Performance Investigation of Diatomite Modified Asphalt Mixtures for Different Diatomite Ratios and Grinding Sizes

Öz

Modification of asphalt mixtures has become almost mandatory today due to increased stresses in pavements, shortening of load cycle times, and decreases in binder quality. For this reason, many additives can be added to bitumen or asphalt mixture. Industrial material wastes can also be among these additives. When diatomite material is used as a performance enhancer in asphalt mixtures, it significantly improves the main performance indicators of the asphalt mixture. However, low temperature cracking of diatomite-modified asphalt mixtures is still controversial in the literature. This study evaluated the asphalt mixture in terms of low-temperature cracking, water damage, and rutting, depending on the diatomite grinding size (gradation) and addition ratio. Three different sizes of diatomite additives (106, 212 and 300-micron maximum diameter) were used at three addition ratios (5, 10 and 15% by weight of bitumen). According to the test results, it was seen that the mechanical properties of asphalt mixtures were significantly affected by the addition ratios and diatomite sizes, and the use of 300-micron maximum diameter diatomite at the rate of 10% and 15% was more effective. However, according to the BBR test results, the use of diatomite additives with a maximum size of 106 µm at 5% slightly increased the low temperature cracking resistance.

Anahtar Kelimeler

• Asphalt mixture
• diatomite
• grinding size
• cracking
• low temperature cracking

Kaynakça

1. U.S. Department of the Interior, Mineral Commodity Summaries 2023, U.S. Geological Survey, Reston, Virginia, USA., 2023.
2. Cameron., N. G., Diatoms, Encyclopedia of Quaternary Science (Second Edition), Elsevier, 522-525, 2013.
3. Jiang, L., Liu, Q. L., Application of Diatomite Modified Asphalt. Applied Mechanics and Materials, 477-478, 959–963, 2013.
4. Cong, P., Chen, S., Chen, H., Effects of Diatomite on the Properties of Asphalt Binder. Constr. Build. Mater., 30, 495–499, 2012.
5. Cong, P., Liu, N., Tian, Yu., Zhang, Y., Effects of Long-term Aging on the Properties of Asphalt Binder Containing Diatoms. Constr. Build. Mater., 123, 534–540, 2016.
6. Cheng, Y., Tao, J., Jiao, Y., Tan, G., Guo, Q., Wang, S., Ni, P., Influence of the Properties of Filler on High and Medium Temperature Performances of Asphalt Mastic. Constr. Build. Mater., 118, 268–275, 2016.
7. Cheng, Y., Li, L., Zhang, Y., Lv, Z., Zhu C., Quantitative Analysis of Effect and Interaction of Diatomite and Basalt Fiber on Asphalt Performance. J. Mater. Civ. Eng., 31 (12), 04019306, 2019.
8. Cheng, Y. C., Tao, J. L., Jiao, Y. B., Guo, Q. L., Li, C., Influence of Diatomite and Mineral Powder on Thermal Oxidative Ageing Properties of Asphalt. Adv. Mater. Sci. Eng., 2015, 1-10, 2015.

