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Dual optimization for instant soluble carob pod powder production by response surface method

Year 2023, , 408 - 419, 15.04.2023

Mehmet Şükrü Karakuş , Merve Akalan , Melike Yücetepe , Kamile Bayrak Akay , Asliye Karaaslan , Bülent Başyiğit , Mehmet Karaaslan

https://doi.org/10.28948/ngumuh.1205063
Cited By: 1

Abstract

In this study, bioactive compounds (phenolics) from carob pod were extracted by using microwave assisted extraction method. Spray drying technique was performed for the conversion of the resulting extract into powder form. Microwave assisted extraction and spray drying steps were optimized using response surface methodology. In the extraction stage, the effect of solvent temperature and extraction time on the total phenolic content was evaluated. Optimum extraction conditions (total phenolic content: 84.48 mg GAE/g) were determined as 55 °C and 26 min. For the final powder production, the maximum process yield (48.00%) was obtained at the point where the spray dryer inlet temperature was 184 °C and the flow rate was 8 mL/min. The presence of phenolic structures in final product was verified by FTIR spectroscopy. Total phenolic content (15.37 mg GAE/g) and antioxidative behavior (DPPH: 0.63 mmol TE/g, ABTS: 0.30 mmol TE/g, FRAP: 0.06 mmol TE/g, CUPRAC: 0.05 mmol TE)/g) of carob powders were evaluated.

Keywords

Keçiboynuzu kabuğu Mikrodalga destekli ekstraksiyon Püskürtmeli kurutma Toplam fenolik madde Antioksidan aktivite

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Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu

Year 2023, , 408 - 419, 15.04.2023

Mehmet Şükrü Karakuş , Merve Akalan , Melike Yücetepe , Kamile Bayrak Akay , Asliye Karaaslan , Bülent Başyiğit , Mehmet Karaaslan

https://doi.org/10.28948/ngumuh.1205063
Cited By: 1

Abstract

Bu çalışmada, mikrodalga destekli ekstraksiyon yöntemi kullanılarak keçiboynuzu kabuğundan elde edilen biyoaktif maddeler (fenolikler) püskürtmeli kurutma tekniği ile çözünür toz forma dönüştürülmüştür. Mikrodalga destekli ekstraksiyon ve püskürtmeli kurutma adımları yanıt yüzey metodolojisi kullanılarak optimize edilmiştir. Ekstraksiyon aşamasında, solvent sıcaklığının ve ekstraksiyon süresinin toplam fenolik madde miktarı üzerine etkisi değerlendirilmiştir. Optimum ekstraksiyon koşulları (toplam fenolik madde miktarı: 84.48 mg GAE/g), 55 °C ve 26 dk olarak belirlenmiştir. Nihai toz üretimi için ise maksimum işlem verimi (%48.00) püskürtmeli kurutucu giriş sıcaklığının 184 °C ve akış hızının 8 mL/dk olduğu noktada sağlanmıştır. Son üründeki fenolik maddelerin varlığı FTIR spektroskopisi ile doğrulanmıştır. Elde edilen tozların toplam fenolik madde miktarı (15.37 mg GAE/g) ve antioksidatif davranışı (DPPH: 0.63 mmol TE/g, ABTS: 0.30 mmol TE/g, FRAP: 0.06 mmol TE/g, CUPRAC: 0.05 mmol TE/g) araştırılmıştır.

Keywords

Keçiboynuzu kabuğu Mikrodalga destekli ekstraksiyon Püskürtmeli kurutma Toplam fenolik madde Antioksidan aktivite

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There are 65 citations in total.

Details

Primary Language Turkish
Subjects Food Engineering
Journal Section Food Engineering
Authors

Mehmet Şükrü Karakuş 0000-0002-1805-8206

Merve Akalan 0000-0002-3926-245X

Melike Yücetepe 0000-0002-9581-225X

Kamile Bayrak Akay 0000-0001-7976-377X

Asliye Karaaslan 0000-0002-3834-0647

Bülent Başyiğit 0000-0002-6617-1836

Mehmet Karaaslan 0000-0001-8097-9535

Publication Date April 15, 2023
Submission Date November 15, 2022
Acceptance Date February 15, 2023
Published in Issue Year 2023

Cite

APA Karakuş, M. Ş., Akalan, M., Yücetepe, M., Bayrak Akay, K., et al. (2023). Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, 12(2), 408-419. https://doi.org/10.28948/ngumuh.1205063
AMA Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. April 2023;12(2):408-419. doi:10.28948/ngumuh.1205063
Chicago Karakuş, Mehmet Şükrü, Merve Akalan, Melike Yücetepe, Kamile Bayrak Akay, Asliye Karaaslan, Bülent Başyiğit, and Mehmet Karaaslan. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12, no. 2 (April 2023): 408-19. https://doi.org/10.28948/ngumuh.1205063.
EndNote Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M (April 1, 2023) Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12 2 408–419.
IEEE M. Ş. Karakuş, M. Akalan, M. Yücetepe, K. Bayrak Akay, A. Karaaslan, B. Başyiğit, and M. Karaaslan, “Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu”, NÖHÜ Müh. Bilim. Derg., vol. 12, no. 2, pp. 408–419, 2023, doi: 10.28948/ngumuh.1205063.
ISNAD Karakuş, Mehmet Şükrü et al. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi 12/2 (April 2023), 408-419. https://doi.org/10.28948/ngumuh.1205063.
JAMA Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. 2023;12:408–419.
MLA Karakuş, Mehmet Şükrü et al. “Kullanıma hazır Suda çözünebilir keçiboynuzu kabuğu Tozu üretiminin yanıt yüzey yöntemi Ile çift aşamalı Optimizasyonu”. Niğde Ömer Halisdemir Üniversitesi Mühendislik Bilimleri Dergisi, vol. 12, no. 2, 2023, pp. 408-19, doi:10.28948/ngumuh.1205063.
Vancouver Karakuş MŞ, Akalan M, Yücetepe M, Bayrak Akay K, Karaaslan A, Başyiğit B, Karaaslan M. Kullanıma hazır suda çözünebilir keçiboynuzu kabuğu tozu üretiminin yanıt yüzey yöntemi ile çift aşamalı optimizasyonu. NÖHÜ Müh. Bilim. Derg. 2023;12(2):408-19.

Cited By

Domates Kabuğu Fenolikleri: Mikrodalga Destekli Ekstraksiyon Koşullarının Optimizasyonu ve Mikroenkapsülasyonu
Journal of the Institute of Science and Technology
https://doi.org/10.21597/jist.1290953

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