Electrochemical sensitivity, selectivity, and sensory properties of a natural polymer-supported titanium nanocomposite electrode towards lysine amino acid

Abstract

In this study, chitosan (Chit) supported titanium (Ti) nanoparticles (Ti@Chit NPs) were synthesized by chemical method. Ti@Chit NPs were calculated to be 7.275 ± 2.15 nm and 18.629 nm according to scanning electron microscopy (SEM) and atomic force microscopy (AFM) results, respectively. The synthesized NPs were modified to the electrode and a sensitivity study was carried out against lysine amino acid. It has been determined that the Ti@Chit electrode has a catalytic performance against the amino acid lysine. The limit of detection (LOD) value is estimated to average 0.0041 µM.

Keywords

• Lysine
• Sensor
• Ti@Chit NPs

Doğal polimer destekli bir titanyum nanokompozit elektrodun lizin amino aside karşı elektrokimyasal duyarlılığı, seçiciliği ve duyusal özellikleri

Abstract

Bu çalışmada kitosan (Chit) destekli titanyum (Ti) nanoparçacıkları (Ti@Chit NPs) kimyasal yöntemle sentezlendi. Ti@Chit NP'leri taramalı elektron mikroskobu (SEM) ve atomik kuvvet mikroskobu (AFM) sonuçlarına göre sırasıyla 7,275 ± 2,15 nm ve 18,629 nm olarak hesaplanmıştır. Sentezlenen NP'ler elektroda modifiye edildi ve lizin amino aside karşı bir duyarlılık çalışması yapıldı. Ti@Chit elektrodunun amino asit lizine karşı katalitik bir performansa sahip olduğu belirlenmiştir. Tespit sınırı (LOD) değerinin ortalama 0,0041 µM olduğu tahmin edilmektedir.

Keywords

• Lizin
• Ti@Chit NPs
• Sensör

References

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