9. Wang, H., Li, H., Zhang, H., Zhang, X., Guo, B., Yu, B., Liu, L., Tian, Y., Experimental Study on the Aging Behavior of Modified Asphalt with Different Types of Fine Solid Wastes Under Different Aging Conditions. Constr. Build. Mater., 291, 123308, 2021.
10. Zhang, P., Guo, Q., Tao, J., Ma, D., Wang, Y., Aging Mechanism of a Diatomite- modified Asphalt Binder Using Fourier-transform Infrared (FTIR) Spectroscopy Analysis. Materials, 12 (6), 988, 2019.
11. Song, Y., Che, J., Zhang, Y., The Interacting Rule of Diatomite and Asphalt Groups. Pet. Sci. Technol., 29 (3), 254–259, 2011.
12. Tian, Y., Sun, L., Li, H., Zhang, H., Harvey, J., Yang, B., Zhu, Y., Yu, B., Fu, K., Laboratory Investigation on Effects of Solid Waste Filler on Mechanical Properties of Porous Asphalt Mixture. Constr. Build. Mater., 279, 122436, 2021.
13. Chen, X. L., Sun, Y. S., Han, Y. X., Zhang, B., The Research on the Performance of Asphalt Mastics Modified by Mineral Fillers. Advanced Materials Research, 158, 287–297, 2010.
14. Mohd Shukry, N. A., Abdul Hassan, N., Abdullah, M. E., Hainin, M. R., Yusoff, N. I. M., Mahmud, M. Z. H., Putra Jaya, R., Warid, M. N. M., Mohd, Satar, M. K. I., Influence of Diatomite Filler on Rheological Properties of Porous Asphalt Mastic. Int. J. Pavement Eng., 21 (4), 428–436, 2018.
15. Mohd Shukry, N. A., Hassan, N. A., Abdullah, M. E., Hainin, M. R., Md Yusoff, N. I., Jaya, R. P., Mohamed, A., Effect of Various Filler Types on the Properties of Porous Asphalt Mixture. IOP Conf. Ser.: Mater. Sci. Eng., 342, 012036, 2018.
16. Aslan, S., Aktas, B., Use of Diatomite and Pumice as Stabilizers in Stone Mastic Asphalt Mixtures. Rev. Constr., 17 (3), 531–541, 2019.
17. Yi-qiu, T., Lei, Z., Xing-you, Z., Investigation of Low-temperature Properties of Diatomite-modified Asphalt Mixtures. Constr. Build. Mater., 36, 787–795, 2012.
18. Yang, C., Xie, J., Zhou, X., Liu, Q., Pang, L., Performance Evaluation and Improving Mechanisms of Diatomite-modified Asphalt Mixture. Materials, 11 (5), 686, 2018.
19. Sun, Y. S., Chen, X. L., Han, Y. X., Zhang, B., Research on Performance of the Modified Asphalt by Diatomite-cellulose Composite. Advanced Materials Research, 158, 211–218, 2010.
20. Wu, C., Li, L., Cheng, Y., Gu, Z., Lv, Z., Wang, R., Guan, B., Effect of Diatomite and Basalt Fibers on Pavement Performance and Vibration Attenuation of Waste Tires Rubber-modified Asphalt Mixtures. Math. Probl. Eng., 2020, 1–13, 2020.
21. Jin, J., Tan, Y., Liu, R., Zheng, J., Zhang, J., Synergy Effect of Attapulgite, Rubber, and Diatomite on Organic Montmorillonite-modified Asphalt. J. Mater. Civ. Eng., 31(2), 04018388, 2019.
22. Wei, H., He, Q., Jiao, Y., Chen, J., Hu, M., Evaluation of Anti-icing Performance for Crumb Rubber and Diatomite Compound Modified Asphalt Mixture. Constr. Build. Mater., 107, 109-116, 2016.
23. Baldi-Sevilla, A., Montero, M. L., Aguiar, J. P., Loría, L. G., Influence of Nanosilica and Diatomite on the Physicochemical and Mechanical Properties of Binder at Unaged and Oxidized Conditions. Constr. Build. Mater., 127, 176-182, 2016.
24. Davar, A., Tanzadeh, J., Fadaee, O., Experimental Evaluation of the Basalt Fibers and Diatomite Powder Compound on Enhanced Fatigue Life and Tensile Strength of Hot Mix Asphalt at Low Temperatures. Constr. Build. Mater., 153, 238-246, 2017.
25. Huang, W. T., Wang, D. Y., He, P. Y., Long, X., Tong, B., Tian, J., Yu, P., Rheological Characteristics Evaluation of Bitumen Composites Containing Rock Asphalt and Diatomite. Appl. Sci.-Basel, 9 (5), 1023, 2019.
