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Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II

Year 2007, Volume: 35 Issue: 2, 123 - 128, 01.04.2007

Dursun Ali Kose Hasan Icbudak Hacali Necefoglu

Abstract

Nicotinamide-acetylsalicylato complexes of Co II , Ni II , Cu II , and Zn II were synthesised and their structural properties were investigated by employing elemental analysis, magnetic susceptibilitiy, solid state UV-vis, direct injectionprobe mass, FTIR and thermoanalytic TG-DTG methods. It was found that ratio of metal:ligand:ligand is 1:2:2 and thedecomposition of each complex starts with dehydration and follows by decomposition of the nicotinamide and acetylsalicylato, respectively. The thermal dehydration of the complexes takes place in steps from one to two. The decomposition mechanism and thermal stability of the investigated complexes are interpreted in terms of their structures. Thefinal decomposition products are found to be the respective metal oxides

Keywords

Nicotinamide N N-diethylnicotinamide acetylsalicylato Thermal decomposition metal complexes

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There are 35 citations in total.

Details

Primary Language English
Journal Section Research Article
Authors

Dursun Ali Kose This is me

Hasan Icbudak This is me

Hacali Necefoglu This is me

Publication Date April 1, 2007
Published in Issue Year 2007 Volume: 35 Issue: 2

Cite

APA Kose, D. A., Icbudak, H., & Necefoglu, H. (2007). Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. Hacettepe Journal of Biology and Chemistry, 35(2), 123-128.
AMA Kose DA, Icbudak H, Necefoglu H. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC. April 2007;35(2):123-128.
Chicago Kose, Dursun Ali, Hasan Icbudak, and Hacali Necefoglu. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry 35, no. 2 (April 2007): 123-28.
EndNote Kose DA, Icbudak H, Necefoglu H (April 1, 2007) Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. Hacettepe Journal of Biology and Chemistry 35 2 123–128.
IEEE D. A. Kose, H. Icbudak, and H. Necefoglu, “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”, HJBC, vol. 35, no. 2, pp. 123–128, 2007.
ISNAD Kose, Dursun Ali et al. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry 35/2 (April 2007), 123-128.
JAMA Kose DA, Icbudak H, Necefoglu H. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC. 2007;35:123–128.
MLA Kose, Dursun Ali et al. “Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II”. Hacettepe Journal of Biology and Chemistry, vol. 35, no. 2, 2007, pp. 123-8.
Vancouver Kose DA, Icbudak H, Necefoglu H. Synthesis and Characterization of the Nicotinamide-Acetylsalicylato Complexes of Co II , Ni II , Cu II , and Zn II. HJBC. 2007;35(2):123-8.

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