Layered Yttrium Oxide Reinforced Graphene Oxide Electrode Surface for Voltammetric Determination of Paracetamol

Year 2024, Volume: 52 Issue: 2, 63 - 75, 01.04.2024

Vildan Şanko , İpek Ömeroğlu

https://doi.org/10.15671/hjbc.1372446

Abstract

In this study, graphene oxide (GO) was synthesized by the Hummers method starting from graphite. Also, the sol-gel method synthesized yttrium oxide (YO) and was characterized by FTIR, XRD, SEM, and TEM techniques. The sensor performance of the modified electrode against the paracetamol analyte was investigated by cyclic voltammetry (CV) and differential pulse voltammetry (DPV). As a result of the optimized voltammetric methods calculated the linear working range was 0.25-10.0 µM and the LOD value was 19.0 nM. With the DPV method, advanced analytical parameters such as stability, reproducibility, and selectivity were studied. Moreover, the performance of the new sensor to detect paracetamol in tablet real samples was examined.

Keywords

Paracetamol detection, rare earth metals, carbon-based materials, electrochemical method.

Thanks

The authors especially thank Assoc. Prof. Dr. Ahmet Şenocak and Assoc. Prof. Dr. Süreyya Oğuz Tümay for their valuable contributions to this study.

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