26. Wang, H., Liu, Q., Wu, S., Lv, Y., Wan, P., Gong, X., Liu, G., Study of Synergistic Effect of Diatomite and Modified Attapulgite on Reducing Asphalt Volatile Organic Compounds Emission. Constr. Build. Mater., 400, 132827, 2023.
27. Tan, B., Su, Y., Fan, Y., Zhang, W., Li, Q., Preparation and Road Performance Study of Rubber–Diatomite Composite Modified Asphalt Mixture. Materials, 16, 7359, 2023.
28. Li, Y., He, T., Tang, J., Performance Evaluation of Asphalt Binders Incorporating Surface-Modified Diatomite and Bio-Oil: A Value-Added Utilization of Natural Resource. Case Stud. Constr. Mater., e02988, 2024.
29. Aksoy, A., Aslan, M. T., Iskender, E., Ayyildiz, D., Sengul, C. E., Evaluation of Asphalt Pavement Performance for Different Diatomite Content. Journal of Engineering and Architecture Faculty of Eskisehir Osmangazi University, 31(3), 893-904, 2023.
30. Highway Technical Specification, General Directorate of Highways, Ankara, (2013).
31. Zhou, Z., Experimental Study on Mix Design of Diatomite Modified Asphalt Mixture. Master’s Thesis, Jilin University, Changchun, China, 2018.
32. Yin, H. Y., Research on the Modification Mechanism of Diatomite and Dry Mixing of Diatomite-Modified Asphalt Miture. Master’s Thesis, Chongqing Jiaotong University, Chongqing, China, 2012.
33. Guo, Q., Li, L., Cheng, Y., Jiao, Y., Xu, C., Laboratory Evaluation on Performance of Diatomite and Glass Fiber Compound Modified Asphalt Mixture. Mater. Des., 66, 51-59, 2015.
34. Orhan, F., Bituminous Mixtures Laboratory Studies, Superstructure Development Branch Directorate, General Directorate of Highways, Ankara, 2012.
35. TS EN 1426, Bitumen and Bituminous Binders - Determination of Needle Penetration, 2015.
36. TS EN 1427, Bitumen and Bituminous Binders - Determination of the Softening Point - Ring and Ball method, 2015.
37. Kok, B.V., Yılmaz, M., Akpolat, M., Evaluation of the Conventional and Rheological Properties of SBS+Sasobit Modified Binder. Constr. Build. Mater. 63, 174–179, 2014.
38. Yaacob, H., Mughal, M. A., Jaya, R. P., Hainin, M. R., Jayanti, D. S., Wan, C. N. C., Rheological Properties of Styrene Butadiene Rubber Modified Bitumen Binder. Jurnal Teknologi, 78 (7–2), 121–126, 2016.
39. Hunter, R. N., Self, A., Read, J., The Shell Bitumen Handbook. ICE Publishing, London, 2015.
40. ASTM D6648, Standard Test Method for Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR), ASTM International, West Conshohocken, PA, USA, 2016.
41. Lu, X., Isacsson, U. L. F., Ekblad, J., Influence of Polymer Modification on Low Temperature Behaviour of Bituminous Binders and Mixtures. Mater. Struct., 36, 652-656, 2003.
42. Kumandas, A., Cavdar, E., Sahan, N., Kok, B. V., Pancar, E. B., Oruc, S., Investigation of Rutting and Low Temperature Cracking Behavior of Reactive Ethylene Terpolymer and Waste Cooking Oil Modified Bitumen. Turk. J. Civ. Eng., 35(4), 2024.
43. AASHTO M 320, Standard Specification for Performance-Graded Asphalt Binder, American Association of State Highway and Transportation Officials, Washington, DC, USA, 2023.
44. Asphalt Institute, Use of the Delta Tc Parameter to Characterize Asphalt Binder Behavior, State-of-the-Knowledge, IS-240, Asphalt Institute Technical Advisory Committee, Lexington, KN, USA, 2019.
45. AASHTO T 283-21, Standard Method of Test for Resistance of Compacted Asphalt Mixtures to Moisture-Induced Damage, 2021.
46. Hoare, T. R., Hesp, S. A., Low-temperature Fracture Testing of Asphalt Binders: Regular and Modified Systems. Transp. Res. Rec., 1728(1), 36-42, 2000.
