlattices and Microstructures 89 (2016) 153-169 Doi:10.1016/j.spmi.2015.10.044

Yıl 2021, Cilt 7, Sayı 1, 9 - 12, 31.03.2021
https://doi.org/10.22399/ijcesen.727304

Öz

Kaynakça

  • [1] Garcia J. C., Scolfaro L. M. R., Lino A. T., Freire V. N., Farias G. A., Silva C. C., Leite Alves H. W., Rodrigues S. C. P. and da Silva Jr E. F.. “Structural, electronic, and optical properties of ZrO2 from ab initio calculations” Journal of Applied Physics 100, 104103 (2006) Doi:10.1063/1.2386967 [2] Ciuparu D., Ensuque A., Shafeev G., Bozon-Verduraz F. “Synthesis and apparent bandgap of nanophase zirconia” Journal Of Materials Science Letters 19 (2000) 931– 933. Doi:10.1023/A:1006799701474 [3] Patel U.S., Patel K.H., Chauhan K.V., Chawla A.K., Rawal S.K. “Investigation of various properties for zirconium oxide films synthesized by sputtering” Procedia Technology 23 ( 2016 ) 336 – 343. Doi:10.1016/j.protcy.2016.03.035 [4] Adnan M. M., Dalod A. R. M., Balci M.H., Glaum J. and Einarsrud M.A. “In Situ Synthesis of Hybrid Inorganic–Polymer Nanocomposites” Polymers 10 (2018) 1129. Doi:10.3390/polym10101129 [5] Yedikardeş F.B. “Preparation And Characterization Of Anti Bacterial, Anti Scratch And Easy To Clean Multifunctional Coatings By Sol Gel Method”, M.Sc. Thesis, ITU, June 2016 [6] Bezir N. Çiçek, Evcin A., Kayali R., Özen M.K., Balyaci G. “Comparison of Pure and Doped TiO2 Thin Films Prepared by Sol-Gel Spin-Coating Method” ACTA PHYSICA POLONICA A, 132 (2017) page 620-624 Doi:10.12693/APhysPolA.132.620 [7] Adamczyk A., “The influence of ZrO2 precursor type on the structure of ZrO2-TiO2-SiO2 gels and selected thin films”, Journal of Molecular Structure 1171 (2018) 706-716 Doi:10.1016/j.molstruc.2018.06.068 [8] Halbus A.F., Horozov T.S. and Paunov V.N. “Self-grafting copper oxide nanoparticles show a strong enhancement of their anti-algal and anti-yeast action” Nanoscale Advances 1 (2019) 2323-2336 Doi:10.1039/c9na00099b [9] Vengadaesvaran B., Arun N., Chanthiriga R., Bushroa A. R., Ramis Rau S., Ramesh K., Vikneswaran R., Alshabeeb G. H. E., Ramesh S. and Arof A. K., “Scratch resistance enhancement of 3-glycidyloxypropyltrimethoxysilane coating incorporated with silver nanoparticles” Surface Engineering 30 (2014) 177-182 Doi:10.1179/1743294413Y.0000000238 [10] Lee M.H., Min B.K., Son J.S. and Kwon T.Y. “Influence of Different Post-Plasma Treatment Storage Conditions on the Shear Bond Strength of Veneering Porcelain to Zirconia” Materials 9:43 (2016) 2-12. Doi:10.3390/ma9010043 [11] Bezir N. Çiçek, Evcin A., Kayali R., Kaşikçi Özen M., Esen K., Cambaz E.B. “Characteristic Properties of Dy-Eu-Ce Co-Doped ZrO2 Nanofibers Fabricated via Electrospinning”, Acta Physica Polonica A, 130, 1 (2016) 300-303 Doi:10.12693/APhysPolA.130.300 [12] Hassanien A.S., Akl A.A. “Effect of Se addition on optical and electrical properties of chalcogenide CdSSe thin films” Superlattices and Microstructures 89 (2016) 153-169 Doi:10.1016/j.spmi.2015.10.044

