Araştırma Makalesi
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Preparation and characterization of ZSM-5 zeolite

Yıl 2023, Cilt: 9 Sayı: 2, 156 - 160, 30.06.2023
https://doi.org/10.22399/ijcesen.1280939

Öz

Recently, zeolites attracted considerable research attention because they exhibit adsorption properties, ion exchange capabilities and a good catalytic property, a specific pore size distribution; a unique chemical and thermal properties and several applications.
Actually zeolites play a crucial role as a catalyst to capture and convert Carbone dioxide into valuable products.
In the present work, hydrothermal synthesis of ZSM-5 zeolite crystals, with composition of the chemical products 0.01 Al2O3,1SiO2,2 NaOH, 0.15 TPABr, 18.34 H2O at 170°C for 48 hours (2 days) at Ph 11 is described.
Results of characterization of the ZSM-5 zeolite by XRD, FTIR, EDAX, SEM, TGA, are presented and discussed.

Destekleyen Kurum

Dgrsdt, crtse

Teşekkür

dgrsdt,crtse

Kaynakça

  • [1] Petrov, I., & Michalev, T. (2012). Synthesis of zeolite A: a review. Научни трудове на русенския университет, 51; 30-35.
  • [2] Ruiz, A., Brühwiler, D., Ban, T. et al (2005). Synthesis of Zeolite L. Tuning Size and Morphology. Monatshefte für Chemie 136; 77–8.
  • [3] SMAIL, Heman A., REHAN, Mohammad, SHAREEF, Kafia M., et al. (2019). Synthesis of uniform mesoporous zeolite ZSM-5 catalyst for friedel-crafts acylation. Chem Engineering, 3(2):35.
  • [4] Ren, Z., Wang, L., Li, Y., Zha, J., Tian, G., Wang, F.,Liang, J. (2022). Synthesis of zeolites by in-situ conversion of geopolymers and their performance of heavy metal ion removal in wastewater: A review. Journal of Cleaner Production, 131441.
  • [5]Houhoune, F., Khemaissia, S., Nibou, D., Chegrouche, S., & Menacer, S. (2018, August). Kinetic study and sorption mechanism of uranium (VI) onto NaY zeolite. In AIP Conference Proceedings (Vol. 1994, No. 1, p. 070008). AIP Publishing LLC.
  • [6]Baouali, N. Y., Nibou, D., & Amokrane, S. (2022). NaY Zeolite and TiO2 Impregnated NaY Zeolite for the Adsorption and Photocatalytic Degradation of Methylene Blue under Sunlight. Iran. J. Chem. Chem. Eng. Research Article 41(6).
  • [7] Lee, J. S., Lee, Y. J., Tae, E. L., Park, Y. S., & Yoon, K. B. (2003). Synthesis of zeolite as ordered multicrystal arrays. Science, 301(5634);818-821.
  • [8] Wang, X., Ma, Y., Wu, Q., Wen, Y., & Xiao, F. S. (2022). Zeolite nanosheets for catalysis. Chemical Society Reviews.
  • [9] Kosinov, N., & Hensen, E. J. (2020). Reactivity, Selectivity, and Stability of Zeolite‐Based Catalysts for Methane Dehydroaromatization. Advanced Materials, 32(44); 2002565.
  • [10] Jonscher, C., Seifert, M., Kretzschmar, N., Marschall, M. S., Le Anh, M., Doert, T.,& Weigand, J. J. (2022). Origin of Morphology Change and Effect of Crystallization Time and Si/Al Ratio during Synthesis of Zeolite ZSM‐5. ChemCatChem, 14(3); e202101248.
  • [11] REN, Nan, SUBOTIĆ, Boris, BRONIĆ, Josip, et al. (2012) Unusual pathway of crystallization of zeolite ZSM-5 in a heterogeneous system: phenomenology and starting considerations. Chemistry of Materials, 24(10);1726-1737.
  • [12]SADOWSKA, K., WACH, Anna, OLEJNICZAK, Zbigniew, et al. (2013). Hierarchic zeolites: Zeolite ZSM-5 desilicated with NaOH and NaOH/tetrabutylamine hydroxide. Microporous and Mesoporous Materials, 167;82-88.
  • [13]CONTE, Marco, LOPEZ-SANCHEZ, Jose A., HE, Qian, et al. (2012). Modified zeolite ZSM-5 for the methanol to aromatics reaction. Catalysis Science & Technology 2(1);105-112.
  • [14]KAMALUDDIN, Huda Sharbini, GONG, Xuan, MA, Pandong, et al. (2022). Influence of zeolite ZSM-5 synthesis protocols and physicochemical properties in the methanol-to-olefin process. Materials Today Chemistry, 26;101061.
  • [15] JEDLI, Hedi, ALMONEEF, M. M., MBAREK, Mohamed, et al. (2022). Adsorption of CO2 onto zeolite ZSM-5: Kinetic, equilibrium and thermodynamic studies. Fuel, 321;124097.
Yıl 2023, Cilt: 9 Sayı: 2, 156 - 160, 30.06.2023
https://doi.org/10.22399/ijcesen.1280939