47. Ishaq, M. A., Giustozzi, F., Correlation Between Rheological Tests on Bitumen and Asphalt Low Temperature Cracking Tests. Constr. Build. Mater., 320, 21, 126109, 2022.
48. Fakhri, M., The Effects of Nano Zinc Oxide (ZnO) and Nano Reduced Graphene Oxide (RGO) on Moisture Susceptibility Property of Stone Mastic Asphalt (SMA). Case Stud. Constr. Mater., 15, e00655, 2021.
49. Hamedi, G. H., Investigating the Use of Nano Coating Over the Aggregate Surface on Moisture Damage of Asphalt Mixtures. Int. J. Civ. Eng., 16, 659-669, 2018.
50. Hamedipour, A. M., Shafabakhsh, G., Sadeghnejad, M., The Impact of Nano-TiO2 Particles on the Moisture Susceptibility and Fracture Toughness of HMA under Mixed-Mode I/II Loading and Various Crack Geometry and Temperatures. J. Mater. Civ. Eng., 35(3), 04022444, 2023.
51. Deb, P., Singh, K. L., Accelerated Curing Potential of Cold Mix Asphalt Using Silica Fume and Hydrated Lime as Filler. Int. J. Pavement Eng., 1-21, 2022.
52. Yousefi, A. A., Haghshenas, H. F., Underwood, B. S., Harvey, J., Blankenship, P., Performance of Warm Asphalt Mixtures Containing Reclaimed Asphalt Pavement, an Anti-stripping Agent, and Recycling Agents: A Study Using a Balanced Mix Design Approach. Constr. Build. Mater., 363, 129633, 2023.
53. Delgadillo, R., Nonlinearity of Asphalt Binders and The Relationship with Asphalt Mixture Permanent Deformation. Ph.D. Thesis, University of Wisconsin - Madison, Madison, USA, 2008.
54. Centeno, M., Sandoval, I., Cremades, I., Alarcon, J., Assessing Rutting Susceptibility of Five Different Modified Asphalts in Bituminous Mixtures Using Rheology and Wheel Tracking Test, Transp. Res. Rec., 08-0705, 2008.
55. Aksoy, A., Iskender, E., Creep in Conventional and Modified Asphalt Mixtures. Proc. Inst. Civ. Eng. Transp., 161(4), 185-195, 2008.
56. Tapkin, S., Çevik, A., Uşar, U., Prediction of Rutting Potential of Dense Bituminous Mixtures with Polypropylene Fibers via Repeated Creep Testing by Using Neuro-Fuzzy Approach. Periodica Polytechnica Civil Engineering, 56(2), 253-266, 2012.
57. BS EN 12697-25, Bituminous mixtures, Test Methods Cyclic Compression Test, 2016.
58. Krcmarik, M., Characteristics and Prediction of The Low Temperature Indirect Tensile Strengths of Michigan Asphalt Mixtures, Master’s Thesis, Michigan State University, USA, 2013.
59. Yue, Y., Moustafa, A., Dong, L., Ahmed, K., Josephine, M., Tangbing, C., Evaluation of the Properties of Asphalt Mixes Modified with Diatomite and Lignin Fiber: A Review. Materials, 12 (3), 400, 2019.
60. Zhang, Y. B., Zhu, H., Wang, G., Chen, T., Evaluation of Low Temperature Performance for Diatomite Modified Asphalt Mixture. Advanced Materials Research, 413, 246-251, 2011.
61. Cheng, Y., Yu, D., Tan, G., Zhu, C., Low-Temperature Performance and Damage Constitutive Model of Eco-Friendly Basalt Fiber–Diatomite-Modified Asphalt Mixture under Freeze–Thaw Cycles. Materials, 11(11), 2148, 2018.
62. Zhu, C., Luo, H., Tian, W., Teng, B., Qian, Y., Ai, H., Xiao, B., Investigation on Fatigue Performance of Diatomite/Basalt Fiber Composite Modified Asphalt Mixture. Polymer, 14(3), 414, 2022.
63. Liu, H. B., Liu, H., Wei, H. B., Chai, C., Zhu, B., Laboratory Evaluation on the Road Performance of Diatomite Modified Porous Asphalt Mixture. In Jour. of Phys.: Confer. Seri., 2047(1), 012028. IOP Publishing, 2021.
64. Du, T., Song, P., Liu, L., Experimental Study on Activated Diatomite Modified Asphalt Pavement in Deep Loess Area. Processes, 10(6), 1227, 2022.