Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II

Dursun Ali Kose; Hasan Icbudak; Hacali Necefoglu

Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II

Year 2007, Volume: 35 Issue: 2, 123 - 128, 01.04.2007

Dursun Ali Kose Hasan Icbudak Hacali Necefoglu

https://izlik.org/JA94PU46CX

Abstract

Nicotinamide-acetylsalicylato complexes of Co II , Ni II , Cu II , and Zn II were synthesised and their structural properties were investigated by employing elemental analysis, magnetic susceptibilitiy, solid state UV-vis, direct injectionprobe mass, FTIR and thermoanalytic TG-DTG methods. It was found that ratio of metal:ligand:ligand is 1:2:2 and thedecomposition of each complex starts with dehydration and follows by decomposition of the nicotinamide and acetylsalicylato, respectively. The thermal dehydration of the complexes takes place in steps from one to two. The decomposition mechanism and thermal stability of the investigated complexes are interpreted in terms of their structures. Thefinal decomposition products are found to be the respective metal oxides

Keywords

Nicotinamide , N , N-diethylnicotinamide , acetylsalicylato , Thermal decomposition , metal complexes

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There are 35 citations in total.

Details

Primary Language	English
Authors	Dursun Ali Kose This is me Hasan Icbudak This is me Hacali Necefoglu This is me
Publication Date	April 1, 2007
IZ	https://izlik.org/JA94PU46CX
Published in Issue	Year 2007 Volume: 35 Issue: 2

Cite

APA	Kose, D. A., Icbudak, H., & Necefoglu, H. (2007). Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. Hacettepe Journal of Biology and Chemistry, 35(2), 123-128. https://izlik.org/JA94PU46CX
AMA	1.Kose DA, Icbudak H, Necefoglu H. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC. 2007;35(2):123-128. https://izlik.org/JA94PU46CX
Chicago	Kose, Dursun Ali, Hasan Icbudak, and Hacali Necefoglu. 2007. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry 35 (2): 123-28. https://izlik.org/JA94PU46CX.
EndNote	Kose DA, Icbudak H, Necefoglu H (April 1, 2007) Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. Hacettepe Journal of Biology and Chemistry 35 2 123–128.
IEEE	[1]D. A. Kose, H. Icbudak, and H. Necefoglu, “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”, HJBC, vol. 35, no. 2, pp. 123–128, Apr. 2007, [Online]. Available: https://izlik.org/JA94PU46CX
ISNAD	Kose, Dursun Ali - Icbudak, Hasan - Necefoglu, Hacali. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry 35/2 (April 1, 2007): 123-128. https://izlik.org/JA94PU46CX.
JAMA	1.Kose DA, Icbudak H, Necefoglu H. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC. 2007;35:123–128.
MLA	Kose, Dursun Ali, et al. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry, vol. 35, no. 2, Apr. 2007, pp. 123-8, https://izlik.org/JA94PU46CX.
Vancouver	1.Dursun Ali Kose, Hasan Icbudak, Hacali Necefoglu. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC [Internet]. 2007 Apr. 1;35(2):123-8. Available from: https://izlik.org/JA94PU46CX

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