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Research Articles
Yazarlar

Atilla EVCİN (Sorumlu Yazar)
AFYON KOCATEPE ÜNİVERSİTESİ, MÜHENDİSLİK FAKÜLTESİ, MALZEME BİLİMİ VE MÜHENDİSLİĞİ BÖLÜMÜ
0000-0002-0163-5097
Türkiye


Harun GÜNEY
AGRI IBRAHIM CECEN UNIVERSITY
0000-0001-9877-2591
Türkiye


Nalan BEZİR
SÜLEYMAN DEMİREL ÜNİVERSİTESİ, FEN-EDEBİYAT FAKÜLTESİ, FİZİK BÖLÜMÜ
0000-0002-5708-1521
Türkiye

Yayımlanma Tarihi 31 Mart 2021
Başvuru Tarihi 26 Nisan 2020
Kabul Tarihi 11 Mart 2021
Yayınlandığı Sayı Yıl 2021, Cilt 7, Sayı 1

Kaynak Göster

Bibtex @araştırma makalesi { ijcesen727304, journal = {International Journal of Computational and Experimental Science and Engineering}, issn = {}, eissn = {2149-9144}, address = {}, publisher = {İskender AKKURT}, year = {2021}, volume = {7}, pages = {9 - 12}, doi = {10.22399/ijcesen.727304}, title = {Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film}, key = {cite}, author = {Evcin, Atilla and Güney, Harun and Bezir, Nalan} }
APA Evcin, A. , Güney, H. & Bezir, N. (2021). Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film . International Journal of Computational and Experimental Science and Engineering , 7 (1) , 9-12 . DOI: 10.22399/ijcesen.727304
MLA Evcin, A. , Güney, H. , Bezir, N. "Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film" . International Journal of Computational and Experimental Science and Engineering 7 (2021 ): 9-12 <https://dergipark.org.tr/tr/pub/ijcesen/issue/57886/727304>
Chicago Evcin, A. , Güney, H. , Bezir, N. "Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film". International Journal of Computational and Experimental Science and Engineering 7 (2021 ): 9-12
RIS TY - JOUR T1 - Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film AU - Atilla Evcin , Harun Güney , Nalan Bezir Y1 - 2021 PY - 2021 N1 - doi: 10.22399/ijcesen.727304 DO - 10.22399/ijcesen.727304 T2 - International Journal of Computational and Experimental Science and Engineering JF - Journal JO - JOR SP - 9 EP - 12 VL - 7 IS - 1 SN - -2149-9144 M3 - doi: 10.22399/ijcesen.727304 UR - https://doi.org/10.22399/ijcesen.727304 Y2 - 2021 ER -
EndNote %0 International Journal of Computational and Experimental Science and Engineering Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film %A Atilla Evcin , Harun Güney , Nalan Bezir %T Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film %D 2021 %J International Journal of Computational and Experimental Science and Engineering %P -2149-9144 %V 7 %N 1 %R doi: 10.22399/ijcesen.727304 %U 10.22399/ijcesen.727304
ISNAD Evcin, Atilla , Güney, Harun , Bezir, Nalan . "Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film". International Journal of Computational and Experimental Science and Engineering 7 / 1 (Mart 2021): 9-12 . https://doi.org/10.22399/ijcesen.727304
AMA Evcin A. , Güney H. , Bezir N. Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film. IJCESEN. 2021; 7(1): 9-12.
Vancouver Evcin A. , Güney H. , Bezir N. Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film. International Journal of Computational and Experimental Science and Engineering. 2021; 7(1): 9-12.
IEEE A. Evcin , H. Güney ve N. Bezir , "Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film", International Journal of Computational and Experimental Science and Engineering, c. 7, sayı. 1, ss. 9-12, Mar. 2021, doi:10.22399/ijcesen.727304

All publised articles in IJCESEN are licensed under under the Creative Commons NoncCommercial 4.0. International LicenseCreative Commons Lisansı