Öz

Kaynakça

  • [1] Petrov, I., & Michalev, T. (2012). Synthesis of zeolite A: a review. Научни трудове на русенския университет, 51; 30-35.
  • [2] Ruiz, A., Brühwiler, D., Ban, T. et al (2005). Synthesis of Zeolite L. Tuning Size and Morphology. Monatshefte für Chemie 136; 77–8.
  • [3] SMAIL, Heman A., REHAN, Mohammad, SHAREEF, Kafia M., et al. (2019). Synthesis of uniform mesoporous zeolite ZSM-5 catalyst for friedel-crafts acylation. Chem Engineering, 3(2):35.
  • [4] Ren, Z., Wang, L., Li, Y., Zha, J., Tian, G., Wang, F.,Liang, J. (2022). Synthesis of zeolites by in-situ conversion of geopolymers and their performance of heavy metal ion removal in wastewater: A review. Journal of Cleaner Production, 131441.
  • [5]Houhoune, F., Khemaissia, S., Nibou, D., Chegrouche, S., & Menacer, S. (2018, August). Kinetic study and sorption mechanism of uranium (VI) onto NaY zeolite. In AIP Conference Proceedings (Vol. 1994, No. 1, p. 070008). AIP Publishing LLC.
  • [6]Baouali, N. Y., Nibou, D., & Amokrane, S. (2022). NaY Zeolite and TiO2 Impregnated NaY Zeolite for the Adsorption and Photocatalytic Degradation of Methylene Blue under Sunlight. Iran. J. Chem. Chem. Eng. Research Article 41(6).
  • [7] Lee, J. S., Lee, Y. J., Tae, E. L., Park, Y. S., & Yoon, K. B. (2003). Synthesis of zeolite as ordered multicrystal arrays. Science, 301(5634);818-821.
  • [8] Wang, X., Ma, Y., Wu, Q., Wen, Y., & Xiao, F. S. (2022). Zeolite nanosheets for catalysis. Chemical Society Reviews.
  • [9] Kosinov, N., & Hensen, E. J. (2020). Reactivity, Selectivity, and Stability of Zeolite‐Based Catalysts for Methane Dehydroaromatization. Advanced Materials, 32(44); 2002565.
  • [10] Jonscher, C., Seifert, M., Kretzschmar, N., Marschall, M. S., Le Anh, M., Doert, T.,& Weigand, J. J. (2022). Origin of Morphology Change and Effect of Crystallization Time and Si/Al Ratio during Synthesis of Zeolite ZSM‐5. ChemCatChem, 14(3); e202101248.
  • [11] REN, Nan, SUBOTIĆ, Boris, BRONIĆ, Josip, et al. (2012) Unusual pathway of crystallization of zeolite ZSM-5 in a heterogeneous system: phenomenology and starting considerations. Chemistry of Materials, 24(10);1726-1737.
  • [12]SADOWSKA, K., WACH, Anna, OLEJNICZAK, Zbigniew, et al. (2013). Hierarchic zeolites: Zeolite ZSM-5 desilicated with NaOH and NaOH/tetrabutylamine hydroxide. Microporous and Mesoporous Materials, 167;82-88.
  • [13]CONTE, Marco, LOPEZ-SANCHEZ, Jose A., HE, Qian, et al. (2012). Modified zeolite ZSM-5 for the methanol to aromatics reaction. Catalysis Science & Technology 2(1);105-112.
  • [14]KAMALUDDIN, Huda Sharbini, GONG, Xuan, MA, Pandong, et al. (2022). Influence of zeolite ZSM-5 synthesis protocols and physicochemical properties in the methanol-to-olefin process. Materials Today Chemistry, 26;101061.
  • [15] JEDLI, Hedi, ALMONEEF, M. M., MBAREK, Mohamed, et al. (2022). Adsorption of CO2 onto zeolite ZSM-5: Kinetic, equilibrium and thermodynamic studies. Fuel, 321;124097.
Toplam 15 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Bölüm Araştırma Makalesi
Yazarlar

Sabiha Anas Boussaa 0000-0003-2384-0056

Djamel Nibou Bu kişi benim

Karime Benfadel Bu kişi benim

Lamia Talbi Bu kişi benim

Assia Boukezzata Bu kişi benim

Yahia Ouadah Bu kişi benim

Djaouida Allam Bu kişi benim

Yayımlanma Tarihi 30 Haziran 2023
Gönderilme Tarihi 17 Nisan 2023
Kabul Tarihi 8 Haziran 2023
Yayımlandığı Sayı Yıl 2023 Cilt: 9 Sayı: 2

Kaynak Göster

APA Anas Boussaa, S., Nibou, D., Benfadel, K., Talbi, L., vd. (2023). Preparation and characterization of ZSM-5 zeolite. International Journal of Computational and Experimental Science and Engineering, 9(2), 156-160. https://doi.org/10.22399/ijcesen.1280939